• Title/Summary/Keyword: Specimen stability

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Study on the Hybridization of Polymer-macromers for the Dimensional Stabilization of Woody Materials (치수안정화를 위한 목질재료의 고분자 하이브리드화에 관한 연구)

  • Lim, Kie-Pyo;Cho, Chong-Su;Kim, Ik-Joo;Na, Eun-Sun
    • Journal of the Korean Wood Science and Technology
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    • v.23 no.4
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    • pp.1-9
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    • 1995
  • This study was carried out to experiment the dimensional stabilization of woods of red pine (Pinus densiflora S. et Z.) and sugi(Cryptomeria japonica D. Don) by vacuum impregnation of polyehtylene glycols(PEG) with mo. wt. 200, 400, 600, 1000; polypropylene glycols (PPG) with mo. wt. 425,725 ; PEG-acryloylates, and PPG-acryloylates synthesized, and then by water soaking. The results obtained are as follows: 1. The density of sapwood and heartwood was different from each other in both species. 2. The PEG and PEG-macromers with lower molecular weight by impregnation has increased the density of wood specimens more higher, thereby caused their higher volume expansion, and those with higher molecular weight than 600 has tended to down their density increment. 3. Before and after water soaking, the density decrease of specimen impregnated was high in woods impregnated with simple PEG and PPG, while lower in specimens impregnated with PEG-macromers and PPG-macromers. 4. So PEG-macromer was expected to hold the original dimension of decayed wood for antiques, but it was necessary to develop another penetration method as well as aqueous solvent.

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A Study on EPMA on Ni-Cr Alloy by Nb content for Porcelain Fused to Metal Crown (Nb이 첨가된 금속소부도재관용 Ni-Cr 합금 표면의 EPMA 관찰)

  • Kim, Chi-Young;Choi, Sung-Min;Cho, Hyeon-Seol
    • Journal of Technologic Dentistry
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    • v.28 no.1
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    • pp.19-26
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    • 2006
  • The effect of Nb on interfacial bonding characteristics of Ni-Cr alloy for porcelain fused to metal crown (PFM) has been studied in order to investigate oxide layer. A specimens of Ni-Cr alloy, which is 0.8mm in thickness, within the porcelain furnace of 1,000$^{\circ}C$ with four tests such as air, vacuum, air for 5 minutes and vacuum for 5 minutes in order to examine an oxide behavior of alloy surface generated by the adding of Nb to be controlled at a rate of 0, 1, 3 and 5. Oxide film was observed form of the fired specimens with scanning electron microscope (SEM), and at the same time it measured Electron Probe Micro Analyzer (EPMA). The result of this study were as follows: 1. Cr oxide film and Nb oxide film were observed from the surface of specimen to be controlled at a rate of Nb 1%. 2. Nb oxide film was observed from the interface of specimens to be controlled at a rate of Nb 1% and 3%. 3. The stability of oxide films that treated in air were more stable than treated under vacuum.

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The Preparation and Electrical Characteristics of BST Thin Film by Spin-Coating Method (회전코팅법을 이용한 BST 박막의 제조 및 전기적 특성에 관한 연구)

  • Ki, Hyun-Chul;Kim, Duck-Keun;Lee, Seung-Woo;Hong, Kyung-Jin;Lee, Jin;Kim, Tae-Sung
    • Proceedings of the KIEE Conference
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    • 1999.11d
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    • pp.918-920
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    • 1999
  • Recently, the ceramics of high permittivity are applied to DRAM and FRAM. In this study, (Ba, Sr)$TiO_3$ (BST) ceramics thin films were prepared by Sol-Gel method. BST solution was made and spin-coated on Pt/$SiO_2$/Si substrate at 4000[rpm] for 10 seconds. Coating process was repeated 3 times and then sintered at $750[^{\circ}C]$ for 30 minutes. Each specimen was analyzed structure and electrical characteristics. Thickness of BST ceramics thin films are about $2000[\AA]$. Dielectric constant and loss of thin films was little decreased at $1[kHz]{\sim}1[MHz]$. Dielectric constant and loss to frequency were 250 and 0.02 in BST3. In accordance with applied voltage, property of leakage current was stability when the was $0{\sim}3$[V]. According to voltage, leakage current was increased exponentially at $4{\sim}7$[V].

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A Study on the AC Interfacial Breakdown Properities of the Interface between Epoxy/EPDM with the variation of spreaded oil (도포된 오일의 변화에 따른 Epoxy/EPDM 계면의 교류 절연 파괴 특성에 관한 연구)

  • Bae, Duck-Kweon;Lee, Su-Kil;Jung, Il-Hyung;Lee, Jun-Eung
    • Proceedings of the KIEE Conference
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    • 1999.11d
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    • pp.897-899
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    • 1999
  • In this paper, the interfacial dielectric breakdown phenomenon of interface between Epoxy/EPDM (ethylene propylene diene terpolymer) was discussed, which affects stability of insulation system of power delivery devices. Specimen structure was designed by using MAGSOFT's FLUX2D based on the finite elements method. Design concepts is to reduce the effect of charge transport from electrode in the process of breakdown and to have the tangential electrical potential with the Epoxy/EPDM interface. AC interfacial breakdown phenomenon of was investigated by variation of interfacial conditions oil and temperature which are supposed to have influence on the interfacial breakdown strength. Interfacial breakdown strength was improved by spreading oil over interfacial surface. The decreasing ratio of the AC interfacial breakdown strength in non-oiled specimens was increased by the temperature rising and its of oiled specimens was not affected by temperature.

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A Study on Relationship Between Basic Frictional Angle and Mineral Composition for Granite Sample (화강암 시험편의 광물조성과 기본마찰각의 상관성에 관한 연구)

  • Lee, Bong-Hyun;Lee, Seung-Joong;Choi, Sung-Oong
    • Tunnel and Underground Space
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    • v.24 no.1
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    • pp.32-45
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    • 2014
  • Basic frictional angle is a parameter that can estimate shear strength of rock, and is a design parameter employed in slope stability analysis. Basic frictional angle generates various results in accordance with mineral composition, apart from rock surface roughness itself. This paper describes the correlation of basic frictional angle and mineral composition. The basic frictional angle is measured with the aid of the modified tilt testing apparatus, and its reliability is improved by the statistical method. Also, mineral composition is identified through the photographic analysis on rock specimen, and verified through the thin section analysis.

Physical and Mechanical Properties of Local Styrax Woods from North Tapanuli in Indonesia

  • Iswanto, Apri Heri;Susilowati, Arida;Azhar, Irawati;Riswan, Riswan;Supriyanto, Supriyanto;Tarigan, Joel Elpinta;Fatriasari, Widya
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.4
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    • pp.539-550
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    • 2016
  • The objective of this research was to evaluate physical and mechanical properties of three species of Styrax woods from North Tapanuli in Indonesia. The woods were more than 15 years old. Physical properties such as specific gravity, green moisture content, and volume shrinkage were determined by the procedures based on BS-373 standard for small clear specimen. Furthermore, mechanical properties, including modulus of rupture, modulus of elasticity, compression parallel to grain and hardness were also tested according to the standard. Along the stem direction, the edge section had better properties compared with those near the pith section. And the base section had also better properties than upper section. Based on the specific gravity, all of the Styrax woods in this research were classified into III-IV strength classes. A good dimensional stability was demonstrated by the value of the tangential and radial ratio which reached one. With the consideration of the mechanical properties, Styrax woods were suitable use for raw materials of light construction, furniture and handy craft.

Structural Properties of Steel-glulam Composite Column

  • Jang, Sang-Sik;Kim, Yun-Hui;Shin, Il-Joong
    • Journal of the Korean Wood Science and Technology
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    • v.38 no.5
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    • pp.399-404
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    • 2010
  • A new green home designed to save money while at the same time saving the environment with some of the finest green features available in the market. Composite column composed of structural steel and structural glued laminated timber is avery Eco-friendly building products for design building because that use recycled or second hand. For compare to compressive strength of structural glued laminated timber (glulam), structural steel, and composite column (steel-glulam), tested compressive strength of each specimen. 1) structural glued laminated timber : Theoretical compressive strength is 151.6 kN similar to elastic limits. 2) structural steel (H type) : Theoretical compressive strength is 148.2 kN little under the elastic limits. 3) structural steel (D type) : Theoretical compressive strength is 147.3 kN upper than the elastic limits. 4) composite column : Actual elastic limits are about 600 kN. Result in, composite column improve compressive strength of Structural steel column and provide structural stability of the building.

The Effect of Adittives on the Sintering Properties of Barium Titanate Powder Prepared by Self-propagating High-temperature Synthesis (자전연소합성법에 의해 제조된 BaTiO3 분말의 소결특성에 미치는 첨가제의 영향)

  • Lim Sung-Jae;Shin Chang-Yun;Won Hyung-Il;Won Chang-Whan
    • Journal of Powder Materials
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    • v.13 no.2 s.55
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    • pp.129-137
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    • 2006
  • In this study, high purity fine $BaTiO_3$ powders were prepared by SHS (Self-propagating High-temperature Synthesis). We would examinate the study of sintering properties and characteristics as a function of temperature with various additives (binder, sintering agent). In separately binder addition, the green and sintered density of specimen were increased as binder content increases. The increased porosity resulted in fine grain size due to the inhibition of grain boundary moving. The $Al_{2}O_{3},\;TiO_{2}$ and MgO playa role of increasing dielectric constants at room temperature. These values were decreased at curie temperature. In case of $SiO_2$, the Curie temperature was decreased. In this study, a high dielectric ceramic capacitor material with temperature stability was synthesized by using various additives.

A Study on the Retained Austenite and Tensile Properties of TRIP Type High Strength Steel Sheet with Cu (Cu 함유 TRIP형 고장력 강판의 잔류오스테나이트 및 인장특성에 관한 연구)

  • Kang, C.Y.;Kim, H.J.;Kim, H.G.;Sung, J.H.;Moon, W.J.
    • Journal of the Korean Society for Heat Treatment
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    • v.12 no.3
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    • pp.231-239
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    • 1999
  • Volume fraction and morphology of retained austenite, tensile properties of TRIP type high strength steel sheet with Fe-C-Si-Mn-Cu chemical composition have been investigated. The retained austenite of granular, bar and film type existing in specimen was obtained after intercritical annealing and austempering. The granular type retained austenite increased with increase of intercritical annealing and austempering temperature. With increase of intercritical annealing temperature, retained austenite and carbon contents increased. Maximum contents of retained austenite was obtained by austempering at $400^{\circ}C$. The maximum tensile strength was obtained by austempering at $450^{\circ}C$ and maximum elongation was obtained at $400^{\circ}C$. T.S${\times}$E.L value increased with increase of retained austenite contents due to the elongation strongly controlled by contents of retained austenite, but tensile strength was affected with various factors such as bainitic structure etc.

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Alveolar ridge preservation of an extraction socket using autogenous tooth bone graft material for implant site development: prospective case series

  • Kim, Young-Kyun;Yun, Pil-Young;Um, In-Woong;Lee, Hyo-Jung;Yi, Yang-Jin;Bae, Ji-Hyun;Lee, Junho
    • The Journal of Advanced Prosthodontics
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    • v.6 no.6
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    • pp.521-527
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    • 2014
  • This case series evaluated the clinical efficacy of autogenous tooth bone graft material (AutoBT) in alveolar ridge preservation of an extraction socket. Thirteen patients who received extraction socket graft using AutoBT followed by delayed implant placements from Nov. 2008 to Aug. 2010 were evaluated. A total of fifteen implants were placed. The primary and secondary stability of the placed implants were an average of 58 ISQ and 77.9 ISQ, respectively. The average amount of crestal bone loss around the implant was 0.05 mm during an average of 22.5 months (from 12 to 34 months) of functional loading. Newly formed tissues were evident from the 3-month specimen. Within the limitations of this case, autogenous tooth bone graft material can be a favorable bone substitute for extraction socket graft due to its good bone remodeling and osteoconductivity.