• Title/Summary/Keyword: Sono-gel

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The Synthesis of Silica Aerogel in the Macroporous Ceramic Structure by Sono-gel Process and Supercritical Drying Process (초음파 겔화 공정과 초임계 건조 공정을 이용한 다공성 세라믹스 구조체 내부에 실리카 에어로겔 합성)

  • Hong, Sun-Wook;Song, In-Hyuck;Park, Young-Jo;Yun, Hui-Suk;Hwang, Ki-Young;Rhee, Young-Woo
    • Journal of the Korean Ceramic Society
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    • v.47 no.6
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    • pp.553-559
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    • 2010
  • The synthesis behavior of nanoporous silica aerogel in the macroporous ceramic structure was observed using TEOS as a source material and glycerol as a DCCA(dry control chemical additive). Silica aerogel in the macroporous ceramic structure were synthesized through a sono-gel process. The wet gel in the macroporous ceramic structure were aged in ethanol for 72 h at $50^{\circ}C$. The aged wet gel was dried under supercritical drying condition. The addition of glycerol has a role of giving the uniform pore size distribution. The reproducibility of aerogel in the macroporous ceramic was improved in the glycerol(0.05 mol%) added to the silica sol and TEOS : $H_2O$=1 : 12.

Analgesic and Anti-inflammatory Effects of Sono-acupoint Therapy (초음파경혈요법의 진통소염효과 연구)

  • Lim, Sabina;Son, Yang-sun;Jin, Soo-hee
    • Journal of Acupuncture Research
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    • v.19 no.5
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    • pp.176-188
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    • 2002
  • Objective : Sono-acupoint (SA) therapy is a new therapeutic technique that combined with acupuncture points, herbal medicine and ultrasound therapy. This study was carried out to investigate the analgesic and anti-inflammatory effects of sono-acupoint therapy. Methods : We performed the tail-flick test with normal rats to examine the tail-flick latency (TFL), and the Freund's adjuvant-induced arthritis rat model to examine the edema, skin temperature and serum concentration of c-reactive protein and rheumatoid factor (RF). Herbal SA (HSA) treatment was performed at bilateral Zusanli (ST36) with the hanbang-gel made of several selected herbal drugs in Sprague-Dawley rats (male, $250{\pm}30g$). General SA (GSA) treatment was performed at bilateral Zusanli (ST36) with the gel used in ultrasound therapy. In arthritis rat model, Freund's adjuvant (50mg/ml) was injected in dorsal part of right foot, and these treatments were performed after 15 days. Results : TFL was lengthened after SA treatments. Skin temperature and RF concentration that were the evidence of arthritis in rats were decreased by HSA treatment (P < 0.05). Conclusion : These results indicate that HSA has the analgesic and anti-inflammatory effects in rats, and further developments will produce the advance of this new therapeutic skill.

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The Synthesis of Hydrophobic Silica Aerogel in the Macroporous Ceramic Structure by Ambient Drying Process (상압 건조 공정을 이용한 다공성 세라믹스 구조체 내부에 소수성 실리카 에어로겔의 합성)

  • Hong, Sun-Wook;Song, In-Hyuck;Park, Young-Jo;Yun, Hui-Suk;Hahn, Yoo-Dong;Hwang, Ki-Young;Rhee, Young-Woo
    • Journal of Powder Materials
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    • v.18 no.3
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    • pp.269-276
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    • 2011
  • The synthesis behavior of nanoporous silica aerogel in the macroporous ceramic structure was observed using TEOS as a source material and glycerol as a dry control chemical additive (DCCA). Silica aerogel in the macroporous ceramic structure was synthesized via sono-gel process using hexamethyldiazane (HMDS) as a modification agent and n-hexane as a main solvent. The wet gel with a modified surface was dried at $105^{\circ}C$ under ambient pressure. The addition of glycerol appears to give the wet gel a more homogeneous microstructure. However, glycerol also retarded the rate of surface modification and solvent exchange. Silica aerogel completely filled the macroporous ceramic structure without defect in the condition of surface modification (20% HMDS/nhexane at 36hr).