• 제목/요약/키워드: Specimen Changes

검색결과 550건 처리시간 0.029초

볼 엔드밀을 이용한 금형 구면 가공의 표면품질 향상에 관한 연구 (Surface Quality Improvements on the Spherical Shaped Mold using Ball End Milling)

  • 윤일우;황종대
    • 한국기계가공학회지
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    • 제19권3호
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    • pp.71-76
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    • 2020
  • Various machining methods are being studied to improve the processing quality of the spherical R shape in press die. In this paper, we confirmed that changes in machining quality were associated with changes in cutting direction, path, and cutting angle, which are commonly used in the machining of molds. We obtained a surface roughness graph with each condition change in one specimen using an instrument that measured geometry and surface roughness simultaneously. The results of the study showed that the best surface roughness in the finish cut of the spherical surface was obtained using upward pick feed machining.

반복세탁 및 건조방법이 드레스셔츠의 물성에 미치는 영향(II) (The Changes in Properties of Dress Shirts by Repeated Washing and Drying (II))

  • 이송자;성수광;권헌선
    • 한국의류산업학회지
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    • 제1권3호
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    • pp.259-263
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    • 1999
  • This study was carried out to investigate the changes of thermal properties such as warmth retaining and contact warm/cool feeling of commercial dress shirts by repeated washing and drying by sun and dryer. Three kinds of fabrics such as cotton 100%, cotton/polyester 80/20% and polyester 100% were repeatedly washed and dried, and then used as specimen. Thermo Labo II type was employed to measure the thermal properties. At the same time, structural properties such as thickness, weight, bulk density, porosity, moisture vapor permeability and air permeability were analysed.

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Experiment and Prediction of Nonlinear Behavior at High Temperatures of Ferroelectric Ceramics Switched by Electric Field at Room Temperature

  • Ji, Dae Won;Kim, Sang-Joo
    • 한국세라믹학회지
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    • 제54권3호
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    • pp.235-242
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    • 2017
  • Changes in polarization and thermal expansion coefficients during temperature increase of a poled lead zirconate titanate (PZT) cube specimen switched by an electric field at room temperature are measured. The measured data are analyzed to construct governing differential equations for polarization and strain changes. By solving the differential equations, an experimental formula for the high temperature behavior of ferroelectric materials is obtained. It is found that the predictions by the formula are in good agreement with measures. From the viewpoint of macroscopic remnant state variables, it appears that the processes of electric field-induced switching at different temperatures are identical and independent of temperature between $20^{\circ}C$ and $110^{\circ}C$.

전력 케이블용 폴리에틸렌의 열처리 효과(I) (Effects of Heat Treatment on Polyethylene Film for Power Cable Insulation(I))

  • 홍진웅;영치보웅;수곡조길
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1993년도 하계학술대회 논문집 B
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    • pp.1174-1176
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    • 1993
  • Morphology of low density polyethylene(LDPE) such as the degree of crystallinity changes with thermal history etc. In order to clarify the effects of morphological changes on electrical breakdown, we studied direct current and impulse breakdown phenomena of LDPE films heat-treated at 100[$^{\circ}C$] for 1[H] in silicone oil and subsequently cooling to various ways. The degree of crystallinity was estimated by the infra red absorption and X-ray diffraction measurements for the specimens of slowly cooled, cooled in water, original, and cooled in liquid nitrogen gas. As the result, we obtained that the first, second, third, and fourth was slowly cooled of 70.23[%], cooled in water of 61.6[%], original specimen of 56.75[%], and cooled in liquid nitrogen gas of 34.7[%] respectively. The crystalline size and distribution of specimens were researched by Differential scanning calolimeter measurements.

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동종 연골을 이용한 가토 측두하악관절원판 재건시 냉동 보존제의 영향에 관한 실험적 연구 (EFFECTS OF CRYOPRESERVATIVE AGENTS ON THE REPAIR OF THE TEMPOROMANDIBULAR JOINT DISK WITH ALLOGENEIC CARTILAGE GRAFTS IN RABBITS)

  • 김원규;김수남;민승기;성길현;권혁도
    • Maxillofacial Plastic and Reconstructive Surgery
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    • 제15권4호
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    • pp.303-316
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    • 1993
  • The auricular cartilage grafts have been widely used in replacement of the temporomandibular joint disk. Cartilage grafts itself have a low metabolism and high survival rate after grafting. In processing the grafting materials, it was important to preserve the properties of chondrocyte proper. We used 15% glycerol and 10% DMSO (Dimethyl Sulfoxide) solutions for cartilage fixation before deep freezing. We have performed the allogenic auricular cartilage graft in the temporomandibular joint of 20 rabbits which 10 specimen was treated with 15% glycerol and the other 10 specimen was treated with 10% DMSO respectively and examined in 1, 2, 4, 6 and 8 weeks after operation histopathologically. The result were : 1. Inflammatory cell infiltration around the grafted material appeared more glycerol groups than DMSO groups at 1 week, but each group has no differences after 2 weeks. 2. Degenerative changes of grafted auricular chondrocytes were more deveolped in glycerol group than DMSO groups till 4 weeks, but there were no differences between two groups after 6 weeks. 3. Fibrous union between grafted fragment and mandibular condyle was prominent in DMSO group. 4. Vascular proliferation of the grafted auricualr cartilage was more developed in DMSO groups than glycerol group in early stage. 5. Amount of the additional growth of grafted auricular cartilage was more existed in DMSO groups than glycerol group. 6. General survival rate after grafting was more prominent in DMSO group. In summary, allogenic auricular cartilage grafts treated with 15% glycerol and 10% DMSO solution have supported to survivalbility as a cryopreservative agents, especially DMSO groups have little inflammatory cell infiltration in early stages and degenerative changes and additional growth are more prominent than glycerol groups.

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초음파 감쇠를 이용한 순 티타늄 판재의 용접부 특성 (Characteristics of Welds of Pure Titanium Plate Using Ultrasonic Attenuation)

  • 선상원;이원;박희동;황영탁
    • 비파괴검사학회지
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    • 제33권2호
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    • pp.205-211
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    • 2013
  • 초음파 감쇠를 이용하여 티타늄 용접부에 대해 기계적 특성, 파단면 및 초음파특성을 연구하였다. 준비된 티타늄 시험편은 아르곤 가스를 이용하여 제작하였다. 티타늄 용접 시험편이 파단 되었을 때 변화하는 초음파 신호변화를 확인하기 위해서 인장시험을 실시하였다. 주사전자현미경을 이용하여 파단면을 관찰하고, 4 MHz 수직 탐촉자를 이용하여 초음파 시계열 신호를 획득하였다. 티타늄 판재에서 용접부는 모재부와 열영향부에 비하여 기계적 특성이 떨어지며 파단면분석을 통해 용접부의 입자크기가 모재부보다 큼을 확인할 수 있었다. RMS 신호 처리한 초음파 포락선의 면적과 인장강도의 상관관계를 나타내었다. 따라서 초음파를 이용하여 티타늄 용접부의 건전성 평가 방법이 유용함을 알 수 있었다.

열처리에 의한 도재용 Ni-Cr합금 표면의 변화에 관한 연구 (METAL SURFACE CHANGES BY HEAT TREATMENT OF Ni-Cr ALLOYS)

  • 김영한;이선형;양재호;정헌영
    • 대한치과보철학회지
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    • 제27권2호
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    • pp.219-248
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    • 1989
  • The purposes of this study were to analyze the microstructural and compositional changes of metal surfaces following different conditions of preoxidizing heat treatment, to investigate the composition of metal oxides, and to evaluate the effect of preoxidation and removal of surface oxides on microstructure and diffusion profiles. The techniques of EDAX (energy-dispersive analysis of x-ray), ESCA (electron spectroscopy for chemical analysis), and EPMA (electron probe micro analysis) were used, along with SEM (scanning electron microscopy). The obtained results were as follows : 1. A surface of the specimen became rough and the amount of the metal oxides increased with increasing the heat treatment time and temperature and the partial pressure of oxygen. 2. At an air pressure of 28' vacuum, the higher the temperature and the longer the time of preoxidation, the higher Ni concentration was detected. 3. Cr concentration in the specimen heat treated with air was higher than that of with vacuum. 4. The oxides in the specimens were mainly composed of Ni and Cr oxides. On the globular growth particles, significant rises in Al concentration of Rexillium III and Ti concentration of Verabond were noted. 5. Atomic diffusion occurred at the ceramic-metal interface, furthermore the amount of the flux was increased with preoxidation heat treatment.

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Effects of Gas Flow Ratio on the Properties of Tool Steel Treated by a Direct Current Flasma Nitriding Process

  • Jang H. K.;Whang C. N.;Kim S. G.;Yu B. G.
    • 한국표면공학회지
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    • 제38권5호
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    • pp.202-206
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    • 2005
  • Nitriding treatments were conducted on tool steel (SKD 61) at a temperature of $500^{\circ}C$ for 5 hr using high vacuum direct current (DC) plasma, with ammonia and argon as source gases. The structural and compositional changes produced in the nitrided layers by applying different ratios of Ar to $NH_{3}\;(n_{Ar}/n_{NH3}) were investigated using glancing x-ray diffraction (GXRD), optical microscopy, atomic force microscopy (AFM), micro-Vickers hardness testing, and pin-on-disc type tribometer. Nitriding case depths of around of $50{\mu}m$ were produced, varying slightly with different ratios of $n_{Ar}/n_{NH3}. It was found that the specimen surface hardness was 1150 Hv with $n_{Ar}/n_{NH3}=1, increasing to a maximum value of 1500 Hv with $n_{Ar}/n_{NH3}=5. With a further increase in ratio to $n_{Ar}/n_{NH3}=10, the surface hardness of the specimen reduced slightly to a value of 1370 Hv. These phenomena were caused by changes of the crystallographic structure of the nitride layers, i.e the $\gamma'-Fe_{4}N$ phase only was observed in the sample treated with $n_{Ar}/n_{NH3}$=1, and the intensity of the $\gamma'-Fe_{4}N$ phase were reduced but new phase of $\varepsilon'-Fe_{3}N$, which was known as a high hardness, with increasing $n_{Ar}/n_{NH3}. Also, the relative weight loss of counterface of the pin-on-disc with unnitrided steel was 0.2. And that of nitrided steel at a gas mixture ($n_{Ar}/n_{NH3}) of 1, 5, 7, and 10 was 0.4, 0.7, 0.6, and 0.5 mg, respectively. This means that the wear resistance of the nitrided samples could be increased by a factor of 2 at least than that of unnitrided steel.

Change in Kinematics of the Spine after Insertion of an Interspinous Spacer for the Treatment of the Lumbar Spinal Stenosis

  • Lee H. S.;Moon S. J.;Kwon S. Y.;Jung T. G.;Shin K. C.;Lee K. Y.;Lee S. J.
    • 대한의용생체공학회:의공학회지
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    • 제26권3호
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    • pp.151-155
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    • 2005
  • Interspinous spacers have been developed as an alternative surgical treatment for laminectomy or fusion with pedicle screws and rods for the treatment of lumbar spinal stenosis. However, its biomedical efficacies are well not known. In this study, we evaluated kinematic behaviors of the surgical and the adjacent levels before and after inserting interspinous spacers. Three porcine lumbar spines were prepared. On each specimen, an interspinous spacer was inserted at the L4-L5. Flexion-extension moments (0, 2.5, 5.0, 7.5, 10Nm) were applied. A stereophotogrammetric set-up with DLT algorithm was used to assess the three-dimensional motions of the specimen where three markers $({\square}0.8mm)$ were attached to each vertebra. Results showed that extension motion decreased by $15-24\%$ at the surgical level (L4-L5) after insertion of interspinous spacer. At the adjacent levels, the range of motion remained unchanged. In flexion, no significant changes in motion were observed regardless of levels. Therefore, our experimental results demonstrated the interspinous spacer is very effective in limiting the extension motion that may cause narrowing of the spinal canal and vertebral foramen while maintaining kinematic behaviors at the adjacent levels. Further, these results suggested that the use of interspinous spacer may be able to prevent lower back pain at the surgical level and to lower the incidence of degenerative changes at the adjacent levels.

pH 순환 모델에서 과포화 용액의 초기 우식 법랑질에 대한 재광화 효과 (THE REMINERALIZING EFFECTS OF EARLY ENAMEL CAR10US LESION BY SUPERSATURATED BUFFER SOLUTION UNDER PH CYCLING MODEL)

  • 김소라;홍석진;노병덕;이찬영;금기연
    • Restorative Dentistry and Endodontics
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    • 제26권4호
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    • pp.341-349
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    • 2001
  • Dental caries is the most common oral disease. There are many factors contributing to its development, but complete understanding and prevention are not fully known. However, it is possible to remineralize the early enamel curious lesion by fluoride containing remineralization solution. Recently the pH-cycling model has been used to examine the effect of fluoride solution on remineralization of artificial caries in vitro as it can closely simulate the conditions encountered in vivo within a carefully controlled environment. The aim of this study was to evaluate the remineralizing effects of supersaturated buffer solutions under pH-cycling model. The specimen with 3mm-diameter was made using mature bovine incisors which has no caries and has sound enamel surface. Early curious lesions were produced by suspending each specimens into demineralization solution at pH 5.0 for 33 hours and the specimen whose surface hardness value ranged from 25 to 45 VHN were used. The pH cycling treatment regimen consisted of 5 min soaks of three treatment solutions four times per days for 15 days and the continuous cycling of demineralization and remineralization were carried out for 15 days. Following the pH-cycling treatment regimen, the specimens' surface microhardness were measured by the Vickers hardness test (VHN) and analyzed by ANOVA and Duncan's multiple-range test. 1. The surface microhardness value of supersaturated solution, Senstime, and Gagline groups were increased after pH cycling, and that of supersaturated solution was significantly Increased compared to saline group(P<0.05). 2. The surface remineralization effect of fluoride containing solutions was accelerated by saliva under pH-cycling mode 3. The pH cycling model was considered appropriate to mimic the intra-oral pH changes when evaluating demineralization and remineralization in vitro. Under the results of above study, salivary remineralization effect can be improved by fluoride containing remineralization solution. The pH-cycling model was considered appropriate to mimic the intra-oral pH changes when evaluating demineralization and remineralization in vitro.

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