• Title/Summary/Keyword: Softening heat treatment

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Effects of Long-term Heat treatment on Mechanical Softening of Mn-Mo-Ni Low-Alloy Steel (Mn-Mo-Ni 저합금강의 기계적 연화에 미치는 장시간 열처리 영향)

  • Kim, Minsuk;Kim, Chungseok
    • Journal of the Korean Society for Heat Treatment
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    • v.34 no.6
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    • pp.294-301
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    • 2021
  • In the present study, we investigate the effects of long-term heat treatment at elevated temperatures on the mechanical softening of the Mn-Mo-Ni low-alloy steel. The influence of long-term heat treatment on microstructure and mechanical strength was evaluated. To simulate the long-term material degradation, heat treatment test was interrupted at several stages up to 10,000 hours in an electric furnace. The Mn-Mo-Ni low-alloy steel shows a typical bainitic phase, which consists of a well-developed lath substructure with fine precipitates along the lath boundaries. However, these fine precipitates were redissolved into the matrix with long-term heat treatment, and then the lath substructures were recovered. Consequently, ultimate tensile strength and yield strength decreased during long-term heat treatment showing a mechanical softening phenomenon.

데침과 열수 침적의 병용 열처리와 trehalose 첨가가 오이 김치의 저장중의 효소 활성의 변화와 관능 검사에 미치는 효과

  • 이혜정
    • Proceedings of the Korean Journal of Food and Nutrition Conference
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    • 2001.12a
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    • pp.131-131
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    • 2001
  • The enzyme activity and organoleptic properties of Korean pickled cucumber were studies for their changes during fermentation. The Korean pickled cucumber were prepared by blanching and high temperature soaking in salt solution and trehalose treatment The results shelved that the effect of combined heat and trehalose treatment significantly reduced the fermentation rate and softening rate of texture while a rather rapid fermentation was for those pleserved with salt. The effect of trehalose treatment enhenced fermentation and it was significantly reduced softening rate of texture by 2% treatment. The sensory evaluation of Korean pickled cucumber was found that combined heat treatment with blanching and hot solution had a positive effect for reduction of softening of cucumber tissue, however, odor and taste were not significantly affected. This study suggested that combined heat and trehalose treatment might have potential for affording protection against softness of cucumber tissue during the fermentation time.

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Local Softening of Hot-stamped Parts using a Laser Heat Treatment (레이저 열처리를 이용한 핫스탬핑 부품의 국부 연화 기술 연구)

  • Kim, K.B.;Jung, Y.I.;Kim, T.J.
    • Transactions of Materials Processing
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    • v.24 no.5
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    • pp.354-360
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    • 2015
  • AHSS (Advanced High Strength Steels) has been increasingly employed by global automotive OEMs in order to satisfy strengthened regulations and reduce weight for fuel efficiency. Hot stamping using boron steels in AHSS increases not only formability but also strength. The typical hot-stamped automotive part is the center pillar that is critical for vehicle side impact. However, the hot-stamped part can be risky for the passenger safety caused by brittle fracture under a vehicle collision. The high power diode laser is suitable for the heat treatment giving AHSS increased elongation that prevents brittle fracture in car crash. Therefore, local softening by laser heat treatment for energy absorption area on the hot-stamped part improves crash-worthiness.

Softening Studies of Raw Sea Tangle Texture for Improvement of Its Processing Compatibility (가공적성 향상을 위한 다시마 조직의 연화에 관한 연구)

  • 송재철;신완철;박현정
    • The Korean Journal of Food And Nutrition
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    • v.17 no.2
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    • pp.186-192
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    • 2004
  • This study was performed to investigate softening methods of raw sea tangle for development of sea tangle processing products and intermediate materials. In examination of various softening agents, it was revealed that 0.3% sodium triphosphate was best effective on softening with heat treatment. Softerness and spreadability of sea tangle treated with sodium triphosphate and heat treatment were indicated to be better than the others. In blanching studies, microwave was extremely effective on softening and the effect was as follows: microwave>steaming>boiling water in softening order. In the case of adding 0.3% sodium triphosphate in blanching treatment, there was synergy effectiveness on softening. The color change of treated sea tangle was significantly different at p<0.05 depending on blanching method and addition amount of the agent.

Changes of Microstructure and Properties of Manufactured Modified Pitches via Pressure Changes during Heat Treatments in Coal Tar Pitch (석탄계 타르의 열처리 중 압력변화에 따른 변성 콜타르 핏치의 미세구조 및 물성 변화)

  • Ko, Hyo Joon;Chung, Sung Mo;Han, Ji Hoon;Park, Chang Uk;Kim, Myung-Soo;Lim, Yun-Soo
    • Korean Journal of Materials Research
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    • v.24 no.6
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    • pp.293-300
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    • 2014
  • Coal-tar pitch, a feedstock which can be heat-treated to create graphite, is composed of very complex molecules. Coal-tar pitch is a precursor of many useful carbon materials (e.g., graphite, carbon fibers, electrodes and matrices of carbon/carbon composites). Modified coal-tar pitch (MCTP) was prepared using two different heat-treatment methods and their properties were characterized and compared. One was prepared using heat treatment in nitrogen gas; the other was prepared under a pressure of 350 mmHg in air. The MCTPs were investigated to determine several properties, including softening point, C/H ratio, coke yield, formation of anisotropic mesophase and viscosity. The MCTPs were subject to considerable changes in chemical composition due to condensation and polymerization in the used-as-received coal-tar pitch after heat-treatment under different conditions. The MCTPs showed considerable increases in softening point, C/H ratio, and coke yield, compared to those of as-received coal-tar pitch. The MCTP formed by heat-treatment in nitrogen showed isotropic phases below $350^{\circ}C$ for 1 h of soaking time. However, MCTP heat-treated under high pressure (350 mmHg) showed isotropic phases below $300^{\circ}C$, and showed anisotropic phases above $350^{\circ}C$, for 1 h of soaking time. The viscosity of the MCTPs increased with increase in their softening points.

The Properties of Blanching and Brining in Hot Solution and Trehalose Treatment on the Quality of Cucumber Kimchi during Fermentation (데침과 열수의 침적과 Trehalose 처리가 오이 물김치의 저장중 품질에 미치는 영향)

  • 이혜정
    • The Korean Journal of Food And Nutrition
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    • v.14 no.4
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    • pp.333-338
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    • 2001
  • In research. which Korean pickled cucumber was treated wish various methods, including blanching. brining in hot solution, and treating with trehalose. I examined the changes of properties of material. The Korean pickled cucumber were fermented 4∼5$^{\circ}C$ for 42 days in 1% salt solution. The physiochemical properties were pH, total acidity, total cell count, lactic acid bacteria and texture properties were also evaluated. The result showed that the effect of blanching and soaking cucumber in 100$^{\circ}C$ hot salt solution significantly reduced the softening rate of texture while a rather rapid fermentation was found for those preserved with salt. The effect of trehalose treatment inhenced fermentation but it was significantly reduced softening rate of texture. The texture evaluation of Korean pickled cucumber was found that heat treatment with blanching after soaked in hot solution and trehalose treatment had a positive effect for reduction of softening of cucumber tissue.

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Fatigue Behavior of 23Cr26Ni Heat Resistant Steel (23Cr26Ni 내열강의 피로 특성)

  • Lee, H.W.;Kwun, S.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.24 no.2
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    • pp.92-98
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    • 2011
  • The influence of the cooling condition after solution treatment on the high temperature fatigue resistance of 23Cr-26Ni heat resistant steel was investigated. Two different cooling conditions were applied to the steel after solution treatment at $1200^{\circ}C$ for 3 hours. One specimen was water quenched immediately after the solution treatment. The other one was furnace cooled at a rate of $0.5^{\circ}C/min$ down to $750^{\circ}C$ after the solution treatment. Then, both specimens were aged at $750^{\circ}C$ for 5 hours. Under two different heat treatment conditions, the low cycle fatigue (LCF) test was performed at $600^{\circ}C$ and room temperature (RT). Only cyclic hardening continued from the beginning until fracture at all strain amplitudes during LCF at $600^{\circ}C$. This phenomenon was attributed to the increase in the dislocation density due to cyclic deformation, which resulted in the interaction between the newly created dislocations and precipitates. Cyclic hardening followed by saturation and cyclic softening was observed at RT. Cyclic softening was attributed to the dislocation annihilation rate exceeding the dislocation generation rate. Other probable factor for cyclic softening was some cavities formed around grain boundaries after 20 cycles. WQ and FC have a similar LCF behavior at RT and $600^{\circ}C$ as shown in the cyclic stress response curves.

Effect of Washing and Subsequent Heat Treatment on Water Repellency and Mechanical Properties of Nylon 6, Triacetate and Silk Fabrics Treated with Hydrocarbon Resins

  • Park, Hyei-Ran;Lee, Mun-Cheul;Nishi, Kenji;Wakida, Tomiji
    • Textile Coloration and Finishing
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    • v.20 no.6
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    • pp.87-91
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    • 2008
  • It is commonly known that water repellency of the fabric treated with fluorocarbon resin brings about a decrease by the washing and recovers by the subsequent heat treatment. In this article, effect of the water repellency was investigated on the nylon 6, triacetate and silk fabrics treated with hydrocarbon and silicon resins. Hydrocarbon and silicon resins have been widely used in the textile finishing as the softening and water proofing agents. The fabrics were treated with hydrocarbon resins, Paragium JQ and RC (Ohara Paragium Chemical Co.) and a silicon resin, Poron MR (Shinetsu Chemical Co.), and then washed and subsequently heat treated. Although the water repellency increased by the resin treatment, it decreased by the washing apparently and recovered a little by the heat treatment. The effect of the heat treatment was small comparing with that of the fluorocarbon resin. Furthermore, as a mechanical property of the treated fabric, KES shearing and bending hysteresis parameters, modulus and hysteresis width of the hydrocarbon resin-treated nylon 6, triacetate and silk fabrics decreased by the heat treatment after washing. Therefore, the treatment is effective at improving the softening of the fabric in water repellent finish.

Effect of Post Weld Heat Treatment on the Mechanical Properties of 2.25Cr-1Mo Steels Valves and Piping (용접후열처리가 2.25Cr-1Mo 강 밸브 및 배관재 물성에 미치는 영향)

  • Kim, Hongdeok;Lee, Yoseob;Lee, Jaegon;Lee, Kyoungsoo
    • Transactions of the Korean Society of Pressure Vessels and Piping
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    • v.11 no.1
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    • pp.33-38
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    • 2015
  • The effects of post weld heat treatment(PWHT) on the mechanical properties of 2.25Cr-1Mo steels were investigated. As the PWHT temperature or holding time increased, the strength of low alloy steels progressively decreased due to softening process. After the conventional PWHT, the strength was larger than the minimum value of materials specification. The Charpy impact energy was hardly affected by the conventional PWHT. The trend of mechanical properties was analyzed in terms of tempering parameter. Most materials replaced from a power plant met the requirements of materials specification except for one heat. Same heat of materials with low impact energy were attributed to the voids formed during casting process.

The softening behavior of Mg-Li-Al(-Zr) alloys (Mg-Li-Al(-Zr) 합금의 연화현상)

  • Kim, Y.W.;Kwang, Y.H.;Lim, Y.J.;Kim, D.H.;Hong, C.P.
    • Journal of the Korean Society for Heat Treatment
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    • v.11 no.1
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    • pp.10-16
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    • 1998
  • The softening behavior of squeeze cast Mg-Li-Al and Mg-Li-Al-Zr alloys have been investigated. The highest hardness values of Mg-Li-Al and Mg-Li-Al-Zr alloys were obtained after solution treatment at $400^{\circ}C$ for 1 hour. The hardness value, however, decreased as the aging temperature and time increased. Microstructural and calorometric analyses showed that quenched-microstructure changed from primary (${\alpha}$ and ${\beta}$)+secondary ${\alpha}$ to primary(${\alpha}$ and ${\beta}$)+secondary ${\alpha}+{\theta}$ after aging. The softening during aging was due to the coarsening of ${\theta}$ precipitates.

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