• Title/Summary/Keyword: Size deviation

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Optimization of Silver Nanoparticles Synthesis through Design-of-Experiment Method (실험계획법을 활용한 은 나노 입자의 합성 및 최적화)

  • Lim, Jae Hong;Kang, Kyung Yeon;Im, Badro;Lee, Jae Sung
    • Korean Chemical Engineering Research
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    • v.46 no.4
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    • pp.756-763
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    • 2008
  • The aim of this work was to obtain uniform and well-dispersed spherical silver nanoparticles using statistical design-of-experiment methods. We performed the experiments using 2 k fractional factorial designs with respect to key factors of a general chemical reduction method. The nanoparticles prepared were characterized by SEM, TEM and UV-visible absorbance for particle size, distribution, aggregation and anisotropy. The data obtained were analyzed and optimized using a statistical software, Minitab. The design-of-experiment methods using quantified data enabled us to determine key factors and appreciate interactions between factors. The measured properties of nanoparticles were dominated not only by individual one or two main factors but also by interactions between factors. The appropriate combination of the factors produced small, narrow-distributed and non-aggregated silver nanoparticles of about 30 nm with approximately 10% standard deviation.

A Study of the Purchasing Traits and the Wearing Satisfaction of Ski Wear (스키웨어의 구매와 착용만족도에 관한 조사연구)

  • Kim, Soon-Boon
    • Fashion & Textile Research Journal
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    • v.8 no.3
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    • pp.295-302
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    • 2006
  • The purpose of this study was to research the purchasing traits and the wearing satisfaction of ski wears to provide the data needed to design ski wears to the related industries. This survey was performed during 2003's and 2004's winter with the 157 questionnaires containing 16 items of purchasing traits, 8 of design satisfaction, 12 of purchasing satisfaction and 13 of satisfaction of using convenience. The data were analysed with the frequency, the percentile, $X^2$-test, the average, the standard deviation and t-test through comparing with the groups of general people and experts, and the groups of male and female. The results were:1.The most preferred style was the two pieces style(88.5%), and then the loose style(61.1%), and the shoulder-wireless style(36.9%). 2.The imported brands were more preferred because of the design(44.1%). 3.The main place of purchasing was the ski wear speciality shop(48.4%), the main source of the merchandise information was the surrounding men(43.3%), the most significant consideration aspect when purchasing was the design(35.7%), and the rate of size perception was 51.6%. 4.The wearing satisfaction score(5) of ski wears were; the satisfaction of design was 3.24, the satisfaction of material 3.00, and the satisfaction of using convenience 3.07. 5.In the rate of design satisfaction, the female(3.10) showed higher than the male(3.35) (p<.05). 6.In the satisfaction of material, 'the discoloration'(2.37), 'the abrasion'(2.75), 'the sense of volume'(2.76) and 'the sense of touch' showed dissatisfaction. 7.In the satisfaction of using convenience, 'the pollution by lifting ticket'(2.36)was showed most dissatisfaction.

A Method for the Preliminary Estimation of Vertical Natural Vibations of High Speed Boats (고속선(高速船) 선체고유상하진동(船體固有上下振動)의 초기추정(初期推定) 방법(方法))

  • K.C.,Kim;H.B.,Kim
    • Bulletin of the Society of Naval Architects of Korea
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    • v.17 no.1
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    • pp.25-29
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    • 1980
  • For the preliminary estimation of the vertical hull natural frequency, the Schlick's or Schlick-type formulae have been traditional ones and are still in common use today. Some investigators have made their efforts, based on statistical data of ships' system parameters, to extend the applicability of Schlick-type formulae to higher modes, or to utilize the Rayleigh method. For instance, the work done by Dinsenbacher et al.[5] belongs to the former and that of Nagamoto et al.[6] to the latter. In a part of his previous paper[7], the author, investigating the case of a cargo ship of medium size, suggested that provided statistically simplified curves such as trapezoid of system parameter distributions are available in hands, direct utlization of an ordinary computer program can be also an another convenient method by which we can obtain both natural frequencies and normal mode shapes. In this paper, to confirm the feasibility of the above suggestion, four high speed boats are investigated. The system parameters of them are originally given in [5]. The computer program used here is one confiled based on a calculation method derived from Myklestal-Prohl modeling of hull, transfer matrix formulation and an extended Gumbel's initial value method for solving frequency equation. The results of the investigation show that the direct calculation based on statistically oriented and reasonably assumed trapezoidal mean curves of system parameter distributions can give us natural frequencies within about 5% deviation up to several-noded modes and normal mode shapes serviceable at least up to 4- or 5-noded modes in comparision with those based on actual distributions of system parameters. For this simplified method the actual data required for input are only of ship length, displacement, total added mass, bending and shear rigidity at amidship. They are available at the early stage of design. By this method we can also easily trace variations of vibration characteristics in the course of ship design cycles.

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Effect of Additives on the Viability of Bifidobacteria Loaded in Alginate Poly-l-lysine Microparticles during the Freeze-drying Process

  • Cui, Jing-Hao;Cao, Qing-Ri;Choi, Yun-Jaie;Lee, Kyung-Hoon;Lee, Beom-Jin
    • Archives of Pharmacal Research
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    • v.29 no.8
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    • pp.707-711
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    • 2006
  • Bifidobacteria-loaded alginate poly-l-lysine microparticles (bap microparticles) were prepared using an air atomization method and then freeze-dried. The viability of the bap microparticles was investigated as a function of the amount of the bifidobacteria cultures, and the addition of a yeast extract, cryoprotectants, antioxidants and neutralizer. The size of the bap microparticles with and without the bifidobacteria was $84.8{\pm}28.5\;{\mu}m$ ($mean{\pm}standard$ deviation) and $113.1{\pm}38.5\;{\mu}m$, respectively. The surface morphology was slightly ellipsoid and wrinkled regardless of the incorporating bifidobacteria. The viability gradually decreased with increasing freeze-drying time. Free-flowing powdered bap microparticles were obtained at least 12 h after freeze-drying the wetted slurry of bap microparticles. However, the particles tended to aggregate when either lactose or ascorbic acid was added. The addition of a yeast extract, cryoprotectants (glycerol and lactose), antioxidants ($NaHSO_3$ and ascorbic acid) and neutralizer $(Mg_3(PO_4)_2)$ resulted in a significantly higher viability of the bifidobacteria in the bap microparticles after freeze-drying (0.34-1.84 log) compared with the culture alone.

Design and Analysis of a Red-Green-Blue Beam Combiner Based on Multimode Waveguides (다중 모드 도파로를 이용한 적녹청 빔 합파기 설계 및 분석)

  • Chung, Youngchul
    • Korean Journal of Optics and Photonics
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    • v.31 no.2
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    • pp.105-110
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    • 2020
  • A compact beam combiner based on two-mode interference (TMI) in multimode waveguides is proposed, and its feasibility is shown through simulation with the three-dimensional beam propagation method. The input waveguides are separated by about 1 ㎛ at the interface with the multimode waveguide, so that the fabricated waveguide pattern is well repeated. The power transmission to the output port from the red, green, and blue input port is 93.5%, 94%, and 93%, respectively. When the wavelength deviation from a center wavelength is 10 nm, the power transmission is maintained to be greater than 90%. When the waveguide width error is 40 nm, the power transmission is maintained to be greater than 85% for all the three colors. The polarization dependence of the beam combiner is almost negligible, and its size is as tiny as 0.02 × 4 ㎟.

Evaluation and Identification of Promising Bivoltine Double Hybrids of the Silkworm Bombyx mori L. for Tropics Through Large Scale In-House Testing

  • Dayananda, Dayananda;Kulkarni, Satish;Rao, Pala Rama Mohana;Gopinath, Obalaiah;Kumar, Sundara Murthy Nirmal
    • International Journal of Industrial Entomology and Biomaterials
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    • v.23 no.2
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    • pp.187-191
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    • 2011
  • An attempt was made to assess the potentiality of bivoltine double hybrids under simulated conditions of farmers to identify the suitable bivoltine double hybrid combination. Four bivoltine double hybrids developed at Central Sericultural Research and Training Institute (CSRTI), Mysore along with popular single hybrid, $CSR2{\times}CSR4$ as control was assessed for economic traits. The rearing results showed significant improvement of 20-24% in fecundity of the double hybrids studied over single hybrid. Among the double hybrids, $[D7{\times}S5]{\times}[D13{\times}S1]$ recorded significantly higher survival (89.58 %), cocoon yield (76.328 kg/ 50,000 eggs), cocoon price (Rs. 180.87/kg) and lower cocoon leaf ratio of 1: 21.80. The performance of the reeling traits were also found significantly superior in $[D7{\times}S5]{\times}[D13{\times}S1]$ with higher filament length (1100 m), reelability (88%), raw silk (18.55%) and neatness (92 points) compared to $CSR2{\times}CSR4$ and other double hybrids evaluated. Besides, the cocoons of $[D7{\times}S5]{\times}[D13{\times}S1]$ exhibit uniformity in size with a standard deviation of < 8. Overall data indicated the superiority of $[D7{\times}S5]{\times}[D13{\times}S1]$ compared to the other hybrids evaluated and it has profound influence in expressing the full potentiality in the field.

Computer Simulation for Developing the Plate and Corner Type In-Situ Thermal Resistance Measuring Device (평판 및 모서리형 현장열저항 측정기기 개발을 위한 Computer Simulation)

  • Kang, Byeong-Woong;Park, Seung-Ik;Yu, Seung-Sun;Park, Hyo-Soon
    • Solar Energy
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    • v.19 no.4
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    • pp.71-80
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    • 1999
  • For developing a new measuring device which enables the thermal resistance at comers of the building envelope in addition to the plate wall measuring device, computer simulations were performed to clarify the problems produced during previous tests. For the optimum design to reduce the temperature deviation in measuring device, the specifications of the measuring devices are to be as follows : Dimension of the device is $500{\times}500{\times}100mm$ in size, heating plate is seperated to some degree from the inner surface of the measuring device, lower temperature of heating plate is as effective as possible, fans should be located at the upper part in the measuring device and face to downward.

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An Improved Calibration Method for the COCOMO II Post-Architecture Model

  • Yoon, Myoung-Young
    • Journal of Korea Society of Industrial Information Systems
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    • v.5 no.2
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    • pp.47-55
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    • 2000
  • To date many software engineering cost models have been developed to predict cost, schedule, and effort of the software under development. The COCOMO Ⅱ is well- suited for the new software development life cycle such as non-sequential and rapid- development processes. The traditional regression approach based on the least square criterion is the most commonly used technique for empirical calibration in the COCOMO Ⅱ model. It has a few assumptions frequently violated by software engineering data sets. The source data is also generally imprecise in reporting size effort, and cost-driver ratings, particularly across different organizations. And that the outlier for the source data is a peculiarity and indicates a data point. To cope with difficulties, in this paper, we propose a new regression method for calibrating COCOMO Ⅱ post-architecture model based on the minimum relative error(MRE) criterion. The characteristic of the proposed method is insensitive to the extreme values of the data in the empirical calibration. As the experimental results, It is evident that our proposed calibration method MRE was shown to be superior to the traditional regression approach for model calibration, as illustrated by the values obtained for standard deviation(^σ), and prediction at level LPRED(L) measures.

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Simplified Noise Modeling of GPS Measurements for a Fast and Reliable Cycle Ambiguity Resolution

  • Park, Byung-Woon;Kee, Chang-Don
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • v.1
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    • pp.535-540
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    • 2006
  • The relationship between the observable noise model and the satellite elevation angle can be modeled quite well by an exponential function.[Jin, 1996] Noise size and dependence on the elevation angle are, however, different for each observation and receiver type. Therefore, the coefficient determination of this model is an issue, and various methods including PR-CP, single difference, and time difference have been suggested. The limitations of them are difficulty to model the carrier phase noise and to eliminate bias. To overcome these disadvantages for using Jin's model, we suggest zero baseline double difference (DD) and noise sorting algorithm. Data DD technique in zero baseline is useful to eliminate all the troublesome GPS biases, and the remaining error is the sum of GPS measurement noises from two satellites. These DD residuals for hours should be sorted by the combination of satellite elevation angles, and then variance value of the residual for each combination can be estimated. Using these values, we construct an over-determined linear equation whose solution is a set of noise variance for each satellite elevation angle. With 24hr Trimble 4000ssi data, we easily worked out the coefficients of the noise model not only for pseudorange but also for carrier phase. We estimated the standard deviation of the measurement DD using our model, and plotted 1 and 3 sigma lines for every epoch to verify the representation of the residual error. 63.3% of pseudorange residual and 65.9% of phase error did not exceed the 1 sigma lines. Additionally, 99.2% and 99.5% of them lied within 3sigma line. These figures prove that the Gaussian property of measurement noise, and that the suggested model by our algorithm corresponds to the observable noise information.

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Determination of Plutonium in HANARO Irradiated Fuel by IDMS (동위원소희석 질량분석법에 의한 조사 후 하나로 핵연료 중 Pu 정량)

  • Jeon, Young Shin;Son, Sae Chul;Kim, Jung Suk
    • Analytical Science and Technology
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    • v.16 no.3
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    • pp.191-197
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    • 2003
  • Two methods, IDMS (Isotope Dilution Mass Spectrometry) and controlled potential coulometry are compared by the determination of Pu for the NBL, CRM No.122, $PuO_2$. The recovery of Pu was found to be $1.002176{\pm}0.000452$ within the relative standard deviation of 0.045% (95% conf. level) although a small size of sample ($0.9{\mu}g$-Pu) was used in IDMS. The recovery using controlled potential coulometry were obtained in the range of 0.9923~0.9960. The analytical results of IDMS and controlled potential coulometry were good agreement within 0.6~1%. Base on these experiment results, The plutonium in HANARO irradiated fuel rod that separated portion of top, middle, and bottom were determined. The measured values of Pu are 1.155 mg, 2.483 mg and 1.920 mg in one gram of sample(fuel+clad), respectively.