• Title/Summary/Keyword: Simultaneous Analysis

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Optimization of Parameters for Simultaneous Multielemental Analysis by Atomic Absorption Spectrometry (원자흡수분광법에 의한 다원소 동시분석시 조건의 최적화)

  • Kim, Hyo Jin;Kang, Jong Seong
    • Analytical Science and Technology
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    • v.6 no.4
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    • pp.359-362
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    • 1993
  • To find compromise experimental conditions that will allow a group of elements to be run on flame atomic absorption spectrometer without changing the burner height or gas flow rates, measurements were carried out. The optimum absorbance for simultaneous analysis of ten elements was observed at high flow rate of air-$C_2H_2$ as fuel and at 2mm of burner height. At the condition, 73% of mean relative absorbance were achieved.

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Characterization and Studies of Compromised Experimental Conditions for the Simultaneous Multielemental Analysis by Flame Atomic Absorption Spectrometry (원자흡수법을 이용한 다원소 동시 분석 실험 조건에 관한 기초 특성 연구)

  • 최성규;이현주;박양순;김효진
    • YAKHAK HOEJI
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    • v.39 no.2
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    • pp.148-152
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    • 1995
  • For comparison between the compromised experimental condition and the best conditions for each element by flame atomic absorption spectrometer, the absorbances were measured with changing the burner height and HCL current. The optimum absorbance for simultaneous analysis of 6 elements was observed at 1 mA of HCL current and at 4 mm of burner height except Cr and Co. The stability of flame atomic absorption spectrometer on each element was found to be better than 5%. To investigated the accuracy of this instrument, POSCO RM-07 as a real sample was analysed at these compromised experimental conditions and found to be better than 0.04%.

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Double Circuit Simultaneous Fault Analysis (이중선로의 동시사고를 고려한 상정사고해석)

  • Kim, J.U.;Moon, Y.H.;Lee, J.G.
    • Proceedings of the KIEE Conference
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    • 2002.07a
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    • pp.136-138
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    • 2002
  • In this paper, we propose the analysis method of the Double Circuit Simultaneous Fault. To improve the accuracy and the promptness of the coontingency analysis, we reformed the Peterson method and extended the Sherman-Morrison equation. We also used the table of trigono -metric factor of Jacobian matrix before the fault, to compute the inverse matrix needed in the loadflow calculation.

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Quantitative Analysis by Derivative Spectrophotometry (III) -Simultaneous quantitation of vitamin B group and vitamin C in by multiple linear regression analysis-

  • Park, Man-Ki;Cho, Jung-Hwan
    • Archives of Pharmacal Research
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    • v.11 no.1
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    • pp.45-51
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    • 1988
  • The feature of resolution enhancement by derivative operation is linked to one of the multivariate analysis, which is multiple linear regression with two options, all possible and stepwise regression. Examined samples were synthetic mixtures of 5 vitamins, thiamine mononitrate, riboflavin phosphate, nicotinamide, pyridoxine hydrochloride and ascorbic acid. All components in mixture were quantified with reasonably good accuracy and precision. Whole data processing procedure was accomplished on-line by the development of three computer programs written in APPLESOFT BASIC language.

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POSTOPERATIVE STABILITY OF FIXATION WITH ABSORBABLES IN SIMULTANEOUS MAXILLOMANDIBULAR ORTHOGNATHIC SURGERY (상하악 동시 악교정수술에서 흡수성 고정판을 이용한 골편고정시 술후 안정성에 대한 연구)

  • Park, Jung-Min;Park, Young-Wook
    • Maxillofacial Plastic and Reconstructive Surgery
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    • v.32 no.2
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    • pp.126-131
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    • 2010
  • Objectives: This study is aimed to determine any differences in the postoperative stability between absorbable and titanium plate systems for fixation in orthognathic surgery with simultaneous maxillomandibular procedures especially including maxillary posterior impaction and advancement. Study Design: Forty patients with dentofacial deformities were randomly assigned into titanium (4 males and 6 females) and absorbable (17 males and 13 females) fixation group. All patients had undergone surgical alterations of maxilla with posterior impaction and advancement. A comparison study of the change in the maxillary position after the simultaneous surgery was performed with 1-day, 6-months postoperative lateral cephalograms compared to preoperative lateral cephalogram by tracing. Wilcoxon rank sum test was used for statistical analysis. Result: The position of the maxilla was stable after surgery and was not changed significantly from 1 day to 6 month after the simultaneous maxillomandibular surgery both in the experimental (absorbable plates) and control (titanium plates). Conclusion: This study suggests that application of absorable plating system in the fixation of maxillary segment in the simultaneous maxillomandibular procedures, leads to a predictable short-term postoperative skeletal stability comparable to the titanium plating system. Long term follow-up and further studies will be needed.

Slope Stability Analysis Considering Multi Failure Mode (다중파괴모드를 고려한 사면안정해석)

  • Kim, Hyun-Ki;Kim, Soo-Sam
    • Journal of the Korean Society for Railway
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    • v.14 no.1
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    • pp.24-30
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    • 2011
  • Conventional slope stability analysis is focused on calculating minimum factor of safety or maximum probability of failure. To minimize inherent uncertainty of soil properties and analytical model and to reflect various analytical models and its failure shape in slope stability analysis, slope stability analysis method considering simultaneous failure probability for multi failure mode was proposed. Linear programming recently introduced in system reliability analysis was used for calculation of simultaneous failure probability. System reliability analysis for various analytical models could be executed by this method. For application analysis for embankment, the results of this method shows that system stability of embankment calculate quantitatively.

Long-term Statistical Analysis of the Simultaneity of Forbush Decrease Events at Middle Latitudes

  • Lee, Seongsuk;Oh, Suyeon;Yi, Yu;Evenson, Paul;Jee, Geonhwa;Choi, Hwajin
    • Journal of Astronomy and Space Sciences
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    • v.32 no.1
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    • pp.33-38
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    • 2015
  • Forbush Decreases (FD) are transient, sudden reductions of cosmic ray (CR) intensity lasting a few days, to a week. Such events are observed globally using ground neutron monitors (NMs). Most studies of FD events indicate that an FD event is observed simultaneously at NM stations located all over the Earth. However, using statistical analysis, previous researchers verified that while FD events could occur simultaneously, in some cases, FD events could occur non-simultaneously. Previous studies confirmed the statistical reality of non-simultaneous FD events and the mechanism by which they occur, using data from high-latitude and middle-latitude NM stations. In this study, we used long-term data (1971-2006) from middle-latitude NM stations (Irkutsk, Climax, and Jungfraujoch) to enhance statistical reliability. According to the results from this analysis, the variation of cosmic ray intensity during the main phase, is larger (statistically significant) for simultaneous FD events, than for non-simultaneous ones. Moreover, the distribution of main-phase-onset time shows differences that are statistically significant. While the onset times for the simultaneous FDs are distributed evenly over 24-hour intervals (day and night), those of non-simultaneous FDs are mostly distributed over 12-hour intervals, in daytime. Thus, the existence of the two kinds of FD events, according to differences in their statistical properties, were verified based on data from middle-latitude NM stations.

Simultaneous Surveys of 22 GHz Water and 44 / 95 GHz Class I Methanol Masers toward High-Mass Protostellar Objects

  • Kim, Chang-Hee;Kim, Kee-Tae;Park, Young-Sun
    • The Bulletin of The Korean Astronomical Society
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    • v.39 no.2
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    • pp.80.1-80.1
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    • 2014
  • We made simultaneous surveys of 22 GHz water and 44 / 95 GHz methanol masers toward 299 high-mass protostellar objects using the Korea VLBI Network (KVN) 21-m telescope. The sources were selected from the catalog of Red MSX Source (RMS) survey. Initial selection of the sample present high-mass protostellar objects in an evolutionary phase prior to ultra-compact HII regions, which have bolometric luminosities > $10^3L_{\odot}$ but are not associated with any radio continuum emission. After the follow-up work of ongoing RMS survey, final samples contains 56 sources classified as HII regions. We performed a simultaneous survey of 22 GHz water and 44 GHz methanol masers in 2011 and then conducted a simultaneous survey of 22 GHz water and 44 / 95 GHz methanol masers in 2012. The primary scientific goals of these surveys are to investigate the relationship among the three masers and to explore the relationship between each maser and the central star or the parental dense core. The detection rates of two epochs are 42% and 38% for water, 25% and 26% for 44 GHz methanol, and 23% (2012 only) for 95 GHz methanol masers. We performed a statistical analysis on subsample associated with a large data found in literature. In this poster, we will the preliminary data analysis results and discuss the implications.

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Analytical Quality by Design Methodology Approach for Simultaneous Quantitation of Paeoniflorin and Decursin in Herbal Medicine by RP-HPLC Analysis

  • Kim, Min Kyoung;Park, Geonha;Hong, Seon-Pyo;Jang, Young Pyo
    • Natural Product Sciences
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    • v.27 no.4
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    • pp.264-273
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    • 2021
  • Simultaneous quantification of multiple marker compounds in herbal medicine by high performance liquid chromatography (HPLC) analysis is still a challenge due to the complexity in various parameters to be considered and co-existing multi-components. As a case study, a reliable HPLC method for simultaneous quantification of paeoniflorin from Paeoniae Radix and decursin from Angelicae Gigantis Radix in various commercial herbal medicine was developed based on analytical quality by design (AQbD) strategy. As a first step, risk assessment was performed to select the critical method parameters (CMPs) which were decided as organic mobile phase ratio and column oven temperature. In order to evaluate the effect of the CMPs on critical method attributes (CMAs) of peak resolution and tailing, central composite design (CCD) was employed. The final chromatographic conditions were optimized as follows: column- C18, 4.6 × 250 mm, 5 ㎛ particle size; mobile phase- A: acetonitrile, B: 0.1% acetic acid water; detection wavelength- 235 nm for paeoniflorin, 325 nm for decursin; column oven temperature- 25℃; flow rate- 1.0 mL/min; gradient mobile phase system as Time (min) : % A, 0:14, 25:14, 30:50, 60:50, 61:100, 65:100, 66:14, 75:14. The method was successfully validated according to the International Conference on Harmonization (ICH) guidelines and piloted for ten commercial herbal medicines.