• Journal of Powder Materials
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• v.16 no.6
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• pp.403-409
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• 2009

Plasma spray forming is recently explored as a near-net-shape fabrication route for ultra-high temperature metals and ceramics. In this study, monolithic tungsten has been produced using an atmospheric plasma spray forming and subsequent high temperature sintering. The spray-formed tungsten preform from different processing parameters has been evaluated in terms of metallurgical aspects, such as density, oxygen content and hardness. A well-defined lamellae structure was formed in the as-sprayed deposit by spreading of completely molten droplets, with incorporating small amounts of unmelted/partially-melted particles. Plasma sprayed tungsten deposit had 84-87% theoretical density and 0.2-0.3 wt.% oxygen content. Subsequent sintering at 2500$^{\circ}C$ promoted the formation of equiaxed grain structure and the production of dense preform up to 98% theoretical density.

• Journal of Welding and Joining
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• v.14 no.1
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• pp.92-98
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• 1996

Al-Fe alloy layers on heated steel sheet were made by Al powder spray for 30 minutes at $700^{\circ}C$, $800^{\circ}C$ and $1000^{\circ}C$, respectively. As a results, for alloy layers formed at $700^{\circ}C$ and $800^{\circ}C$, main phases were brittle phase $FeAl_3 and Fe_2Al_5$, hardnesses were very high (Hv 700~800), corrosion resistances were good and surfaces were smooth, but wear resistances were bad. For alloy layer formed at $1000^{\circ}C$, main phase was ductile phase $Fe_3Al$, hardness was low (Hv 300~400), corrosion and wear resistances were excellent, but surface was rough. Therefore, alloy layers that formed at $700^{\circ}C$ and $800^{\circ}C$ were heat treated at $1000^{\circ}C$ for 10 minutes for the purpose of smooth surface and excellent wear resistance in this study. It was investigated that brittle phase $FeAl_3 and Fe_2Al_5$ of alloy layers fromed by Al powder spray at $700^{\circ}C$ and $800^{\circ}C$ turn into ductile phase $Fe_3Al$ by heat treated at $1000^{\circ}C$ for 10 minutes without changing smooth surface. It was concluded that the alloy layers formed by Al powder spray on heated steel sheet at $700^{\circ}C$ and $800^{\circ}C$ for 30 minutes and heat treated at $1000^{\circ}C$ for 10 minutes were excellent on wear and smooth surface.

• Journal of the Korean Society of Propulsion Engineers
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• v.3 no.3
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• pp.9-15
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• 1999

The Analysis of spray characteristics for combined spray group are necessary to develop large rocket engine. In this study, basic effects of interaction from spray fan formed by impinging jets were investigated with respect to mass distribution, droplet velocities and diameter. Patternater and PDPA are used for experimental apparatus. Water was used as a test fluid When momentum ratio is 1, effect of interaction from collision of spray fan on mass distribution are small. Also, effect of interaction from collision of spray fan on droplet velocities and diameter are small. But, droplet diameter is smaller near collision point due to second collision. Therefor, for the same momentum ratio from spray fan formed by impinging jets, we may neglect effect of interaction on mass distribution, droplet velocities and diameter.

• Korean Journal of Materials Research
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• v.22 no.4
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• pp.211-214
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• 2012

Optimal conditions for HA plasma spray-coating on Ti6Al4V alloy were investigated in order to obtain enhanced bone-bonding ability with Ti6Al4V alloy. The properties of plasma spray coated film were analyzed by SEM, XRD, surface roughness measurement, and adhesion strength test because the film's transformed phase and crystallinity were known to be influential to bone-bonding ability withTi6Al4V alloy. The films were formed by a plasma spray coating technique with various combinations of plasma power, spray distance, and auxiliary He gas pressure. The film properties were analyzed in order to determine the optimal spray coating parameters with which we will able to achieve enhanced bone-bonding ability with Ti6Al4V alloy. The most influential coating parameter was found to be the plasma spray distance to the specimen from the spray gun nozzle. Additionally, it was observed that a relatively higher film crystallinity can be obtained with lower auxiliary gas pressure. Moderate adhesion strength can be achievable at minimal plasma power. That is, adhesion strength is minimally dependent on the plasma power. The combination of shorter spray distance, lower auxiliary gas pressure, and moderate spray power can be recommended as the optimal spray conditions. In this study, optimal plasma spray coated films were formed with spray distance of 70 mm, plasma current of 800 A, and auxiliary gas pressure of 60 psi.

• Transactions of the Korean Society of Automotive Engineers
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• v.13 no.6
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• pp.70-76
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• 2005

A new stratified charge combustion system has been introduced and developed for GDI engines. Before this new GDI system, the stratified mixture was formed by a high pressure swirl injector. But, the special feature of new system is employed of a thin fan-shaped fuel spray formed by a slit type nozzle. Also, this system has been adopted a shell-shaped piston cavity. We made high pressure gasoline injection system and investigated the fan-shaped spray characteristics such as spray tip penetration, spray angle, SMD and velocities of droplets using PDPA(Phase Doppler Particle Analyzer) system and spray visualization system to obtain the concept of the new design and the fundamental data for the next generation GDI system. The experiment was performed at the injection pressures of 5 and 9MPa under the atmospheric condition.

• Proceedings of the Korean Society of Marine Engineers Conference
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• 2006.06a
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• pp.265-266
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• 2006

The chemical conversion coating formed on magnesium alloy investigated for low cost and harmless in environment by using the colloidal silica as the main component. The film formed in 298 K is thick, the film, which was thought combination of Si-O, was formed. The film formed in 313 K is thinner than that in 298 K. The quantity of film formed at high temperature such as 333 K and 353 K is smaller than dissolved quantity. At the anodic polarization experiment, corrosion resistance in sealing by hot water after chemical conversion treatment in basic solution condition get worse than that in comparison with basic solution condition. In salt spray test, the ratio of black rust on specimen that did not conducted chemical conversion treatment was five times or more compared with those of chemical conversion treated specimen. The film thickness of chemical conversion coating produced by alkali treatment process is thinner than in comparison with that of specimen produced in basic chemical conversion treatment solution condition. It is thought, however, that it showed good corrosion resistance during salt spray test because the area of microcracks is small.

• Transactions of Materials Processing
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• v.21 no.5
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• pp.330-335
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• 2012

Roll formed steel bolts are electrodeposited with Zn-Ni to protect themselves from corrosion. However, white storage stain or white rust(corrosion) is found on Zn-Ni electrodeposited surface of steel bolts when they are exposed to moisture. In this paper a new process is introduced to protect Zn-Ni electrodeposited steel bolt from white storage stain or white rust for a long time under the salt spray test and high humidity test conditions. The better corrosion resistance could be gotten by the additional process of Ni-P electroless deposition and heat treatment to conventional manufacturing method of Zn-Ni coated steel bolt. The corrosion resistance of Zn-Al powder slurry coated steel bolt showed better than that of Zn-Ni electrodeposited one.

• Journal of ILASS-Korea
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• v.7 no.4
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• pp.32-41
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• 2002

The breakup characteristics of liquid sheets formed by like-doublet injector were investigated in the cold-flow and atmospheric ambient pressure condition. The sheet breakup wavelength, which induces the sheet to be broken into ligaments, as well as the sheet breakup length, which is important for the flame location, was measured using a stroboscopic light. The liquid ligaments are formed intermittently after the breakup of sheet, and the wavelength of ligaments has been believed to have a relation to the combustion instability of liquid rocket engine. Therefore, the wavelength of ligaments and the breakup length of ligaments into fine drops were also measured. Since these spray characteristics are affected by the flow characteristics of two liquid jets before they impinge on each other, we focused on the effects of orifice internal flow such as the cavitation phenomenon that occurs inside the sharp-edged orifice. From the experimental results, we found that the liquid jet turbulence delays the sheet breakup and makes shorter wavelengths for both sheets and ligaments. Since the turbulent strength of sharp-edged orifice is stronger than that of round-edged orifice, the shape of orifice entrance results in large differences in the spray characteristics. Using these results, we proposed empirical models on the spray characteristics of the like-doublet injector, and these models are believed to provide some useful and actual data for designing liquid rocket combustors.

• Journal of Powder Materials
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• v.19 no.4
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• pp.317-321
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• 2012

In this study, Cu-5Ni-10Sn(wt%) spinodal alloy was manufactured by gas atomization spray forming, and the microstructural features and mechanical properties of Cu-5Ni-10Sn alloy have been investigated during homogenization, cold working and age-hardening. The spray formed Cu-5Ni-10Sn alloy consisted of an equiaxed microstructure with a mixture of solid solution ${\alpha}$-(CuNiSn) grains and lamellar-structure grains. Homogenization at $800^{\circ}C$ and subsequent rapid quenching formed a uniform solid solution ${\alpha}$-(CuNiSn) phase. Direct aging at $350^{\circ}C$ from the homogenized Cu-5Ni-10Sn alloy promoted the precipitation of finely distributed ${\gamma}$' or ${\gamma}-(Cu,Ni)_3Sn$ phase throughout the matrix, resulting in a significant increase in microhardness and tensile strength. Cold working prior to aging was effective in strengthening Cu-5Ni-10Sn alloy, which gave rise to a maximum tensile strength of 1165 MPa. Subsequent aging treatment slightly reduced the tensile strength to 1000-1100 MPa due to annealing effects.

• Journal of the Korean Society of Propulsion Engineers
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• v.1 no.1
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• pp.1-7
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• 1997

Experimental study was carried out to investigate the interaction effect between spray fan formed by gas/liquid swirl injector. Test variables were supply pressure and injector distance. Water and air were the simulant for the experiment. For water supply only; Collected water mass was concentrated at the lower part of the two spray fan, but this effect was reduced with increasing supply pressure. Both air and water supply1; Collected water mass was again concentrated at the lower part of the impingement point, but this effect was reduced when air/water supply pressure ratio was increased.