• 한국재료학회지
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• 제12권9호
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• pp.706-711
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• 2002

High-pure tantalum powder was fabricated through Na reduction process and has been produced by using $K_2$TaF$_{7}$, and KCI, KF for raw material and diluent, respectively. A raw material and diluent were charged at the hestalloy bomb by the weight rate of 1:2, 1:1, 1:0.5 and 1:0.25 each other, investigated properties of morphology, chemical composition and yield and particle size after reduced. Ta metal has been achieved by reduction of $K_2$$TaF_{7}$ 500g with 1% sodium in excess of stoichiometric amount in the charge at a reduction temperature of $850^{\circ}C$ for 3hours. According to amount of the diluent, a formation of the powder doesn't have an effect. The diluent prevented the temperature rising caused from the heat of reaction and it maintained the speed of reducing reaction. But in the mixture ratio of raw material and diluent in the 1 : 2 and 1 : 0.25, an oxide and partially not reacted K were detected. As the amount of diluent increased, the size of tantalum powder decreased. According as raw material and the mixture ratio of diluent change from 1:0.25 to 1:2, the size is decreased from 5$\mu\textrm{m}$ to 1$\mu\textrm{m}$, and a particle size distribution which is below 325 mesh in fined powder increases from 71% to 83%. In the case of average size of Tantalum powder which is the mixture ratio (1:0.5), we would get the Ta powder with grain size about 3$\mu\textrm{m}$, which come close to the average size (2~4$\mu\textrm{m}$) of tantalum powder which is used commonly in the present is Ta powder about 3$\mu\textrm{m}$.

• 한국재료학회지
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• 제15권4호
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• pp.263-270
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• 2005

In order to prepare the uniform copper particles from copper chloride solution, the reduction behavior of copper particles from copper chloride and the effects of reduction agent and dispersing agent was investigated. In the case that 2.56 M of $C_6H_8O_6$ was used as a reduction agent, the highly dispersed Cu particles with sharp size distribution were generated from 0.96M of copper chloride solution, and the size of Cu particles was $6\~10\;{\mu}m$. To form $Cu(NH_3)_4Cl_2$ complex solution, $NH_4OH$ was added in the copper chloride solution before the reductive reaction of Cu ion. The generated Cu particles have a two kind of shape, spherical and rod-like. In the case that $N_2H_4{\cdot}H_2O$ was used as a reduction agent, the very fine spherical Cu particles with the size of $0.2\~0.5\;{\mu}m$ was obtained. Arabic gum as a dispersing agent was more effective than $Na_4P_2O_7{\cdot}10H_2O$.

• 한국분말재료학회지
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• 제20권5호
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• pp.359-365
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• 2013

In this study, we fabricated $Nd_2Fe_{14}B$ hard magnetic powders with various sizes via spray drying combined with reduction-diffusion process. Spray drying is widely used to produce nearly spherical particles that are relatively homogeneous. Thus, the precursor particles were prepared by spray drying using the aqueous solution containing Nd salts, Fe salts and boric acid with the target stoichiometric composition of $Nd_2Fe_{14}B$. The mean particle sizes of the spray-dried powders are in the range from one to seven micrometer, which are adjusted by controlling the concentrations of precursor solutions. After debinding the as-prepared precursor particles, ball milling was also conducted to control the particle sizes of Nd-Fe-B oxide powders. The resulting particles with different sizes were subjected to subsequent treatments including hydrogen reduction, Ca reduction and washing for CaO removal. The size effect of Nd-Fe-B oxide particles on the formation of $Nd_2Fe_{14}B$ phase and magnetic properties was investigated.

• 한국방재학회 논문집
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• 제10권3호
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• pp.109-118
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• 2010

본 연구에서는 소규모 저류시설의 유출저감효과를 NRCS 유출곡선지수의 감소율로 정량화하였다. 저류시설로 유입되는 유출용적을 계산하기 위해 수정합리식을 이용하였다. 다양한 강우 특성(강우 빈도, 지속시간)과 저류시설의 규모에 따라 설치 전후의 NRCS 유출곡선지수 감소율을 정량화하였다. 마지막으로 저류시설의 규모에 따른 유출곡선지수의 감소율을 나타내는 도표를 개발하였다. 이 도표는 저류시설의 최적 위치 및 용량 결정을 할 경우 저류시설의 효율을 평가하는데 합리적이고 효율적으로 활용될 수 있을 것으로 기대된다. 본 연구에서 제안된 방법에 의한 결과는 또한 기존 연구와의 비교를 통해 검증하였다.

• 한국수자원학회논문집
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• 제39권11호
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• pp.915-922
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• 2006

본 연구는 소방방재청에서 계획하고 있는 도시유역의 침수피해를 방지하기 위한 대책 수립의 일환으로 도시유역의 중상류부에 중소규모의 저류지를 설치하는 방안에 대한 유출저감 효과 분석에 관한 것이다. 이를 위해 시범유역을 선정하여 유출분석을 실시하였고 저류지의 위치와 규모에 따른 유출저감 정도 및 치수안전도 확보 효과를 분석하였다. 분석결과 유역의 유출량을 모두 하도에서 소통시키는 개념이 아닌 유역에서 홍수량의 일부를 저류하여 유량을 분담하는 유역분담 저류지를 설치함으로써 하도의 부담을 완화시킬 수 있음을 확인하였고 저류지의 입지 및 규모의 선정에 따라 그 효과에 큰 차이가 있음을 알 수 있었다. 따라서 중상류부에 저류지를 설치하는 경우 하류부 유출 저감에는 상당히 효과적인 것으로 나타나 유역의 치수안전도 확보에 효율적인 방안이 될것으로 기대된다.

• 상하수도학회지
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• 제26권6호
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• pp.735-745
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• 2012

Storage method is one of major measures for reduction of CSOs pollutant loads and several projects have been done nationwide. But systematic analysis of intercepting capacity has not been studied to determine optimum size of storage facility. In this research, not only storage volume but also intercepting capacity which means flow capacity from intercepting facility to CSOs storage facility was studied and optimum sizing method for storage facility was proposed. The result shows that pollutants reduction efficiency can be increased significantly by increasing intercepting capacity and it might reduce storage volume and total construction costs. Intercepting capacity for the study area was evaluated and it was shown as equivalent to 83 % probability rainfall intensity.

• 품질경영학회지
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• 제31권2호
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• pp.131-142
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• 2003

QFD(Quality Function Deployment) is design method which is focused to guarantee of quality and function to satisfy for customer’s need. QFD are used entire manufacturing, specially new production development and design. HOQ(House of Quality) are important tool of QFD, which is implement that complex function and communications of customer. Actually implementation of HOQ are difficult by HOQ's size. It is well known that complexity of HOQ are exponentially increasing by increasing of HOQ’s size. In this Paper, we study of HOQ Complexity reduction by Quantification Method of Type Ⅲ. That method is efficiency and minimize of loss information by reduction HOQ. We give example and prove our suggestion method is better than other methods.

• 한국분말재료학회지
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• 제21권2호
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• pp.93-96
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• 2014

Cobalt coated tungsten carbide-cobalt composite powder has been prepared through wet chemical reduction method. The cobalt sulfate solution was converted to the cobalt chloride then the cobalt hydroxide. The tungsten carbide powders were added in to the cobalt hydroxide, the cobalt hydroxide was reduced and coated over tungsten carbide powder using hypo-phosphorous acid. Both the cobalt and the tungsten carbide phase peaks were evident in the tungsten carbide-cobalt composite powder by X-ray diffraction. The average particle size measured via scanning electron microscope, particle size analysis was around 380 nm and the thickness of coated cobalt was determined to be 30~40 nm by transmission electron microscopy.

• 산업기술연구
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• 제29권B호
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• pp.229-232
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• 2009

We prepared gold nanoparticles (Au NPs) by reduction-oxidation reaction between $HAuCl_4$ and trisodium citrate and measured the size and morphology of Au NPs by TEM for various molar ratios of $HAuCl_4$ to citrate and for various concentrations of $HAuCl_4$. UV-vis spectroscopy was used to characterize the optical properties of Au NPs. Au NPs in the size range from 14.3 nm to 20.3 nm were prepared with monodisperse distribution.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2005년도 추계학술강연 및 발표대회강연 및 발표논문 초록집
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• pp.87-88
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• 2005

Ultra-fine copper powders with particle size about 150 nm were synthesized from copper hydroxide slurry by wet method using hydrazine as reduction agent and several sur factants at below $80^{\circ}C$. The particle size distribution and dispersion of synthesized powders as function of temperature, feeding rate of reduction and especially, sur factants were character ized by XRD, BET, PSA and SEM by this process.