• 한국주조공학회지
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• 제13권2호
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• pp.155-162
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• 1993

This study has been focused on the influence of the metallic mold cooling effects on the solidification structures and the mechanical properties for Al-10%Si alloy castings by the variation of pouring temperatures, metallic mold temperatures and Cooling part of metallic mold. The dendrite arm spacing of Al-10%Si alloy was decreased with increasing cooling rate. In case of bottom cooling of metallic mold, DAS was appeared to be $20-22{\mu}m$ and in the middle cooling, it was increased to $36-40{\mu}m$. The DAS decreased proportionally $with(cooling\;rate)^{-3/2}$ at pouring temperatures $680^{\circ}C$ and $(cooling\;rate)^{-1/2}$ at pouring temperature $760^{\circ}C$, but it was proportionally increased to $(local\;solidification\;time)^{1/2-1/3}$ at pouring temperature $680^{\circ}C$ and $760^{\circ}C$. The maximum tensile strength of Al-10%Si alloy casting was obtained in case of bottom cooling of mold at pouring temperature $680^{\circ}C$ and metallic mold temperature $320^{\circ}C$.

• 한국주조공학회지
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• 제18권3호
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• pp.283-288
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• 1998

Interest in rapid solidification of magnesium alloys stems from the fact that conventional ingot metallurgy alloys exhibit poor strength, ductility, and corrosion resistance. Such properties can be improved by microstructural refinement via rapid solidification processing. In this study, Mg-Zn alloys have been produced as continuous strips by melt overflow technique. In order to evaluate the influence of additional elements on the grain refinement and mechanical properties, Th and Zr were added in rapidly solidified Mg-5wt%Zn alloy. Then the microstructual observations were undertaken with the objective of evaluating the grain refinement as function of the cooling rate and the additional elements. The tremendous increase in hardness of Mg-Zn base alloys was mainly due to the refinement of the grain structure by the effect of rapid solidification and alloying elements. The formation of intermetallic phases on the grain boundaries may have a positive effect on the corroion resistance. Therefore, despite competition from many other developments, the rapid solidification processing of magnesium alloys emerges as a valuable method to develop superior and commercially acceptable magnesium alloys.

• Nuclear Engineering and Technology
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• 제32권1호
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• pp.34-45
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• 2000

This study is concerned with the experimental test and numerical analysis of the heat transfer and solidification of the molten metal pool with overlying coolant with boiling. In the test, the metal pool is heated from the bottom surface and coolant is injected onto the molten metal pool. Experiments were performed by changing the test section bottom surface temperature of the metal layer and the coolant injection rate. The two-phase boiling coolant experimental results are compared against the dry test data without coolant or solidification of the molten metal pool, and against the crust formation experiment with subcooled coolant. Also, a numerical analysis is performed to check on the measured data. The numerical program is developed using the enthalpy method, the finite volume method and the SIMPLER algorithm. The experimental results of the heat transfer show general agreement with the calculated values. The present empirical test and numerical results of the heat transfer on the molten metal pool are apparently higher than those without coolant boiling. This is probably because this experiment was performed in concurrence of solidification in the molten metal pool and the rapid boiling of the coolant. The other experiments were performed without coolant boiling and the correlation was developed for the pure molten metal without phase change.

• 한국주조공학회지
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• 제42권3호
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• pp.153-160
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• 2022

초내열합금 625 튜브의 제조에 필요한 원심주조품의 두께에 따라 응고조직과 기계적 특성에 미치는 영향을 고찰하였다. 10, 17, 50 mm 두께로 원심주조한 625합금에서 두께의 증가에 따라 주상정 부분의 길이와 2차 수지상 간격이 약간 증가하였으나 상온 인장특성은 큰 차이를 보이지 않았다. 주상정 부분의 응고는 일방향응고의 형태로 응고가 진행되기 때문에 일방향응고 조건을 변화시켜 2차 수지상의 간격을 비교하여 각 두께의 주조품에서 응고속도를 계산하였다. 두꺼운 주조품일수록 내부 다결정 조직의 비율이 증가하였다. 다결정 부분의 인장특성은 주상정 부분의 평균값과 유사한 값을 보였으며 이는 2차 수지상의 간격보다 결정립 형태의 영향인 것으로 사료된다.

• 한국주조공학회지
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• 제11권1호
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• pp.63-70
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• 1991

Aluminium alloy castings, which can be not only manufactured in larger geometrically complex shapes, but also show good mechanical properties in addition to light weight, have kept their potential use as structures in the field of automotives, industrial machines and aircrafts. The variations of eutectic Si size a great effect on the elongation, impact value, fracture toughness and fatigue crack propagation rate without changes in the tensile strength or yield strength. The cooling curves with the solidification rate between $1.4^{\circ}C\;/min$ and $19.1^{\circ}C\;/min$ were obtained. With the increase of solidification rate, DAS, eutectic Si size and grain size were all decreased, which enhanced the mechanical properties. The tensile strength and yield strength were the most greatly influenced by DAS, and the elongation and impact value by eutectic Si size.

• Corrosion Science and Technology
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• 제23권2호
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• pp.104-112
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• 2024

Al-Zn-Mg-Si alloy coatings have been developed to inhibit corrosion of cold rolled steel sheets, and an understanding of the alloy system helps prevent coating defects. We used a Bridgman furnace to characterise the nature and formation mechanisms of the phases present in the quaternary system with 0.4 wt% Fe. In the directional solidification experiments we imposed steep temperature gradients and varied the pull rate. After the samples were quenched in the furnace, detailed characterization of the samples was carried out by electron microscopy (SEM/EDS). From the dT/dt vs T plots of the cooling curves of the alloys, the solidification path was determined to be $Liquid{\longrightarrow[80]^{544-558}}{\alpha}-Al{\longrightarrow[80]^{453-459}}Al/Mg_2Si{\longrightarrow[80]^{371-374}}Al/Zn{\longrightarrow[80]^{331-333}}Zn/mgZn_2$. The formation mechanisms of the Mg and Zn containing phases and their morphology was discussed together with the effects of the cooling rate. Key findings include the lengthening of the mushy zone in directionally solidified samples remelted against a positive temperature gradient, as well as an enrichening of the α-Al phase by Zn through remelting. Mg₂Si and other Si based phases were observed to adopt a much finer faceted microstructure in favour of a script-like microstructure when exposed to the higher cooling rate of coolant quenching.

• 한국주조공학회지
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• 제21권6호
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• pp.343-349
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• 2001

The effect of cooling rate on the solidification microstructure and segregation behavior of 7075 and 7050 aluminum alloy was investigated. Samples were solidified with cooling rates from 0.3 to $17^{\circ}K/sec$. Using the cooling curves of each sample, liquidus, eutectic and intermetallic reaction temperatures were estimated. The microstructures were characterized in terms of dendrite arm spacing and eutectic volume fraction. The segregation behavior of each alloying element of these alloys in various cooling rates was discussed.

• 한국주조공학회지
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• 제2권1호
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• pp.2-11
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• 1982

In order to investigate the relationship between the thermal characteristics of the various molds as green sand mold, dry sand mold, $CO_2$ mold and shell mold, and the solidification characteristics of molten metal, the thermal analysis of rarious molds and melt were performed. The structure of Al-Castings was a/so observed. Results obtained in this experiment were as follows : 1) The heating rate of the molds was increased in the order of green sand mold, $CO_2$ mold, dry sand mold and shell mold, On the other hand the solidification time of the melts was shortened in the order of dry sand mold castings, $CO_2$ mold castings, green sand mold castings and shell mold castings. 2) The arrest temperature period in the heating curve of the green sand mold was resulted from the eraporation of moisture contained in mold, which was transfered to the outer side of the mold. 3) The temperature fluctuation of the melt in the shell mold was considered to be resulted from the combution heat of resin contained in the mold. 4) The amounts of heat absorption of the molds were increased in the order of dry sand mold, $CO_2$ mold, green sand mold and shell mold. 5) The higher the solidification rate was, the longer was its shrinkage pipe and the finer its grain size.

• 한국재료학회지
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• 제12권5호
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• pp.398-406
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• 2002

VAR process is required to control its various operating parameters. Heat transfer simulation has been accomplished to understand development of solidification micro and macro-structures during VAR process in Ti alloys. Optimum VAR process parameters could be also estimated in this study. It was found that macro-structures were closely related to the shape and depth of liquid pool, and solidification parameters, such as temperature gradient, heat flux, solid fraction. The cooling rates were higher at bottom, top, and center part respectively. As cooling rates increased, the $\alpha$ phase decreased in length, width and fraction. In order to evaluate which parameter affects the result of heat transfer calculation most sensitively, the sensitivities of input parameters to the simulation result were examined. The pool depth and cooling rate showed more sensitive to the temperature of the molten metal, heat transfer coefficient, and liquidus respectively. Also, these thermal properties became more sensitive at higher temperatures.

• 한국주조공학회지
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• 제15권2호
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• pp.164-174
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• 1995

New metallic powder making processes, named "Centrifugal Emulsification Process(CEP)" and "Mixer and Settler(MS)" have been developed to synthesize rapid solidified metallic powders. Through CEP and MS processings, the high temperature metals as well as the low temperature alloys are manufactured. Also, the effects of rapid solidification on the undercooling, solidification rate and crystallization behaviors can be evaluated effectively through the processes. The standard deviations of the synthesized typical Pb-Sn eutectic powders are 1.63 and 1.51 for CEP and MS respectively, and the average size of the MS powders was $18{\mu}m$. The possibility of the customized not only size and shape control but microstructure control was also shown. Both of the new methods can be applied to continuous powder making processes.