• Proceedings of the Korean Vacuum Society Conference
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• 2012.08a
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• pp.79-79
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• 2012

A high temperature and a low temperature plasma process technologies were developed and demonstrated for synthesis, hybrid formation, surface treatment and CVD engineering of nano powder. RF thermal plasma is used for synthesis of spherical nano particles in a diameter ranged from 10 nm to 100 nm. A variety of nano particules such as Si, Ni, has been synthesized. The diameter of the nano-particles can be controlled by RF plasma power, pressure, gas flow rate and raw material feed rate. A modified RF thermal plasma also produces nano hybrid materials with graphene. Hemispherical nano-materials such as Ag, Ni, Si, SiO2, Al2O3, size ranged from 30 to 100 nm, has been grown on graphene nanoplatelet surface. The coverage ranged from 0.1 to 0.7 has been achieved uniformly over the graphene surface. Low temperature AC plasma is developed for surface modification of nano-powder. In order to have a three dimensional and lengthy plasma treatment, a spiral type of reactor has been developed. A similar plasma reactor has been modfied for nano plasma CVD process. The reactor can be heated with halogen lamp.

• Transactions of Materials Processing
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• v.31 no.4
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• pp.207-213
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• 2022

In this study, variations in the microstructure and hardness of a low-carbon SCM415 steel with austenitizing temperature and cooling rate are investigated. When the austenitizing temperature is lower than the A₁ temperature (738.8 ℃) of the SCM415 steel, the microstructures of both the air-cooled and water-cooled specimens consist of ferrite and pearlite, which are similar to the microstructure of the initial specimen. When heat treatment is conducted at temperatures ranging from the A₁ temperature to the A₃ temperature (822.4 ℃), the microstructure of the specimen changes depending on the temperature and cooling rate. The specimens air- and water-cooled from 750 ℃ consist of ferrite and pearlite, whereas the specimen water-cooled from 800 ℃ consists of ferrite and martensite. At a temperature higher than the A₃ temperature, the air-cooled specimens consist of ferrite and pearlite, whereas the water-cooled specimens consist of martensite. At 650 ℃ and 700 ℃, which are lower than the A₁ temperature, the hardness decreases irrespective of the cooling rate due to the ferrite coarsening and pearlite spheroidization. At 750 ℃ or higher, the air-cooled specimens have smaller grain sizes than the initial specimen, but they have lower hardness than the initial specimen owing to the increased interlamellar spacing of pearlite. At 800 ℃ or higher, martensitic transformation occurs during water cooling, which results in a significant increase in hardness. The specimens water-cooled from 850 ℃ and 950 ℃ have a complete martensite structure, and the specimen water-cooled from 850 ℃ has a higher hardness than that water-cooled from 950 ℃ because of the smaller size of prior austenite grains.

• Journal of the Korean Society for Heat Treatment
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• v.37 no.3
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• pp.121-127
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• 2024

We investigate the effect of T6 heat treatment on the microstructure and mechanical properties of AA365 (Al-10.3Si-0.37Mg-0.6Mn-0.11Fe, wt.%) alloy fabricated by vacuum-assisted high pressure die casting by means of thermodynamic calculation, X-ray diffraction, scanning and transmission electron microscopy, and tensile tests. The as-cast alloy consists of primary Al (with dendrite arm spacing of 10~15 ㎛), needle-like eutectic Si, and blocky α-AlFeMnSi phases. The solution treatment at 490 ℃ induces the spheroidization of eutectic Si and increase in the fraction of eutectic Si and α-AlFeMnSi phases. While as-cast alloy does not contain nano-sized precipitates, the T6-treated alloy contains fine β' and β' precipitates less than 20 nm that formed during aging at 190℃. T6 heat treatment improves the yield strength from 165 to 186 MPa due to the strengthening effect of β' and β' precipitates. However, the β' and β' precipitates reduce the strain hardening rate and accelerate the necking phenomenon, degrading the tensile strength (from 290 to 244 MPa) and fracture elongation (from 6.6 to 5.0%). Fractography reveals that the coarse α-AlFeMnSi and eutectic Si phases act as crack sites in both the as-cast and T6 treated alloys.