• Title/Summary/Keyword: SrO

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Fabrication of Bi-2223 high-Tc superconducting current lead (Bi-2223 고온초전도 전류리드의 제조)

  • Ha, D.W.;Oh, S.S.;Ryu, K.S.;Chang, H.M.
    • Proceedings of the KIEE Conference
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    • 1996.07c
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    • pp.1660-1662
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    • 1996
  • Superconducting current lead is one of the promising applications of the oxide high-Tc superconductors, because they have the advantage of decreasing heat conduction to low temperature region, comparing with a conventional cooper alloy lead. High critical current density is a key factor for the applications such as current lead. $(Bi,Pb)_{2}Sr_{2}Ca_{2}Cu_{3}O_{x}$ high Tc superconductor hase been investigated in terms of critical current density. Bi-2223 superconducting current lead made by CIP and solid state sintering process. Bi-2223 current lead that heat treated at $836\;^{\circ}C$ for 240 h in 1/13 $PO_2$ had over $500\;A/cm^2$ of critical current density at 77K. We knew that the superconducting properties of tube type current leads were better than rods type of them. And we investigated the relation of Bi-2223 formation and heat treatment condition by XRD and SEM analysis.

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Change of Luminescent Properties of Phosphors Through pH and Rw Control in Sol-gel Reaction (졸-겔반응에서 pH 및 Rw제어를 통한 Sr3-xMgSi2O8:EUx (0.01≤x≥0.1) 형광체의 발광특성 변화)

  • Ahn Joong-In;Han Cheong-Hwa;Kim Chang-Hae
    • Korean Journal of Materials Research
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    • v.15 no.6
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    • pp.419-425
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    • 2005
  • In this paper, we describe the luminescent properties of the phosphors synthesized via sol-gel technique. When the phosphor prepared by sol-gel technique, reaction factors, such as pH condition, $R_w$ and drying temperature affected the luminescent intensity, particle size and morphology of final product. Therefore, we attempt to control these reaction factors in order to improve the luminescent efficiency of phosphors. As a result of our study, when the acid catalyst (HCl) was used, emission intensity was higher than the case of base catalyst $(NH_4OH)$. The product prepared at $R_w=60$ indicated the maximum intensity. As the increase of the $R_w$ value, the particle was agglomerated and emission intensity was decreased. Finally, optimum drying temperature of gel was found to be$ 180^{\circ}C$.

The electrical and structual characteristics of BSCCO film by MOD method (MOD법을 제작된 BSCCO 고온초전도체의 구조적 전기적 특성)

  • Kim, Sun-Mi;Yoon, Soon-Il;Park, Mi-Hwa;Lee, Kie-Jin;Cha, Deok-Joon
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07a
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    • pp.553-556
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    • 2003
  • 금속유기물 용액 증착법(MOD)법은 금속유기물 용액을 스핀 코팅하여 고온 열처리를 통해 대면적의 고온 초전도 박막을 만들 수 있으며, 고가의 진공 시스템이 필요하지 않기 때문에 매우 경제적인 박막 증착 방법이다. 본 연구에서는 MOD법을 이용해서 고온초전도체 마이크로파 필터나 터널접합 소자와 같은 전자 소자 응용 연구를 위해 요구되는 높은 임계전류 특성을 갖도록 박막 성장 조건을 변화시켜서 제작된 고온 초전도체 Bi2Sr2CaCu2O8+d (BSCCO2212) 박막을 제작하였다. 박막 특성은 x-ray diffraction (XRD), scanning electron microscope (SEM)으로 표면적, 구조적 특성을 관찰하고 저항-온도 (R-T) 변화 및 전류-전압 (I-V) 특성 측정을 통해 전기적 특성을 연구하여 임계전류를 향상 시킬 수 있는 박막제작 조건에 관해 논의하였다.

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Superconducting Joint of Multi-filament BSCCO(2223) Tapes by using Single-filament Tape (BSCCO(2223) 단심 초전도 선재를 이용한 다심 초전도 선재의 접합공정 연구)

  • 김규태;김정호;장석헌;주진호;강형구;고태국;하홍수;오상수
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.16 no.10
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    • pp.923-930
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    • 2003
  • We jointed Bi(Pb)-Sr-Ca-Cu-O multifilament tapes and evaluated their electrical and mechanical properties. In order to improve connectivity of multifilaments, one or two single-filament tape was inserted between two multifilament tapes. The critical current ratio(CCR) and n-value of the jointed tapes were evaluated as a function of uniaxial pressure. It was observed that critical current ratio and n-value were 24.8-29.0% and 2.5-2.8 for MM lap-jointed tape. On the other hand, the corresponding values were improved to 24.7-53.9% and 3.1-4.2 for MSM jointed tape, and 63.4-76.0% and 3.4-5.1 for double MS:vr lap-jointed tape, respectively. The highest electrical properties of double MSM lap-jointed tape are considered to be owing to the presence of single core, causing better interconnections of multifilaments between the two tapes. The mechanical property of jointed tape was evaluated and correlated to the microstructural evolution. The strength of jointed tapes was 44-64% less than that of the unjoined tape. The strain tolerance of jointed tape was also reduced compared to that of the unjoined tape. These lower mechanical properties of jointed tape are probably due to the induced nonuniform microstructure such as the existence of cracks and Ag-intrusion in the joined region.

A Study on the Fabrication of Superconductor Using Pyrolysis Methods for Electric power Machinery (열분해법에 의한 전력기기용 초전도 합성 기술에 관한 연구)

  • Lee, Sang-Heon;Lee, Young-Hie
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.153-154
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    • 2005
  • A high Tc superconducting with a nominal composition of $Bi_2Sr_2Ca_2Cu_3O_Y$ was prepared by the citarte method. The solid precursor produced by the dehydration of the gel at 120$^{\circ}C$ for 12h is not in the amorphous state as expected but in a crystalline state. X-ray diffraction peaks of nearly the same angular position as the peaks of high Tc phase were observed in the precursor. After pyrolysis at 400$^{\circ}C$ and calcination at 840$^{\circ}C$ for 4h, the (001)peak of the high Tc phase was cleary observed. Experimental results suggest that the intermediate phase formed before the formation of the superconducting phase may be the most important factro in determining whether it is easy to form the high Tc phase or not, because the nucleation barriers of the two superconducting phase may be altered by the variation of the crystal structures of those intermediate phase.

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Dry etching properties of PST thin films using chlorine-based inductively coupled plasma (Chlorine-based 유도결합 플라즈마를 이용한 PST 박막의 건식 식각 특성)

  • Kim, Gwan-Ha;Kim, Kyoung-Tae;Kim, Dong-Pyo;Lee, Cheol-In;Kim, Chang-Il
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07a
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    • pp.400-403
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    • 2003
  • Etching characteristics of (Pb,Sr)$TiO_3$(PST) thin films were investigated using inductively coupled chlorine based plasma system as functions of gas mixing ratio, RF power and DC bias voltage. It was found that increasing of Ar content in gas mixture lead to sufficient increasing of etch rate and selectivity of PST to Pt. The maximum etch rate of PST film is $562\;{\AA}$/min and the selectivity of PST film to Pt is 0.8 at $Cl_2/(Cl_2+Ar)$ of 20 %. It was proposed that sputter etching is dominant etching mechanism while the contribution of chemical reaction is relatively low due to low volatility of etching products.

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Construction and Operation of High-$T_c$ Scanning SQUID Microscope

  • Baeka, B.;Kim, Ho-chul;Khim, Z.G.;Lee, S.M.;Moon, S.H.;Oh, B.
    • Progress in Superconductivity
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    • v.1 no.1
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    • pp.20-25
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    • 1999
  • We constructed a high-$T_c$ scanning SQUID microscope (SSM) operating in the liquid nitrogen. We used a washer-type YBCO SQUID with inner and outer dimensions of $12{\mu}m$ and $36{\mu}m$, respectively, which was grown on the $SrTiO^3$ bicrystal substrate. The sample, rather than SQUID, was scanned using two stepping motors. We also developed readout electronics, stepping motor controller, and the software for system control and data display. We took images of various samples using our SSM and found that the spatial resolution is about $40{\mu}m$ and noise level is lower than $10^{-7}T/{\surd}Hz$ at 100 Hz and higher at lower frequencies. The noise level was much higher than that of a typical SQUID due to the other coupling from the electric parts. We present a simple argument on the inductive coupling between the sample and the SQUID which should be under-stood for the proper interpretation of the obtained images. By comparing the measured data with the simulation results the gap between the SQUID and the sample is estimated to be $40{\mu}m$.

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Josephson Vortex Dynamics in Tilted Magnetic Fields (경사 자기장 하에서의 조셉슨 볼텍스 동역학)

  • Jin, Yong-Duk;Ki, Dong-Keun;Lee, Hu-Jong
    • Progress in Superconductivity
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    • v.9 no.2
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    • pp.140-145
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    • 2008
  • We report on the Josephson vortex dynamics in $Bi_2Sr_2CaCuO_{8+\delta}$ natural Josephson junctions by c-axis tunneling measurements. Beside the quasiparticle branches in the current-voltage characteristics, a new set of multiple branches, referred to as Josephson-vortex-flow branches (JVFBs), are observed. The JVFBs emerge in an in-plane magnetic field above $H_0\;=\;{\Phi}_0/{\gamma}s^2$ and show highly hysteretic behavior, which can be explained in terms of the recently proposed dynamic-phase-separation model. In this work we examined the effect on the JVFBs by the presence of pancake vortices generated as the external magnetic field was applied slightly tilted from the in-plane direction. JVFBs were found to become larger and prominent with increasing pancake vortex density as the tilt angle increased, which were presumably caused by slowing down of a Josephson vortex lattice in the presence of pancake vortices.

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Effect of Slope Exposure on Winter Hardiness of Grasses (경사방향이 목초의 월동성에 미치는 영향)

  • 이주삼;천소을
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.14 no.2
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    • pp.93-98
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    • 1994
  • This experiment was canied out to investigated the effect of slope exposure on winter hardiness of grasses in mountainous pastures of Taekwalyong area The results obtained were summarized as follows; 1. Plant vigour(PV) before wintering influenced on the growth of next spring, field survival rates and winter hardiness of grasses. 2. The dry weight of plant per relative tiller appearance rates(DW/RTAR) was significantly negative correlated with plant vigour(PV) before wintering, but the weight of plant per relative tiller appearance rates(DW1 RTAR) were significantly positive correlated with the number of tiller per plant before wintering($NT_O$), number of tillers per plant of 1st cutting(NT), dry weight of plant(DW), field survival rates(SR) and relative tiller appearance rate(RTAR). 3. There ranking order of high winter hardiness of grasses, it were west(W), north-north west(NNW), eastsoutheast( ESE) and south-southwest(SSW) exposure, respectively.

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Study on deposition conditions of YBGO films grown by pulsed laser deposition (PLD 법에 의한 YBCO 박막의 증착 조건에 따른 특성)

  • Choi, S.J.;Jeong, J.K.;Park, Y.M.;Ko, R.K.;Song, K.J.;Park, C.;Yu, S.I.
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2003.02a
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    • pp.109-112
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    • 2003
  • The high temperature superconducting YBCO films were deposited on the SrTiO$_3$(100) single crystals to find out the proper deposition conditions of YBCO on biaxially-textured metal substrates. Different sets of the substrate temperature, oxygen partial pressure and laser fluence were used to investigate the effect of deposition conditions on the superconducting properties. The new apparatuses for measuring critical temperature (Tc) and critical current (Ic) were designed and manufactured, which were used to obtain Tc's and Ic's of the deposited films. The accuracy of the new apparatus was confirmed by comparing the results with those from SQUID magnetometer. The results on the YBCO films deposited on single crystal substrates which will be used to get the optimum deposition conditions of YBCO films in the coated conductor, are summarized in this report.

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