• Structural Engineering and Mechanics
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• v.84 no.6
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• pp.733-741
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• 2022

The amount of natural gas that is used on a worldwide scale is continuously going up. Natural gas and acidic components, such as hydrogen sulfide and carbon dioxide, cause significant corrosion damage to transmission lines and equipment in various quantities. One of the fundamental processes in natural gas processing is the separation of acid gases, among which the safety and environmental needs due to the high toxicity of hydrogen sulfide and also to prevent wear and corrosion of pipelines and gas transmission and distribution equipment, the necessity of sulfide separation Hydrogen is more essential than carbon dioxide and other compounds. Given this problem's significance, this endeavor aims to extend the lifespan of the transmission lines' pipes for gas and oil. Zinc oxide nanoparticles made from the environmentally friendly source of Allium scabriscapum have been employed to accomplish this crucial purpose. This is a simple, safe and cheap synthesis method compared to other methods, especially chemical methods. The formation of zinc oxide nanoparticles was shown by forming an absorption peak at a wavelength of about 355 nm using a spectrophotometric device and an X-ray diffraction pattern. The size and morphology of synthesized nanoparticles were determined by scanning and transmission electron microscope, and the range of size changes of nanoparticles was determined by dynamic light scattering device.

• The Journal of the Acoustical Society of Korea
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• v.27 no.8
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• pp.418-426
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• 2008

In this paper, we propose an algorithm for the frequency channel segmentation using peaks and valleys in spectrogram. The frequency channel segments means that local groups of channels in frequency domain that could be arisen from the same sound source. The proposed algorithm is based on the smoothed spectrum of the input sound. Peaks and valleys in the smoothed spectrum are used to determine centers and boundaries of segments, respectively. To evaluate a suitableness of the proposed segmentation algorithm before that the grouping stage is applied, we compare the synthesized results using ideal mask with that of proposed algorithm. Simulations are performed with mixed speech signals with narrow band noises, wide band noises and other speech signals.

• Applied Chemistry for Engineering
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• v.31 no.1
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• pp.103-107
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• 2020

The purpose of this study is to resource calcium ions contained in most industrial by-products, and confirm the characteristics of calcium ions by extraction and separation conditions. Calcium oxide was used as a calcium extraction source, and hydrochloric acid as an extraction solvent, and the extraction amount according to the concentration of the extraction solvent and the pH dependent characteristics of the extract were analyzed. As the extractant concentration increased, the extracted amount increased while the pH for the extraction was kept constant. In order to separate extracted calcium ions, an acid-basic solution was injected and the formation of precipitates and also the form of precipitates were analyzed. When the sulfuric acid and sodium hydroxide solution of acid and basic substances were injected into the calcium extract, precipitates were formed and separated into CaSO₄ and Ca(OH)₂ forms.

• Journal of Satellite, Information and Communications
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• v.10 no.4
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• pp.58-63
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• 2015

Due to GPS signal's vulnerability of jamming attack, various enhancement techniques are needed. Among variety of techniques, we focused on GPS receiver's anti-jamming techniques. There are many anti-jamming methods at GPS receivers which include filtering methods in time domain, frequency domain and space domain. However, these methods are ineffective to signals, which include both jamming and noise. To solve the problem, this paper proposes a jamming separation scheme by using a BSS method in a jamming environment. As separated GPS signals include noise after the jamming separation method, it is difficult to receive accurate GPS signals. For this reason, this paper also proposes a wavelet de-noising method to effectively eliminate noise. Experimental results of this paper are based on a real field test data of an integrated GPS/QZSS/Wi-Fi positioning system. At the end, the simulation result demonstrates its superiority by showing improved positioning accuracy.

• The Journal of the Acoustical Society of Korea
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• v.35 no.4
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• pp.303-309
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• 2016

This paper proposes a novel approach to the problem of audio signal clustering using a stacked autoencoder. The proposed stacked autoencoder learns an efficient representation for the input signal, enables clustering constituent signals with similar characteristics, and therefore the original sources can be separated based on the clustering results. STFT (Short-Time Fourier Transform) is performed to extract time-frequency spectrum, and rectangular windows at all the possible locations are used as input values to the autoencoder. The outputs at the middle, encoding layer, are used to cluster the rectangular windows and the original sources are separated by the Wiener filters derived from the clustering results. Source separation experiments were carried out in comparison to the conventional NMF (Non-negative Matrix Factorization), and the estimated sources by the proposed method well represent the characteristics of the orignal sources as shown in the time-frequency representation.

• Journal of Ginseng Research
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• v.40 no.3
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• pp.220-228
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• 2016

Background: Among the various ginseng strains, Shizhu ginseng is endemic to China, mainly distributed in Kuandian Manchu Autonomous County (Liaoning Province, China); however, not much is known about the compounds (especially saponins) in Shizhu ginseng. Methods: A rapid, sensitive, and reliable ultra-high performance liquid chromatography coupled with MS/MS (UHPLC-MS/MS) method was developed to separate and identify saponins in Shizhu ginseng. Results: The separation was carried out on a Waters ACQUITY UPLC BEH $C_{18}$ column ($100mm{\times}2.1mm$, $1.7{\mu}m$) with acetonitrile and 0.1% formic acid aqueous solution as the mobile phase under a gradient elution at $40^{\circ}C$. The detection was performed on a Micromass Quattro Micro API mass spectrometer equipped with electrospray ionization source in both positive and negative modes. Under the optimized conditions, a total of 31 saponins were identified or tentatively characterized by comparing retention time and MS data with related literatures and reference substances. Conclusion: The developed UHPLC-MS/MS method was suitable for identifying and characterizing the chemical constituents in Shizhu ginseng, which provided a helpful chemical basis for further research on Shizhu ginseng.

• Membrane and Water Treatment
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• v.7 no.3
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• pp.223-240
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• 2016

In this study, poly(vinyl-alcohol) and water insoluble ${\beta}$-cyclodextrin polymer (${\beta}$-CDP) cross-linked with citric acid, have been used as macrocyclic carrier in the preparation of polymer inclusion membranes (PIMs) for aniline (as molecule model) extraction from aqueous media. The obtained membranes were firstly characterized by X-ray diffraction, Fourier transform infrared and water swelling test. The transport of aniline was studied in a two-compartment transport cell under various experimental conditions, such as carrier content in the membranes, stirring rate and initial aniline concentration. The kinetic study was performed and the kinetic parameters were calculated as rate constant (k), permeability coefficient (P) and flux (J). These first results demonstrated the utility of such polymeric membranes for environmental decontamination of toxic organic molecules like aniline. Predictive modeling of transport flux through these materials was then studied using design of experiments; the design chosen was a two level full factorial design $2^k$. An empirical correlation between aniline transport flux and independent variables (Poly ${\beta}$-CD membrane content, agitation speed and initial aniline concentration) was successfully obtained. Statistical analysis showed that initial aniline concentration of the solution was the most important parameter in the study domain. The model revealed the existence of a strong interaction between the Poly ${\beta}$-CD membrane content and the stirring speed of the source solution. The good agreement between the model and the experimental transport data confirms the model's validity.

• Journal of Environmental Analysis, Health and Toxicology
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• v.21 no.4
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• pp.237-242
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• 2018

Strontium (Sr) commonly exists in rock, groundwater, soil, plants, and animals. The Sr isotope ratio offers important information as a tracer on nature because the Sr isotopic composition is not fractionated by any biological process in these ecosystems. Hence, Sr isotope ratio has been used in several studies on tracing the Sr source for contaminated sites and human migration. In this study, we developed a separation method for Sr content, and then improved Sr isotope analysis using multi-collector inductively coupled plasma mass spectrometry (MC-ICP-MS). A powdered rock standard (NIST 2710a) was used to determine the removal of interference elements (Rb and Ca) and the recovery rate of Sr content. The results ranged from 98% to 106%. Additionally, three standard samples (NBS 987, IAPSO and NIST 1486) were analyzed to evaluate the precision and accuracy of the results. The measured $^{87}Sr/^{86}Sr$ ratio for all the samples were consistent with the reported values, within an error. These results indicate that our established Sr separation and Sr isotope measurement methods are reliable and can hence be useful in the fields of environmental and forensic sciences.

• The Journal of the Acoustical Society of Korea
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• v.39 no.5
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• pp.461-467
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• 2020

In noisy and multi-speaker environments, the performance of speech recognition is unavoidably lower than in a clean environment. To improve speech recognition, in this paper, the signal of the speaker of interest is extracted from the mixed speech signals with multiple speakers. The VoiceFilter model is used to effectively separate overlapped speech signals. In this work, clustering by Probabilistic Linear Discriminant Analysis (PLDA) similarity score was employed to detect the speech signal of the interested speaker, which is used as the reference speaker to VoiceFilter-based separation. Therefore, by utilizing the speaker feature extracted from the detected speech by the proposed clustering method, this paper propose a speaker diarization system using only the mixed speech without an explicit reference speaker signal. We use phone-dataset consisting of two speakers to evaluate the performance of the speaker diarization system. Source to Distortion Ratio (SDR) of the operator (Rx) speech and customer speech (Tx) are 5.22 dB and -5.22 dB respectively before separation, and the results of the proposed separation system show 11.26 dB and 8.53 dB respectively.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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• v.3 no.4
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• pp.309-317
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• 2005

A study on the separation of $^{99}Tc,\;^{94}Nb,\;^{55}Fe,\;^{90}Sr\;and\;^{59/63}Ni$ in various radioactive wastes discharged from nuclear power plants has been performed for a use in their quantification which is indispensible for the evaluation of the radionuclide inventory Ni was recovered along with Ca, Mg, Al, Cr, Ti, Mn, Ce, Na, K, and Cu through the sequential separation procedure of Re(as a surrogate of $^{99}Tc$), Nb, Fe and Sr by anion exchange and Sr-Spec extraction chromatography. In this research, chemical separation of Ni from the co-existing elements was investigated by cation exchange and Ni-Spec extraction chromatography. Precipitation behaviour of Ni and the co-existing elements with dimethylglyoxime(DMG) was investigated in ammonium $citrate/ethanol-H_2O$ and tartaric $acid/acetone-H_2O$ in order to purify separated Ni fractions and to prepare $^{59/63}Ni$ source for the radioactivity measurement using a gas proportional counter. Recovery of Ni separated through ion exchange chromatographic separation procedure was $92.1\%$ with relative standard deviation of $0.9\%$. In addition, recovery of Ni with DMG in the tartaric $acid/acetone-H_2O$ was $85.6\%$ with relative standard deviation of $1.9\%$.