• The Korean Journal of Ceramics
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• 제7권2호
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• pp.74-79
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• 2001

Alumina composite reinforced by chopped alumina fiber was fabricated by filter-pressing the fiber slurry followed by the infiltration of alumina slurry. The chopped fiber was coated with nickel by electroless plating method. The green samples were densified by hot-pressing. Microstructures were studied by SEM and the mechanical properties such as bending strength and fracture toughness were measured. The resulting mechanical properties were analyzed in relation with processing parameters such as preform density and resulting microstructures. The load-displacement curve of the specimen with Ni interlayer but without Ni inclusion showed brittle fracture mode due to the direct contact between matrix and fiber. The load-displacement curve of the specimen with Ni interlayer and Ni inclusion in the matrix which is introduced by high applied pressure during specimen preparation showed non-brittle fracture mode due to the fiber pull-out and dutile phases in the matrix.

• 한국세라믹학회지
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• 제46권2호
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• pp.131-136
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• 2009

Radio frequency (RF) plasma treatment is studied for the size reduction and the spheroidization of coarse particles to change them into nano-sized powders of spherical shape in MLCC fields. The uni-nanoadditives manufactured by RF plasma processing for high dispersion have been investigated for the effect on core-shell structure in dielectrics of MLCC. Microstructures have been characterized using scanning electron microscope (SEM), transmission electron microscope (TEM) and Electron Probe Micro Analyzer (EPMA). We compared the distribution of core-shell grains between specimens manufactured using uni-nanoadditive and using mixed additive. In addition, the uniformity of rare earth elements in the core-shell structured grains was analyzed. It was shown, from TEM observations, that the sintered specimen manufactured using uni-nanoadditives had more dense small grains with well-developed core-shell structure than the specimen using mixed additives, which had a homogeneous microstructure without abnormal grain growth and shows broad temperature coefficient of capacitance (TCC) curves in all temperature ranges because of well dispersed additives.

• 소성∙가공
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• 제19권1호
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• pp.25-31
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• 2010

To achieve desired microstructure and mechanical property of a manufacturing product, heat treatment process is applied as a secondary process after forging. Especially, quenching process is used for improving strength, hardness, and wear resistance since phase transformation occurs owing to rapid heat transfer from the surface of the specimen. In the present paper, a study on surface temperature measurement for water quenching of eutectoid steel was investigated. In order to determine the temperature history in experiments, three different measuring schemes were used by varying installation techniques of K-type thermocouples. Depending on the measured temperature distribution at the surface of the specimen, convective heat transfer coefficients were numerically determined as a function of temperature by the inverse finite element analysis considering the latent heat generation due to phase transformation. Based on the inversely determined convective heat transfer coefficient, temperature, phase, and hardness distributions in the specimen after water quenching were numerically predicted. By comparing the experimental and computational hardness distribution at three different locations in the specimen, the best temperature measuring scheme was determined. This work clearly demonstrates the effect of temperature measurement on the final mechanical property in terms of hardness distribution.

• 열처리공학회지
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• 제9권4호
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• pp.271-280
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• 1996

This study has been performed to investigate into some effects of power density and traverse speed of laser beam on optical microstructure, hardness and wear characteristics of gray cast iron treated by laser surface hardening technique. Optical micrograph has shown that large martensite and a small amount of retained austenite appear in outermost surface layer with fine martensite in inside hardened zone. Hardness measurements have revealed that the range of maximun hardness value is $Hv=650{\pm}15$ and as the power density increases and the traverse speed decreses, the depth of hardened zone increases due to as increase in input power density. Wear test has exhibited that wear rasistance of laser surface hardened specimen is superier compared to that of untreated specimen under the condition of same load at a given sliding distance, showing that absorption results of an wxidized substance due to a heavy abrasion appear in untreated specimen. The amount of weight loss of laser surface hardened specimen with respect to sliding distance at a given load decreses with increasing traverse speed at a given power density and with increasing power density at a given traverse speed.

• 한국안전학회지
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• 제38권3호
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• pp.20-26
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• 2023

Fiber-reinforced composite materials with carbon, glass, and aramid fibers are widely applied to industrial field structures due to their excellent properties. However, carbon fibers are vulnerable to external impacts, whereas aramid fibers degrade when exposed to water. This study evaluated carbon/aramid fiber composites degraded and damaged by high-temperature saline environments using acoustic emission (AE). The test specimen was molded using an autoclave and immersed in seawater at 70 ℃ for 224 days. In order to imitate the damage, a 3-mm-diameter hole was drilled using a diamond drill. Additionally, the specimen with the perforation was repaired by patch attachment processing. Three-point bending was used to conduct the flexural experiment, and an AE sensor with a 150-kHz resonance frequency was attached to evaluate the damage and the effect of patch attachment. AE accumulative counts obtained at the maximum load were 69.2, 67.1, and 91.2 for a high-temperature seawater deteriorated condition, a hole specimen, and a repaired patch specimen, respectively. Furthermore, the maximum amplitude of AE was detected at low values of 28 dB, 31.3 dB, and 30.3 dB.

• 한국분말재료학회지
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• 제9권6호
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• pp.455-462
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• 2002

The microstructures and properties of TiC dispersed nickel-base alloy were studied in this work. The alloy prepared by powder metallurgical processing was solution treated, 1st-aged at $880^{\circ}C$ for 16 hours, and then 2nd-aged at $760^{\circ}C$ for 4 hours. Microstucture of sintered specimen showed that TiC particles are uniformly dispersed in Ni base alloy. In the specimen aged at $880^{\circ}C$ for 8 hours, the fine $\gammaNi_3$(Al,Ti) precipitates with round shape are observed and the very fine $\gammaNi_3$(Al,Ti) particles with round shape are precipitated in the specimen aged at $760^{\circ}C$ for 4 hours. The presence of ${\gamma}$precipitates in TiC/Ni base alloy increased the hardness and wear resistance of the specimen. The hardness and wear resistance of the Ni-base with TiC are higher than those of conventional Ni-base superalloy X-750 because of dispersion strengthening of TiC particles. The hardness, transverse rupture strength and resistance of the specimen 2nd-aged at $760^{\circ}C$ for 4 hours are higher than those of 1st-aged specimen due to ultrafine $\gammaNi_3$(Al,Ti) precipitates.

• 한국강구조학회 논문집
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• 제12권6호
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• pp.701-713
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• 2000

본 연구에서는 하중비전달형 필렛용접부를 대상으로 순수휨 상태에서 그라인딩 처리 및 TIG 처리에 따른 피로강도 향상정도 및 피로특성을 정량적으로 평가하기 위해서 일련의 4점 휨실험을 실시하였다. 피로실험결과 그라인딩 처리한 경우와 TIG 처리한 경우 $2{\times}106$회 피로강도가 한등급 향상되는 것을 알 수 있었으며, 국내 외의 피로설계기준에서 규정하고 있는 피로강도등급을 대체로 만족하고 있음을 알 수 있었다. 용접지단부의 기하학적 형상에 대한 매개변수해석결과 하중비전달형 필렛용접부에서 응력집중계수에 영향을 미치는 인자는 곡률반경과 비드접선각도임을 알 수 있었다. 한편 파괴역학적 해석 결과 피로균열 발생초기에는 균열보정계수에 가장 큰 영향을 미치는 인자는 기하학적 형상 보정계수임을 알 수 있었으며, 상대깊이가 0.4 이상이 되면 기하학적 형상보정계수 보다는 유한판 보정계수가 보다 큰 영향을 미치는 것을 알 수 있었다. 또한 유한요소해석결과로부터 산정한 응력확대계수범위와 피로균열성장속도의 관계식으로부터 하중비전달형 필렛용접부의 피로수명을 비교적 정확하게 산정할 수 있었다.

• Tribology and Lubricants
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• 제37권3호
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• pp.106-111
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• 2021

There are several studies on reducing the friction that occurs on the relative sliding contact surface of moving parts under extreme environments. In particular, a solid lubricated bearing is studied to solve the tribological problem with friction reduction and durability parts using solid lubricants (lead or silver) in a vacuum atmosphere. Galinstan is mainly used as a liquid metal lubricant, but it is inevitable to have limited tribological applications owing to its high coefficient of friction. Many researchers work on surface texturing for surface modification and precision processing methods. To increase durability and low friction, DLC coating with hydrophobicity is applied on the contact surface texture. Therefore, using an untextured specimen, a dimple specimen, and a DLC-coated dimple specimen under liquid metal lubrication, this paper presents the following experimental sliding friction characteristics in the sliding friction test. 1) The average coefficient of friction of the DLC-coated dimple specimen and dimple specimen are lower compared to that of a non-patterned specimen. 2) In the DLC-coated dimple specimens, the average coefficient of friction changes according to the change in the dimple density. 3) DLC-coated dimple specimens with a density of 12.5 have the lowest average coefficient of friction under 41.6 N of normal load and 143.3 RPM.

• 소성∙가공
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• 제31권4호
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• pp.207-213
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• 2022

In this study, variations in the microstructure and hardness of a low-carbon SCM415 steel with austenitizing temperature and cooling rate are investigated. When the austenitizing temperature is lower than the A₁ temperature (738.8 ℃) of the SCM415 steel, the microstructures of both the air-cooled and water-cooled specimens consist of ferrite and pearlite, which are similar to the microstructure of the initial specimen. When heat treatment is conducted at temperatures ranging from the A₁ temperature to the A₃ temperature (822.4 ℃), the microstructure of the specimen changes depending on the temperature and cooling rate. The specimens air- and water-cooled from 750 ℃ consist of ferrite and pearlite, whereas the specimen water-cooled from 800 ℃ consists of ferrite and martensite. At a temperature higher than the A₃ temperature, the air-cooled specimens consist of ferrite and pearlite, whereas the water-cooled specimens consist of martensite. At 650 ℃ and 700 ℃, which are lower than the A₁ temperature, the hardness decreases irrespective of the cooling rate due to the ferrite coarsening and pearlite spheroidization. At 750 ℃ or higher, the air-cooled specimens have smaller grain sizes than the initial specimen, but they have lower hardness than the initial specimen owing to the increased interlamellar spacing of pearlite. At 800 ℃ or higher, martensitic transformation occurs during water cooling, which results in a significant increase in hardness. The specimens water-cooled from 850 ℃ and 950 ℃ have a complete martensite structure, and the specimen water-cooled from 850 ℃ has a higher hardness than that water-cooled from 950 ℃ because of the smaller size of prior austenite grains.

• 소성∙가공
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• 제31권1호
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• pp.17-22
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• 2022

Hot stamping is widely used to manufacture structural parts to satisfy requirements of eco-friendly vehicles. Recently, hot forming technology using uncoated steel sheet is being studied to reduce cost and solve patent problems. In particular, research is focused on process technology capable of suppressing the generation of an oxide layer. To evaluate the oxide layer in the hot stamping process, Gleeble testing machine can be used to evaluate the oxide layer by controlling the temperature history and the atmosphere condition. At this time, since cooling by gas injection is impossible to protect the oxide layer on the surface of a specimen, research on a method for securing a quenching speed through natural cooling is required. This paper proposes a specimen shape design method to secure a target quenching speed through natural cooling when evaluating the oxide layer of an un-coated boron steel sheet by Gleeble test. For the evaluation of the oxide layer of the un-coated steel sheet through the Gleeble test, dog-bone and rectangular type specimens were used. In consideration of the hot stamping process, the temperature control conditions for the Gleeble test were set and the quenching speed according to the specimen shape design was measured. Finally, the quenching speed sensitivity according to shape parameter was analyzed through regression analysis. A quenching speed prediction equation was then constructed according to the shape of the specimen. The constructed quenching speed prediction equation can be used as a specimen design guideline to secure a target quenching speed when evaluating the oxide layer of an un-coated boron steel sheet by the Gleeble test.