• 한국자기공명학회논문지
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• 제16권2호
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• pp.103-110
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• 2012

Membrane proteins play a essential role in the biological systems and it is not easy to handle a membrane protein for its structural study. Solid-state NMR (ssNMR) can be a good tool to investigate the structures and dynamics of membrane proteins. In ssNMR, Magic Angle Spinning (MAS) and Cross Polarization (CP) can be utilized to reduce the line-broadening, leading to high resolution and sensitivity in the spectrum. ssNMR, if combined with other spectroscopic methods, can provide us a enough knowledge on structures and dynamics of membrane proteins in biological condition.

• 대한약학회:학술대회논문집
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• 대한약학회 2003년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.2-2
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• pp.236.1-236.1
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• 2003

Evaluation of solid surface properties is very important for formulation of solid dosage form, specially insoluble drugs. The contact angle of insoluble drugs was measured by the penetration rate into powder bed using Washburn equation and wicking method. From the measured contact angle data, the surface free energy value of pharmaceutical powders ${\gamma}$s was divided and analysized into the polar component, ${\gamma}$s$\^$p/ and the dispersion component, ${\gamma}$s$\^$d/. Furthermore, the data was interpreted for acid part, ${\gamma}$s$\^$+/ and base part, ${\gamma}$s$\^$$\square$/ of surface free energy. (omitted)

• 한국가시화정보학회지
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• 제21권3호
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• pp.7-14
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• 2023

In this study, we investigated the freezing delay time on surfaces with different patterns under -30° conditions through visualization experiments. Among various pattern structures, we fabricated the shape and surface of liquid from the spacing using circular filaments and hole structures. Additionally, using a high-speed camera, we visualized the freezing scenes, enabling us to obtain freezing images and measure the freezing time of the liquid. For each structure, the contact angle and solid fraction of the surface varied. We observed that the freezing delay time was longest when the contact angle was largest and the solid fraction was smallest within the experimental results. We analyzed the variation in anti-icing time using the heat exchange equation between the patterned surface and the liquid.

• Structural Engineering and Mechanics
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• 제23권4호
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• pp.339-352
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• 2006

Observing the unique stress-strain curves of the superelastic shape memory alloy (SMA) in tension and compression, the primary intention of this study is to investigate the behavior of the shafts made of the same material, under torsional loading-unloading cycles for large angle of twist. Experiments have been performed for the superelastic SMA shafts with different unsupported lengths and angles of twist and the results are compared with those of stainless steel (SUS304) shafts under similar test conditions. As expected for the superelastic SMA, the residual strains are small enough after each cycle and consequently, the hysteresis under loading-reverse loading is much narrower than that for the SUS304. For large angle of twists, the torsional strength of the superelastic SMA increases nonlinearly and exceeds that of SUS304. Most interestingly, the slender solid superelastic SMA shafts are found to buckle when acted upon torsion for large angle of twist.

• 한국자기공명학회논문지
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• 제3권2호
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• pp.127-139
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• 1999

In this paper we discussed how multiple quantum coherences evolve in the presence of anisotropic distribution of dipolar couplings. The magnitude of dipolar couplings were varied by changing the tile angle of crystal axis. The stronger was dipolar coupling, the higher was frequency of multiple quantum coherence. That is, the order of multiple quantum coherence varies in proportion to the magnitude of dipolar couplings. The theoretical prediction for the multiple quantum coherence at magic angle 54.7$^{\circ}$ in solid NMR spectroscopy was verified in this study. The excitation pattern of n-quantum coherence, which can induce the effective size to characterize spin system, is expected in a larger and more complicated spin system for understanding of the relation of dipolar coupling and multiple quantum coherence.

• 설비공학논문집
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• 제13권10호
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• pp.1042-1048
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• 2001

When a liquid is supplied through a nozzle onto a relatively non-wetting inclined solid surface, a narrow rivulet forms. This work provides novel physical insights into the following phenomena in the rivulet flow that have not been well understood to date. Firstly, the fundamental mechanism behind the transition of a linear rivulet to a droplet flow is investigated. The experiments show that the droplet flow emerges due to the necking of a liquid thread near the nozzle. Based on the observation, it is argued that when the axial velocity of a liquid is slower than the retraction velocity of its thread, the bifurcation of the liquid thread occurs, and this argument is experimentally verified. Secondly, a discussion on the curled motion of a meandering rivulet is given. This study proposes the contact angle hysteresis as a primary origin of the centripetal force that enables the rivulet\`s curved motion. A simple scaling analysis based on this assumption predicts a radius of curvature which agrees with the experimental observation.

• Carbon letters
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• 제4권1호
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• pp.10-13
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• 2003

The structural studies of amorphous isotropic carbon prepared from pyrolysis of phenol formaldehyde resin have been carried out using X-ray diffraction. X-ray diffraction from as prepared sample at $1000^{\circ}C$ and a sample treated at $1900^{\circ}C$ revealed that both are amorphous even though there are small differences in short range order. It is found that both are graphite like carbon (GLC) with predominantly $sp^2$ hybridization. Small angle X-ray scattering results show that as prepared sample mainly consists of thin two dimensional platelets of graphitic carbon whereas they grow in thickness to become three dimensional materials of nano dimensions.

• 대한설비공학회지:설비저널
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• 제16권3호
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• pp.285-294
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• 1987

Parametric study on the efficiency of Rotary Solid Dehumidifer are reported. Experi-ments have been performed by varying regeneration temperature, regeneration humidity, flow rate of regeneration air, angular velocity of dehumidifer rotor and regeneration angle. To improve the energy efficiency, MODE 2,3 where coding zone is constructed and MODE 4, 5 where recirculating zone is constructed, were studied through experimental method $\ldots$. These results show that economical operating ranges exist in regeneration temperature, flow rate of regeneration air, angular velocity of dehumidifier rotor and regeneration angle. MODE 2,3 where cooling zone is constructed between regeneration Bone and process zone, is far better than MODE 1 in view of energy effiency, and optimum cooling angle and flow rate of cooling air exist. But MODE 4 and MODE 5, where recirculating zone is constructed, are similar to MODE 1.

• Bulletin of the Korean Chemical Society
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• 제30권5호
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• pp.1077-1079
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• 2009

To minimize the variance in the quantification of solid-state phases in powder samples, gently placing polycrystalline samples one next to another directly in a sample holder is better than trying to mix them homogeneously prior to transferring to a sample holder. However, the solid-state cross polarization-magic angle spinning (CP-MAS) nuclear magnetic resonance (NMR) spectroscopy results demonstrated that it is essential in this sampling method to place all the samples in the location of consistent signal sensitivity. The same sampling method may be employed in other spectroscopic quantification techniques of solid-state phases if the method to limit the sample to the location with uniform signal sensitivity in the sample holder is adapted to each technique.

• 대한의생명과학회지
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• 제25권2호
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• pp.170-176
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• 2019

The objective of this study was to evaluate the characteristics of the mixtures of choline alphoscerate (alpha-glycerylphosphorylcholine, alpha-GPC), in the liquid form, and sucrose ester, which formed a solid composite. The choline alphoscerate solid composites were prepared using different ratios of sucrose ester, and different preparation methods, such as air drying and rotary evaporation, were compared for their preparation efficacy. We examined the characteristics of the solid composites by using scanning electron microscopy (SEM), angle of repose, and moisture content. The ideal mixing ratio of choline alphoscerate and sucrose ester was determined as 1:3 and air drying was found to be more suitable for the preparation of solid composites than rotary evaporation. SEM measurements of the degree of dispersion and the size of particles indicated that a high-temperature air method was more suitable. These results demonstrated the successful preparation of choline alphoscerate solid composites that have potential for industrial use.