• Title/Summary/Keyword: Solution film thickness

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Internal Flow Stability for Tangential Entry Conditions in a Swirl Injector (스월 인젝터에서 접선방향 유입구 조건이 내부유동의 안정성에 미치는 영향에 대한 연구)

  • Kim, Sung-Hyuk;Khil, Tae-Ock;Cho, Seong-Ho;Yoon, Young-Bin
    • Journal of the Korean Society of Propulsion Engineers
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    • v.12 no.6
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    • pp.30-37
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    • 2008
  • Many theoretical and experimental studies have been conducted to investigate elements of swirl injector hydrodynamics, such as variations in liquid film thickness or air core diameter. From these studies, some theoretical relationships have been established through an approximate analytical solution of flow hydrodynamics in a swirl nozzle. However, experimental studies on elements such as the stability of internal flow have not produced conclusive results. In this study, the stability of the internal flow under tangential entry conditions was examined by visualizing the formation of the air core in the swirl chamber and measuring the liquid film thickness in the orifice.

Dielectric $Al_2O_3-SiO_2$ Films from Metal Alkoxides

  • Soh, Deawha;Natalya, Korobova E.
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2003.10a
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    • pp.957-962
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    • 2003
  • The preparation of $Al_2$O$_3$-SiO$_2$ thin films from less than one micron to several tens of microns in thickness had been prepared from metal alkoxide sols. Two methods, dip-withdrawal and electrophoretic deposition, were employed for thin films and sheets formation. The requirements to be satisfied by the solution for preparing uniform and strong films and by the factors affecting thickness and other properties of the films were examined. for the preparation of thin, continuous $Al_2$O$_3$-SiO$_2$ films, therefore, metal-organic-derived precursor solutions contained Si and Al in a chemically polymerized form has been developed and produced in a clear liquid state. In the process of applying to substrates, this liquid left a transparent, continuous film that could be converted to crystalline $Al_2$O$_3$-SiO$_2$ upon heating to 100$0^{\circ}C$. And, a significant change of the film density took place in the crystallization process, thus leading to the strict requirements as to the film thickness, which could survive crystallization.

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The Effect of Coloring Condition on the Surface Characteristic of 304 Stainless Steel (304 스테인리스강의 착색 처리 조건이 표면 특성에 미치는 영향)

  • Kim, Ki-Ho
    • Journal of the Korean institute of surface engineering
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    • v.44 no.5
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    • pp.220-225
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    • 2011
  • 304 stainless steel plate was colored by hot dip and electrochemical treatment in a solution containing sulphuric and chromic acids. In the process, treatment variables such as operating time and methode were changed. The surface characteristics that changed by the treatment of the samples such as surface composition, oxide film thickness, color, surface roughness and reflectivity were studied. Surface composition was varied as follows. Fe was decreased, but Cr and O were increased. Ni was increased until 20 min, but reveals decreasing tendency as time passed after that. These means the surface film becomes chrome rich oxide phase as the treatment times increase. The thickness of film was about 220 nm at 30 min by dip treatment and it reduced as the treatment times increased. On the other hand, the thickness was about 150 nm at 10 min by electrochemical method and it doesn't increased with time. Surface color changed from metallic white of the base plate to gray, black, red, and green-blue, gradually, as the treating time increased. The reflectivity of colored surface measured by UVVIS-NIR spectrophotometer was reduced from max 38% of basis metal to min 3.5%.

Sensitivity and Error Propagation Factors for Three-Parameter Ellipsometry

  • Ihm, Hye-Ran;Chung, Gyu-Sung;Paik, Woon-Kie;Lee, Duck-Hwan
    • Bulletin of the Korean Chemical Society
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    • v.15 no.11
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    • pp.976-980
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    • 1994
  • The sensitivity factors and the error propagation factors are defined for the three-parameter ellipsometry (TPE). The sensitivity factor is useful for understanding the nature of the TPE measurements in connection with determination of the optical properties and the thickness of a film. On the other hand, the error propagation factors provide a quantitative tool for predicting the optimum condition for TPE experiments. Their usefulness is demonstrated for the passive film formed on nickel in aqueous solution.

Electrical Capacitance of Polypyrrole-Perchlorate and Polypyrrole-Naflon Film Electrodes

  • 엄재웅;백운기
    • Bulletin of the Korean Chemical Society
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    • v.17 no.4
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    • pp.349-352
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    • 1996
  • Electrical capacitance at the interface between electrolyte solution and conducting polypyrrole film electrode was measured by a simple electrochemical method. The polymer films were electropolymerized in the presence of perchlorate (PPy-ClO4) or Nafion (PPy-Nafion) anions as the dopant ions. Both polymers exhibited large double layer capacitances which were slightly potential dependent within the potential range where the polymers are conductive. The capacitance increased in proportion to the polymer thickness. The specific capacitance were about 10 Fg-1and 44 F g-1 for PPy-Nafion and PPy-ClO4, respectively.

Sensing and Degradation Properties in the QCM Gas Sensor Coated with the PVC and GC Blended Liquid (PVC 및 GC물질의 혼합액을 코팅한 QCM가스센서의 센싱 및 열화특성)

  • 장경욱;김명호;이준웅
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.07a
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    • pp.483-486
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    • 2000
  • In the recognition of the gases using the quartz crystal rnicrobalance (QCM) coated with the film materials, it is important to obtain the recognition ability of gases, and the stability of film coated above the QCM. Especially, the thickness of film coated above the QCM is decreased according with the using circumstance and time of QCM gas sensor. Therefore, the sensing chararcteristics of film is changed with these. In this paper, we coated the lipid GC materials varing with the blended amount of PVC(Po1y Vinyl Chloride) and solution (Tetra Hydrofan:THF) above QCM to obtain the stability of lipid PC film. QCM gas sensors coated with film materials were measured the frequency change in the chamber of stationary gas sensing system injected 1-hexane, ethyl acetate, ethanol and benzene of 20.4 respectively. Also, we measured the degradation characteristics of QCM gas sensor to show the properties of stability.

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Study on Properties of Antimony-doped Tin Oxide Thin Films Prepared by Sputtering (Sputtering 방법에 의해 제조된 Sb가 도핑된 주석산화물 박막의 특성에 관한 연구)

  • 김층완;김광호;이환수;이혜용
    • Journal of the Korean Ceramic Society
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    • v.33 no.7
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    • pp.735-742
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    • 1996
  • Antimony-doped Tin oxide (ATO) thin films were deposited on soda-lime glass substrates by DC magnetron sputtering technique. Effects of DC power film thickness and post heat-treatment on electrical conductivity of ATO film were investigated. Other properties of ATO film such as optical anti-chemical and wear properties were also reported in this work. The obtained ATO films showed electrical resistivities ranging from 5$\times$10-3 $\Omega$cm to 3$\times$10-3 $\Omega$cm with the average optical transparency above 80% in visible wavelength range and excel-lent anti-chemical properties where the electrical resistivity was not changed even after soaking the films in 1M HCl or 1M NaOH solution for 10 days. These properties were found to be related to the crystallinity of ATO film and the films having higher crystallinity showed better properties.

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The Structural properties of PZT thick film with preparation condition states (제작조건에 따른 PZT후막의 구조적 특성)

  • Kang, Jung-Min;Cho, Hyun-Moo;Lee, Sung-Gap;Lee, Sang-Heon;Lee, Young-Hie;Bae, Seon-Gi
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2004.07a
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    • pp.142-145
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    • 2004
  • [ $Pb(Zr_{0.8}Ti_{0.2})TiO_3$ ] powder were prepared by the sol-gel method using a solution of Pb-acetate, Zr n-propoxide and Ti iso-propoxide. PZT thick film were fabricated by the screen printing method. and then the structural properties as a function of the sintering temperature were studied. PZT film thickness, obtained by four screen printing, was approximately $70{\sim}90{\mu}m$. The PZT thick film, sintered at $1050^{\circ}C$, showed deuse and uniform grain stractures and percent porosity of the thick film was 25.43%.

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A Study on the Breakdown Characteristics of Electrodeposited Polyimide Film at High Temperature (전착된 폴리이미드 박막의 고온영역에서 절연파괴 특성에 관한 연구)

  • Yu, Y.B.;Sin, D.K.;Kim, B.J.;Kim, J.S.;Pak, K.S.;Kim, S.K.;Cho, D.H.;Han, S.O.
    • Proceedings of the KIEE Conference
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    • 1996.07c
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    • pp.1498-1501
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    • 1996
  • To evaluate insulating properties of polyimide thin film on high temperature over $100\;^{\circ}C$, polyimide film were prepared by electrophoretic deposition onto metal surface from nonaqueous emulsion. The emulsion is made by adding a solution of the resin to a precipitant, which is an organic liquid compeltely miscible with the solvent of the organic resin solution, but which does not dissolve the resin. The polyimide film obtained by annealing shows good insulation properties of 5.8 MV/cm at elevated temperature and breakdown strength of the film reveals thickness dependence.

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The study on preparation of $Sr_xBa_{1-x}$ $Nb_2O_6$ piezoelectric Thin Film of tungsten-bronze type by Metal Organic Decomposition Process and their properties (MOD 공법을 이용한 텅스텐 브론즈구조의 $Sr_x Ba_{1-x}$ $Nb_2O_6$ 압전 박막의 제조 및 특성 연구)

  • Kim, Kwang-Sik;Kim, Kyoung-Won;Jang, Gun-Ik;Ur, Soon-Chul
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.248-249
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    • 2005
  • The tungsten bronze type of strontium barium niobate(SBN) thin film was synthesized by metal organic decomposion method for SBN stock solution and the SBN thin film process were deposited by spin-coating process on Pt-deposited si-wafer(100) by magnetron sputtering system. The thickness of SBN thin film was 150$\sim$200 nm and were optimized for rpm of spin-coater system. The structural variation of SBN thin film was studied by TG-DTA and XRD. The deposited SBN stock solution on annealing at $400\sim800^{\circ}C$ a pure tungsten bronze SBN phase and the corresponding average grain size about 500$\sim$1000 nm influenced by annealing temperature.

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