• 대한치과보철학회지
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• 제55권3호
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• pp.264-271
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• 2017

목적: 본 연구에서는 4종의 간접복합레진에 대하여 금합금과 Ni-Cr합금에 대한 결합강도의 차이와 각각의 합금에 표면형태를 다르게 하여 일정한 온도의 증류수에 보관 전과 후에 전단결합강도의 차이가 있는지 알아보고자 하였다. 재료 및 방법: 금속 시편을 주조 제작하였는데, 금합금과 Ni-Cr합금의 표면형태를 flatting, bead, loop로 하여 4종의 간접복합레진(Gradia, Tescera Sinfony and in;joy)당 60개씩 총 240개를 준비하였다. 이후 금속표면에 각각의 제조사에서 지시한대로 간접 복합레진을 접착하였다. 간접복합레진의 중합 24시간 후에 만능시험기를 이용하여 전용 지그에 금속시편을 부착 후, 전단결합강도를 측정하였다. 또한 증류수에 240시간 보관 후에 같은 방법으로 전단결합강도를 측정하였다. 결과: 금속의 표면 형태에 따른 전단결합강도 측정에서 4종의 레진 모두 bead군에서 높은 결합강도를 보였고 loop, flatting 순이었다 (P < .05). 수조에서 240시간 보관 후에는 Gradia가 모든 군에서 다른 레진 군에 비해 비슷하거나, 통계적으로 유의하게 높은 (P < .05) 전단결합강도를 나타내었다. 결론: 금속표면의 형태에 따라, 금속의 종류에 따라, 물속 보관 전후에 따라 금속과 간접복합레진의 결합력의 차이를 나타내었고 추가 실험을 통해 최적의 조합에 따른 임상에서의 적용가능성을 보여주었다.

• 구강회복응용과학지
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• 제22권2호
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• pp.125-136
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• 2006

Statement of problem. The success of the bonding between electroforming gold and resin is dependent on the surface-conditioning technique but its effective technique has net been studied widely. Purpose. The purpose of the study was to evaluate the bond strength between the electroforming gold and resin with varying the surface-conditioning technique. Materials and methods. Sixty rectangular shaped metal specimens were made and one side of each specimen were gold hard plated. The sand-blasted specimens were divided into four experimental groups with fifteen specimens in each group and were treated as follows. Group 1: Silicoating (Rocatec, 3M ESPE)+ Sinfony (3M ESPE), Group 2: SR Link+ SR Adoro (Ivoclar Vivadent), Group 3: Tin plating (Microtin, Danville Engineering)+ SR Link+ SR Adoro, Group 4: Tin plating (Micro tin, Danville Engineering)+ Silicoating (Rocatec)+ Sinfony. Shear bond strength at metal-resin interface were measured using universal testing machine. Energy Dispersive x-ray analysis was done and scanning electron microscope images were taken and observed. Results and Conclusion. The following conclusions were drawn. 1. The mean shear bond strength values in order were 11.69MPa (Group 2), 22.35MPa (Group 3), 22.40MPa (Group 1) and 27.71MPa (Group 4). There was no significant difference in Group 1, Group 3 and Group 4(P>0.05). 2. In the EDX line analysis, the Au was detected on the surface of all specimen. $SnO_2$ showed on the surface of Group 2 and $SiO_2$ was detected on the surface of Group 1. 3. Increasing of roughness by sandblasting(Group 2), formation of micro-irregularities and tin crystals by electrolytic tin plating(Group 3) and formation of surface irregularities and $SiO_2$ layer(Group 1,4) were observed in SEM photo. 4. Tin plating(Group 3) and Rocatec treatment(Group 1) showed clinically effective shear bond strength(>20MPa), but when the two surface conditioning method were used together higher bond strength were achieved.

• 대한치과기공학회지
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• 제35권4호
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• pp.333-341
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• 2013

Purpose: The purpose of this study was to evaluate the flexural strength of indirect composite resins with different polymerization conditions. Methods: Ten specimens ($2mm{\times}2mm{\times}25mm$) of each composite resins (Tescera (T), Gradia (S) and Sinfony (S)) were fabricated by two polymerization methods : manufacturers's and light heat pressure. Composite resins polymerized by manufacturers's method and light heat pressure served as control (TS, GS and SS) and experimental groups (TE, GE and SE), respectively. The composite resins were tested for flexural strength and the surface of composite resins were observed with scanning electron microscope (SEM) under X1,000 magnification. Results: The flexural strength values of cured composite resin decreased in the following order: TE (195.4MPa), TS (179.8MPa), GE (169.9MPa), SE (137.7MPa), SS (111.1MPa) and GS (100.9MPa) groups. Conclusion: The flexural strength values between the control and the experimental groups were not significantly different although experimental groups showed higher flexural strength values than control groups.

• 대한치과기공학회지
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• 제30권2호
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• pp.23-29
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• 2008

The purpose of this study is to evaluate possibility of using indirect composite resin instead of porcelain through the measurement of shear bond strength between zirconia core and indirect composite resin under treatment of $Rocatec^{TM}$ system for improving the adhesion of indirect composite resin. 20 cylindrical zirconia core specimens were divided into 2 groups, according to zirconia surface treatment and attached materials: 1) treated with sandblast and attached with indirect composite resin, 2) treated with sandblast + $Rocatec^{TM}$ system and attached with indirect composite resin. The shear bond strength of each experimental group was measured by MTS and the changes of zirconia core surface according to surface treatments were obtained by SEM observation and measurements of surface roughness. The mean shear bond strength values are $0.55\;{\pm}\;0.11MPa$(Group SC) and $1.16\;{\pm}\;0.46MPa$(Group SRC). The mean Ra values for the surface treatments were follows: $0.39\;{\pm}\;0.13$($100{\beta}_{{\mu}m}$ sandblast) and $0.50\;{\pm}\;0.03$($100{\beta}_{{\mu}m}$ sandblast + $Rocatec^{TM}$ system). In the analysis of EDS, Si element was detected in the Group SC. The shear bond strength between zirconia core and indirect composite resin was improved significantly by using $Rocatec^{TM}$ system.