• 한국세라믹학회지
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• 제36권7호
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• pp.767-772
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• 1999

The effect of B2O3 addition on the sintering behavior dielectric and ferroelectric properties of Ba0.7Sr0.3TiO3 ceramics were investigated. The sample with 0.5wt% B2O3 was sintered under 115$0^{\circ}C$. The dielectric and ferroelectric properties of BST with 0.5wt% B2O3 was as good as BST without B2O3 sintered at 135$0^{\circ}C$ and its dielectric loss was even better When B2O3 was added over 1.0wt% the overdoped B2O3 remained in the specimens and formed a second phase which degraded the sintering behaivor dielectric properties of BST.

• 한국분말재료학회지
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• 제19권2호
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• pp.105-109
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• 2012

Magnetic properties and the microstructures of magnets prepared by spark plasma sintering were investigated in order to enhance magnetic properties by grain size control. Nd-Fe-B magnets were fabricated by the spark plasma sintering under 30 MPa at various temperatures. The grain size was effectively controlled by the spark plasma sintering and it was possible to make Nd-Fe-B magnets with grain size of 5.9 ${\mu}m$.

• 한국분말재료학회지
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• 제9권4호
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• pp.218-226
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• 2002

The purpose of the present study is to investigate the influence of thermal debinding and sintering conditions on the sintering behavior and mechanical properties of PIMed 316L stainless steel. The water atomized powders were mixed with multi-component wax-base binder system, injection molded into flat tensile specimens. Binder was removed by solvent immersion method followed by thermal debinding, which was carried out in air and hydrogen atmospheres. Sintering was done in hydrogen for 1 hour at temperatures ranging from 1000℃ to 1350℃ The weight loss, residual carbon and oxygen contents were monitored at each stage of debinding and sintering processes. Tensile properties of the sintered specimen varied depending on the densification and the characteristics of the grain boundaries, which includes the pore morphology and residual oxides at the boundaries. The sinter density, tensile strength (UTS), and elongation to fracture of the optimized specimen were 95%, 540 MPa, and 53%, respectively.

• 한국세라믹학회지
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• 제33권7호
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• pp.779-784
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• 1996

The spinel/cubic stabilized zirconia composites were fabricated via, The reaction sintering of monoclinic zirco-nia(baddeleyite) added with MgAl powder. During heating Mg and Al were oxidizedfirst and subsequently the oxides formed spinel (MgAl2O4) and finally remained MgO stabilized the zirconia, Because the oxides formed during the oxidation process would have very fine grain size (order of submicron) mainly due to the effects of attrition milling the reaction sintering was more effective in densification and improvement of strength and fracture toughness than conventional sintering with direct addition of MgO. The sintering behavior phase transformation during firing and mechanical properties of sintered body were investigated with emphasis on the relations between spinel formation due to MgAl addition and sintering and mechanical properties.

• 한국전기전자재료학회논문지
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• 제18권6호
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• pp.543-549
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• 2005

The electrical and dielectric properties of $ZnO-Pr_6O_{11}-CoO-Cr_2O_3-based$ varistors were investigated in the sintering time range of $1\~3$ h. Increasing sintering time improved the densification of ceramics, whereas deteriorated the nonlinearity, in which the nonlinear exponent greatly decreased from 55.3 to 38.2 and the leakage current increased from 0.1 to $1.1\;{\mu}A$. The donor concentration and density of interface states increased in the range of $(1.06\~1.60)\times10^8/cm^3\;and\;(3.15\~3.67)\times10^{12}/cm^2$ with increasing sintering time, respectively. while, in dielectric properties, the increase of sintering time increased in the range of $0.0228\~0.0505$ in tans and $1.32\~1.36\;{\mu}s$ in relaxation time.

• 한국전기전자재료학회논문지
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• 제27권1호
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• pp.22-26
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• 2014

$(Ba_{0.85}Ca_{0.15})(Ti_{0.9}Zr_{0.1})O_3$ + 0.04 wt% $CeO_2$ lead-free ceramics were prepared by conventional oxide-mixed method and the effect of sintering temperature on microstructure, dielectric and piezoelectric properties were investigated. Improved piezoelectric properties have been observed at $1,400^{\circ}C$ sintering temperature which show the optimal electrical properties, $k_p{\sim}0.412$, $d_{33}{\sim}316pC/N$, $Q_m{\sim}144$, ${\varepsilon}_r{\sim}3,345$ and $T_c{\sim}85^{\circ}C$. These results show that the sintering temperature plays an important role in piezoelectric properties.

• 한국세라믹학회지
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• 제46권1호
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• pp.81-85
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• 2009

$B_4C$ ceramics were fabricated by a hot-press sintering method and their sintering behavior, microstructure and mechanical properties were evaluated. Relative density of $B_4C$ ceramics were obtained by a hot-press sintering method reached as high as 99% without any sintering additives. The mechanical properties of $B_4C$ ceramics was improved by a methanol washing process which can remove $B_2O_3$ phase from a $B_4C$ powder surface. This improvement results from the formation of homogeneous microstructure because the grain coarsening was suppressed by the elimination of $B_2O_3$ phase. Particularly, mechanical properties of the sintered specimen using a methanol washed powder improved compared with the specimen using an as-received commercial powder.

• 열처리공학회지
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• 제11권4호
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• pp.241-246
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• 1998

It is well known for 410L ferritic stainless steel powder to applicate a sensor ring in anti-lock brake system of automobile, several studies, because of its excellent magnetic properties. This study was carried out to investigate the magnetic properties such as the maximum magnetic induction, coercivity and maximum permeability of the materials with functions of sintering density, time and temperature, and concluded as follows: 1. Sintering under the circumstances of Ar gas and the temperature of $1250^{\circ}C$ for 60min, showed that nitrogen was increased, whereas carbon and oxygen decreased in quantities. 2. Both maximum magnetic induction value of 4700Gauss and permeability of 200 were obtained at the maximum sintering density of $6.89g/cm^2$. Here, the properties showed a linear increasement with increasing the sintering density. 3. Coercivity sharply decreased with incresing the sintering density and reached to 7.6Oe at the maximum sintering density of $6.89g/cm^2$.

• 한국전기전자재료학회논문지
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• 제18권3호
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• pp.237-242
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• 2005

In this paper, in order to develop the low temperature sintering ceramics for multilayer piezoelectric transformer, PMN-PZT ceramics were manufactured with the variations of sintering times, and their microstructural, piezoelectric and dielectric properties were investigated. Li$_2$CO$_3$ and Bi$_2$O$_3$ were used as sintering aids and the specimens were sintered during 30, 60, 90, 120, 150, and 180 minutes, respectively. At the specimen sintered during 90 minute, mechanical quality factor(Qm), electro-mechanical coupling factor(kp) and dielectric constant were showed the optimum values of 2,356, 0.504 and 1,266, respectively.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.621-622
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• 2006

In this paper, we show some experimental results of binder-free WC sintered by Pulsed Electric Current Sintering (PECS) also known as Field Assisted Sintering Technology (FAST). These binder-free WC have extremely hardness and stiffness. However, these mechanical properties are dependent on the sintering condition, e.g., maximum temperature, applied pressure, etc. We show some relationship between mechanical properties and sintering condition to improve to sinter the binder-free WC.