• Title/Summary/Keyword: Sonic

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The Influence of Temperature, Ultrasonication and Chiral Mobile Phase Additives on Chiral Separation: Predominant Influence of β-Cyclodextrin Chiral Mobile Phase Additive Under Ultrasonic Irradiation

  • Lee, Jae Hwan;Ryoo, Jae Jeong
    • Bulletin of the Korean Chemical Society
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    • v.33 no.12
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    • pp.4141-4144
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    • 2012
  • This paper introduces a technique for resolving amino acids that combines the advantages of the conventional CSP (chiral stationary phase) method with the CMPA (chiral mobile phase additive) method. A commercially available chiral crown ether column, CROWNPAK CR(+), was used as the CSP and three cyclodextrins (${\beta}$-CD, ${\gamma}$-CD, HP-${\beta}$-CD) were used as the mobile phase additives. Chromatographic resolution was performed at $25^{\circ}C$ and $50^{\circ}C$ with or without sonication. A comparison of the chromatographic results under ultrasonic conditions with those under non-ultrasonic conditions showed that ultrasound decreased the elution time and enantioselectivity at all temperatures. In the case of the ${\beta}$-CD mobile phase additive, the elution time and enantioselectivity under ultrasonic condition were significantly higher than under non-sonic condition at all temperatures. Commercially available Chiralpak AD, Whelk-O2 and Pirkle 1-J columns were used as CSPs to examine more meticulously the effects of ultrasonication and temperature on the optical resolution. The optical resolution of some chiral samples analyzed at $25^{\circ}C$ and $50^{\circ}C$ with or without sonication was compared. As in the previous case, the enantioselectivity was lower at $25^{\circ}C$ but similar enantioselectivity was observed at $50^{\circ}C$.

Buzz Characteristic of Supersonic Propulsion System with Spray Injection and Combustion (액적 분사/연소를 고려한 초음속 엔진의 buzz 특성)

  • Kim, Seong-Jin;Yeom, Hyo-Won;Sung, Hong-Gye;Gil, Hyun-Yong;Yoon, Hyun-Gull
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2010.05a
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    • pp.411-414
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    • 2010
  • In supersonic propulsion system, the inlet buzz phenomenon in the subcritical operation arises large pressure oscillation, combustion instability, and thrust loss, etc. Inlet Buzz phenomenon and the spray injection/combustion are figured out by the unified unsteady numerical analysis. TAB(Taylor Analogy Breakup) model was applied. Acoustic mode of the entire engine was investigated by detail analysis of pressure fluctuation at each location of the engine.

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Deep RIE를 이용하여 제작된 마이크로 노즐 내에서 유체의 거동에 대한 컴퓨터 시뮬레이션 분석

  • Jeong, Gyu-Bong;Song, U-Jin;Cheon, Du-Man;Yeo, Jun-Cheol;An, Seong-Hun;Lee, Seon-Yeong
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.37.2-37.2
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    • 2009
  • 다이렉트 프린팅 방식에 대한 수요가 높아지면서 마이크로 노즐에 대한 수요도 높아지고 있다. 마이크로 노즐은 Nano particle deposition system (NPDS)에서 가장 중요한 부분으로 금속이나 세라믹 분말을 음속으로 가속시키는 역할을 한다. 또한 마이크로 노즐은 마이크로 스페이스 셔틀과 주사바늘이 없는 약물 주사 시스템 등의 많은 분야에서 사용 가능하다. 이러한 마이크로 노즐은 대부분 기계적 절삭법을 이용하여 알루미늄으로 만들어져왔다. 하지만 알루미늄으로 만들어진 마이크로 노즐은 경도가 낮아 세라믹 나노 입자를 적층하는 것에 적절치 못하며 사용가능한 수명이 짧다는 단점을 가지고 있다. 또한 가장 큰 단점으로 노즐목을 1mm이하로 제작하는 것이 어렵다는 것이다. 따라서 본 연구에서는 Si wafer를 Deep RIE 방식을 이용하여 3차원적으로 제작하였다. Deep RIE 방식 중 BOSCH process를 이용하였다. 이렇게 만들어진 마이크로 노즐은 다이렉트 프린팅 방식중 하나인 NPDS에 적용하였다. Si wafer로 만들어진 마이크로 노즐이 적용된 NPDS를 이용하여 graphite 분말을 가속하여 적층 실험을 실시하였다 이와 함께 전산 유체 역학(CFD)를 이용하여 마이크로 노즐일 이용한 초음속 가속 가능 여부를 판단하였다. 전산 유체 역학은 유한 요소법을 이용하여 유체의 거동을 시뮬레이션을 통하여 예측하는 것으로 마이크로 노즐 내에서 유체의 흐름을 예상할 수 있다. 실제 실험의 결과와 전산 유체 역학을 이용한 시뮬레이션 결과dml 비교 분석을 실시하였다.

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A Rear Alarm System using Ultra-sonic Wave Sensor (초음파센서를 이용한 후방경보시스템)

  • Lee, Yeong-Roh;Lee, Jeung-Hyun;Park, Jeung-Soo;Kim, Tae-Hyun;Cho, Wan-Hee;Lee, Dong-Hyun;Soh, Dea-Wha
    • Journal of the Speleological Society of Korea
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    • no.79
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    • pp.47-51
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    • 2007
  • As time goes by, ultrasonic wave is getting important and new technology, which is adapted to ultrasonic wave is used to industry such as home appliance, automobile, and high-tech industry. Especially, ultrasonic wave is used an alarm device whether there are things at the rear of I. It's do important device in automobile system because it can prevent car-accident from inattention of the driver. Actually, there has already been lots of the alarm device. But it's expensive and so difficult to set the device. So almost driver don't set device at their automobile. We focus on these problems. We want to make cheap md easy setting device. Ultrasonic wave sensor emits Ultrasonic-signal at outgoing part and receive part accept the signal. Sensor analyzes the signal and Distance is displayed on LCD of device. The device makes alarm if distance is near from something of rear. The device makes break-system operate to prevent drivers from crashing if distance is so near. This device is portable. So normal deriver can set it easily.

The Development of HeadZmouse for Computer Access Using Gyroscopic Technology and Macro-Interface for Computer Access (컴퓨터접근을 위한 매크로 인터페이스 및 자이로센서기술을 사용한 헤드마우스의 개발)

  • Rhee, K.M.;Woo, J.S.
    • Journal of rehabilitation welfare engineering & assistive technology
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    • v.1 no.1
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    • pp.1-6
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    • 2007
  • Applying the gyroscopic technology, HeadZmouse has been developed to simulate left and right mouse click, double click, drag and drop, and even a wheel function for navigating web. This device was designed to work on both PC and Macintosh environments using a USB cable. The first time you use this device, you'll find out how much freedom it offers to someone who can't use his or her hands freely. Rather than being tied to your computer, simple manipulation such as blowing an air (breathing) into a sonic sensor can simulate all the functions which standard mouse has, even including a wheel function. Also, a macro-interface device has been developed. By storing repetitive tasks into a memory, you can carry out repetitive tasks just by clicking a button once.

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Imparting Disperse and Cationic Dyeability to Polypropylene through Melt Blending

  • Teli M. D.;Adivarekar R. V.;Ramani V.Y.;Sabale A.G.
    • Fibers and Polymers
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    • v.5 no.4
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    • pp.264-269
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    • 2004
  • The present paper deals with improvement in disperse dyeablility as well as imparting of cationic dyeablility to difficultly dyeable polypropylene by a melt blending technique. Isotactic polypropylene (PP) was blended with fibre grade polybutylene terephthalate (PBT), cationic dyeable polyethylene terephthalate (CDPET) and polystyrene (PS), individually. The resulting binary blends were spun and drawn into fibres at draw ratio 2, 2.5, and 3. The compatibility of blends, structural changes of fibres in terms of X-ray crystallinity, relative crystallinity, sonic modulus, birefringence and thermal stability were examined. The blended fibres were found to be disperse dyeable by the conventional method of high temperature and high pressure dyeing. And this dye ability increased with increase in the level of substitution. PP/CDPET blend also exhibited dyeablility with cationic dyes in addition to that with disperse dyes. The optimum level of blending was predicted keeping in view of tenacity and thermal stability of melt blend fibres. The wash fastness properties of the dyed fibres were found to be of high rate.

Fabrication Process and Characterization of Sonic Polymer-Metal Composite Actuators by Electroless Plating of Platinum (백금의 무 전해 도금에 의한 이온성 고분자-금속 복합물 액추에이터의 제작 공정 및 특성 측정)

  • Cha, Seung-Eun;Park, Jeong-Ho;Lee, Seung-Gi
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.51 no.9
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    • pp.455-463
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    • 2002
  • Ionic Polymer metal composite(IPMC), one of new actuation materials of EAPs is fabricated by electroless plating of platinum on both sides of the perfluorosulfonic acid film or Nafion film and its electromechanical characteristics are investigated. The IPMC strip bends towards anode under electrical field. As the number of plating cycle increases, the distance between plated platinum electrodes on both sides of Nafion membrane decreases and also the displacement is almost inversely proportional to the number of plating. The displacement of IPMC strip depends on voltage magnitude and applied signal frequency and its maximum deformation is observed at a critical frequency, resonant frequency. Low pressure sandblasting is used for surface treatment of Nafion membrane and at 8 times of plating cycle produced actuator with high displacement performance. For more efficiency of fabricated IPMC, it is useful to add one or two surface developing step which is the second reduction process using hydrazine.

Consequence Analysis of Energy Facility(City Gas Pipeline) (에너지시설(도시가스배관)의 사고시 영향 평가)

  • Park Kyo-Shik;Lee Jin-Han;Jo Young-Do;Park Jin-Hee
    • Journal of the Korean Institute of Gas
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    • v.7 no.1 s.18
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    • pp.10-18
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    • 2003
  • Consequence model has been suggested to evaluate consequence of city gas accident considering actual situation. Through event tree analysis(ETA), probable accidents were summarized and listed. Then release rate was calculated both sonic and subsonic conditions. Among city gas accidents, fire damage is the dominant one and mainly discussed; fatality, burning injury, and damage to building were estimated using the consequence model suggested. With an appropriate conditions, calculating total cost by accident was suggested.

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Optimization of Electro Polishing Processing Conditions for Deburring of Micro Fuel Cell bipolar plate (마이크로 연료 전지 분리판 디버링을 위한 Electro Polishing 가공 조건 최적화)

  • Chung, Jea-Hwa;Kim, Byung-Chan;Kim, Woon-Young;Cho, Myeong-Woo
    • Design & Manufacturing
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    • v.11 no.3
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    • pp.51-55
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    • 2017
  • Micro fuel cells have high reliability and long usage time. Among them, PEMFC (polymer Electrolyte Membrane Fuel Cell) is suitable as a portable power source because it is easy to fix electrolyte and simple structure. The bipolar plate, a key component of the fuel cell, is produced by cutting. In the case of micro fuel cell separator, burr is very small and the flow channel size in the separator is very small. Therefore, it is difficult to remove burrs in the usual way such as a brushing or ultra-sonic method. Therefore, this study proposed electrolytic polishing process and analyzed the characteristics of each condition by introducing the concept of roughness reduction rate. In addition, the ultrasonic process was added to analyze the effect of ultrasonic addition.

The Effect of Ultrasonic Vibration on Heat Transfer Augmentation of Forced Convective Flow in Circular Pipes (초음파 진동이 관내 강제대류 유동의 열전달 증진에 미치는 영향)

  • Jeong Ji Hwan
    • Journal of Energy Engineering
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    • v.13 no.4
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    • pp.275-280
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    • 2004
  • Augmentation of heat transfer by ultrasonic vibration in pipes are investigated. Measurements of convective heat transfer coefficients on circular pipe walls are made with and without ultrasonic vibration applied to water. These data are compared with each other to quantify the effects of ultrasonic vibration on heat transfer enhancement. Numerical analysis has been also performed in order to extend the ranges of examined temperature and flow rate. FLUENT Ver.6.1 is used to simulate velocity and temperature fields and evaluate heat transfer coefficient with and without ultrasonic vibration. The results show that the ultra- sonic vibration enhances the Nusselt number of forced convection flow and the increase rate strongly depends on flow rate.