• Applied Microscopy
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• v.48 no.2
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• pp.49-53
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• 2018

A successful transmission electron microscope (TEM) analysis is closely related to the preparation of the TEM specimen and should be followed by the suitable TEM specimen preparation depending on the purpose of analysis and the subject materials. In the case of the Si-based anode material, lithium atoms of formed Li silicide were removed due to ion beam and electron beam during TEM specimen preparation and TEM observation. To overcome the problem, we proposed a new technique to make a TEM specimen without the ion beam damage. In this study, two types of test specimens from the Si-based anode material of Li-ion battery were prepared by respectively adopting the only focused ion beam (FIB) method and the new FIB-ultramicrotome method. TEM analyses of two samples were conducted to compare the Ga ion damage of the test specimen.

• Journal of the Korean Wood Science and Technology
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• v.26 no.4
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• pp.26-33
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• 1998

Acoustical properties of chestnut and paulownia woods have been determined in four film thicknesses of oriental lacquering and cashew varnishing on double surfaces of soundboard to elucidate effects of finishing. Accelerometer was attached to the specimen at one third position from one end, and specimen was hit by the impact hammer at one third position from opposite end. Data were processed by vibration analyzer. The ratio of axial-to-transverse sound velocity of untreated specimens of chestnut and paulownia were 3.25 and 5.34, respectively. Natural frequency, specific Young's modulus, acoustical coefficient, sound velocity, damping of sound radiation(DSR) and acoustical converting efficiency(ACE) decreased by oriental lacquering and cashew varnishing for both species. Damping of internal friction of chestnut decreased by oriental lacquering and cashew varnishing, but that of paulownia increased. Natural frequency. specific Young's modulus, acoustical coefficient, sound velocity, and DSR decreased with increased film thickness of both finishing materials. However, damping of internal friction and ACE showed irregular tendency with increased film thickness. Acoustical properties of cashew varnished chestnut specimen were better than those of oriental lacquered specimen. Acoustical properties of oriental lacquered paulownia specimen were better than those of cashew varnished specimen.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2005.05a
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• pp.245-248
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• 2005

This paper is concerned with manufacturing technology of thin foil tensile specimen using CIP(Cold Isostatic Press) and measurement of precision mechanical property. This thin foil tensile specimen manufacturing technology is a method that can make a metal thin foil specimen for micro tensile testing. We can get a burr free micro metallic thin foil specimen using this technology. For testing mechanical property of this micro thin foil, we use a nano scale material testing machine that was developed by KITECH. In this paper, micro tensile specimens of nickel and copper thin foil are fabricated with CIP and precision mechanical properties of these materials could be measured. We will expect that precision mechanical property of micro/nano material and component. Micro and Nano mechanical property can be measured using this technology and mechanical property data base of micro/nano material and component can be constructed.

• Journal of the Korean Society of Mechanical Technology
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• v.13 no.2
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• pp.115-121
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• 2011

The size of hydrogen molecule is not so small as to invade into the lattice of material, and therefore, hydrogen invades into the material as atom. Hydrogen movement is done by diffusion or dislocation movement in the near crack tip or plastic deformation. Hydrogen appeared to have many effects on the mechanical properties of the Cr-Mo steel alloys. The materials for this study are 1.25Cr-0.5Mo and 2.25Cr-1Mo steels used at high temperature and pressure. The hydrogen amount obtained by theoretical calculation was almost same with the result solved by finite element analysis. The distribution of hydrogen concentration and average concentration was calculated for a flat specimen. Also, finite element analysis was employed to simulate the redistribution of hydrogen due to stress gradient. The calculation of hydrogen concentration diffused into the material by finite element method will provide the basis for the prediction of delayed fracture of notched specimen. The distribution of hydrogen concentration invaded into the smooth and notched specimen was obtained by finite element analysis. The hydrogen amount is much in smooth specimen and tends to concentrate in the vicinity of surface. Hydrogen embrittlement susceptibility of notched specimen after hydrogen charging is more remarkable than that of smooth specimen.

• Journal of the Korean Society of Industry Convergence
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• v.24 no.5
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• pp.517-523
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• 2021

In this study, in the selection of materials for the elements of a small plant, those with high resistance to corrosion are selected and the material properties of coatings for corrosion prevention are evaluated. In addition, corrosion characteristics and material analysis were performed on the welded part, and the hardness characteristics of the welded part, heat-affected part, and the base metal were evaluated. In the case of the post-weld-heat-treated(PWHT) specimen, the corrosion resistance of STS 316 was lower than that of the specimen without the PWHT due to the formation of intergranular carbide. As a result of evaluating the distribution of the hardness of the weld before and after the PWHT, the hardness of the specimen after the PWHT increased by about 20 Hv. As a result of the corrosion test on the welded specimen, the weight loss tended to increase as the time increased. In the case of the PWHT specimen, the corrosion resistance tended to be significantly lower than that of the specimen without PWHT due to the formation of intergranular carbide.

• Journal of the Semiconductor & Display Technology
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• v.20 no.4
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• pp.177-181
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• 2021

Scaffolds protect the sensor in the body. Scaffolds are made of a bioabsorbable polymer. The polymer process is sensitive to humidity. Inside of the 3D printer has been improved to control the humidity. Specimens were produced by injection molding and 3D printer. 3D printed specimens were printed under various humidity conditions. We measured tensile strength of the injection-molded specimen and tensile strength of the 3d printing specimen. We compared tensile strength of the injection-molded specimen and tensile strength of the 3d printing specimen. Tensile strength of the injection-molded specimen is 557 kgf/cm². We confirmed tensile strength of the specimen was highest at 741 kgf/cm² when the humidity was 10 %. We confirmed lower the humidity, higher tensile strength of the polymer product.

• Transactions of Materials Processing
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• v.33 no.2
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• pp.118-122
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• 2024

Micro-electromechanical systems (MEMS) based in-situ heating holders have been developed to enable high resolution imaging of heat treatment analysis. However, unlike the standard 3 mm metal disk specimens used in the furnace-based heating holder and general transmission electron microscopy holder, the MEMS-based in-situ heating holder requires thin specimens that can be penetrated by electrons to be transferred onto the MEMS chip. Previously, focused ion beam milling was used to transfer metal specimens, but it has the disadvantage of being expensive and the risk of specimen damage due to gallium ions. Therefore, in this study, we devised a method of transferring metallic materials by ultrasonic treatment using a transmission electron microscopy specimen made by electro jet polishing. A 3mm electropolished metal disk was placed in an appropriate solution, ultrasonicated, and then drop casted. The transfer of the specimen was successful, but it was confirmed that dislocations were formed inside the specimen due to ultrasonic treatment. This study provides a novel method for transferring metallic materials onto MEMS chips, which is cost-effective and less gallium ion damaging to the specimen. The results of this study can be used to improve the efficiency of heat treatment analysis using MEMS-based in-situ heating holders.

• Journal of the Korea institute for structural maintenance and inspection
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• v.27 no.5
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• pp.9-15
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• 2023

In this study, the lamination performance and strength characteristics of cement-based composite materials according to the laminated specimens manufacturing method were analyzed. As a result of evaluating the buildability according to the layer height, the highest dimensional stability was shown when the layer height was 10 mm in all parts. The mold casting specimen and the printing-Z specimen showed the same compressive strength performance at the age of 28 days. On the other hand, the compressive strength at 28 day of printing-X specimen was the lowest at 71.72 MPa, and 8% lower than that of the mold casting specimen and the printing-Z specimen. The split tensile strength of the laminated specimen may show similar performance to that of the mold casting specimen, but the strength performance may decrease by more than 10% depending on the direction of the layer and the number of layers in the specimen. As a result of the interface analysis of the laminated specimen through X-ray CT analysis, it was confirmed that pores of a certain size were distributed along the interface of the layer.

• Structural Engineering and Mechanics
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• v.73 no.3
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• pp.239-257
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• 2020

In the present study, an innovative steel bracket and haunch hybrid scheme is devised, for retrofitting of earthquake damaged deficient beam-column sub-assemblages. Formulations are presented for evaluating haunch force factor under combined load case of lateral and gravity loads for the design of double haunch retrofit. The strength hierarchies of control and retrofitted beam-column sub-assemblages are established to showcase the efficacy of the retrofit in reversing the undesirable strength hierarchy. Further, the efficacy of the proposed retrofit scheme is demonstrated through experimental investigations carried out on gravity load designed (GLD), non-ductile and ductile detailed beam-column sub-assemblages which were damaged under reverse cyclic loading. The maximum load carried by repaired and retrofitted GLD specimen in positive and negative cycle is 12% and 28% respectively higher than that of the control GLD specimen. Further, the retrofitted GLD specimen sustained load up to drift ratio of 5.88% compared with 2.94% drift sustained by control GLD specimen. Repaired and retrofitted non-ductile specimen, could attain the displacement ductility of three during positive cycle of loading and showed improved ductility well above the expected displacement ductility of three during negative cycle. The hybrid haunch retrofit restored the load carrying capacity of damaged ductile specimen to the original level of control specimen and improved the ductility closer to the expected displacement ductility of five. The total cumulative energy dissipated by repaired and retrofitted GLD, non-ductile and ductile specimens are respectively 6.5 times, 2.31 times, 1.21 times that of the corresponding undamaged control specimens. Further, the damage indices of the repaired and retrofitted specimens are found to be lower than that of the corresponding control specimens. The novel and innovative steel bracket and haunch hybrid retrofit scheme proposed in the present study demonstrated its effectiveness by attaining the required displacement ductility and load carrying capacity and would be an excellent candidate for post-earthquake retrofit of damaged existing RC structures designed according to different design evolutions.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2005.04a
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• pp.146-149
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• 2005

The using of composite material is an aviation field but it changes into a general industry. Especially composites are expanding the use on transportation vehicles like automobiles, ships, and aircrafts. The main factor of this expansion is high specific strength. It can supply a high quality and efficiency of energy. But manufacturing of composite products requires many raw materials and tooling cost for special process, so we needs a reduction of these costs to achieve best efficiency. In the present study, we contrast the change of mechanical and physical properties between VaRTM(Vacuum Assisted Resin Transfer Molding) and hand lay-up process. VaRTM process can offer a high quality the same as autoclave products, and low cost like hand lay-up process. In the results of mechanical tests, VaRTM specimen is stronger than hand lay-up specimen and hand lay-up specimen became delamination. In the results of physical tests, the resin content of VaRTM specimen is lower than hand lay-up specimen. On micrograph, the strength of specimen by VaRTM between fiber and resin is stronger than that of one by hand lay-up. And the specimen by hand lay-up contains more defects than one by VaRTM. So, VaRTM process can practically apply for automobile engine hood. This paper shows that VaRTM process is one of the most suitable processes for composite parts of automobile.