• Title/Summary/Keyword: Shape of Lattice

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Fabrication of High-Density Nickel Hydroxide Powder-I (고밀도 수산화니켈 분말의 제조에 관한 연구-I)

  • 신동엽;조원일;신치범;조병원;강탁;윤경석
    • Journal of the Korean institute of surface engineering
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    • v.28 no.2
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    • pp.92-100
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    • 1995
  • To increase the capacity of positive electrode materials for matching the high capacity negative electrode materials in alkaline rechargeable batteries, high-density nickel hydroxide powders were made through a continuous process from nickel sulfate reacted with ammonia and sodium hydroxidc. The effect of operating conditions on structure, shape, size distribution, apparent density and tap density of powders were investigated. Crystal structure of nickel hydroxide powder was hcp according to Bravais Lattice. The increase of mean residence time promoted the growth of (101) plane. The shape of powder was nearly spherical. Their size was in the range of $2~50\mu\textrm{m}$. The size distribution of the powders prepared was narrower than that of commercially obtained nickel hydroxide. Apparent density and tap density were 1.6~1.7g/cc and 2.0~2.1g/cc, respectively.

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The Jeogori Included in The Buddist Statue in 1748 (1748년 불복장 저고리 소고)

  • 김선경;조효숙
    • Journal of the Korea Fashion and Costume Design Association
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    • v.5 no.2
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    • pp.65-74
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    • 2003
  • The Purpose of this study is to investigate the jeogori included in the buddist statue in 1748. The jeogori was similar in shape to excavated costume of Andong Kwon, Papyung Yoon, and Chungyeongunju in 18th century. This jeogori was useful to estimate the interesting process of shape change of jeogori in 18th century. Four different silk fabrics were used in the jeogori. Outer fabrics were satin weave with floral, lattice strip, dragon, and cloud patterns. The ground area was 5-harness warp faced satin and the patterned area was 5-harness filling faced satin. An inner fabric was simple plain weave. Warp and filling yarns of all fabrics in this jeogori had no twist.

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Structural Analysis of Zn-Ni electrodeposition (Zn-Ni 도금강판의 도금층 구조 분석)

  • Lee, D.H.;Park, S.H.
    • Analytical Science and Technology
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    • v.12 no.1
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    • pp.40-46
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    • 1999
  • Zn-Ni alloy electrodeposition on steel has been examined by means of X-ray diffraction and scanning electron microscopy. The effect of current density, $Ni^{2+}$ ion concentration, and $Cl^-$ ion concentration on the structure as well as morphology of the electrodeposit have been studied. The Ni content of the electrodeposit increased with decreasing current density in the range studied in this work. The Ni content of the electrodeposit also increased with increasing $Ni^{2+}$ ion and $Cl^-$ ion concentrations. The structure change of the electrodeposit was closely related to the Ni content. In fact, the mixture phase of ${\eta}$ and ${\gamma}$ was found below 10 wt.% of Ni while the ${\gamma}$ phase only was observed above 10 wt.% of Ni. In addition, the lattice parameter, a, of then phase structure increased and the lattice parameter, c, of it decreased as the Ni content of the electrodeposit increased. The morphology of the electrodeposit varied from the plate-like shape to the fine granular shape depending upon the change in composition and structure of the electrodeposit.

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X-ray Photoelectron Spectroscopy Study of LaFeO3 Powders Synthesized by Solution Combustion (용액연소법으로 제조한 LaFeO3의 XPS 특성)

  • Hwang, Yeon;Kang, Dae-Sik;Park, Mi-Hye;Cho, Sung-Baek
    • Korean Journal of Materials Research
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    • v.18 no.6
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    • pp.313-317
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    • 2008
  • [ $LaFeO_3$ ] powders were synthesized using a method involving solution combustion, and the surface properties of these powders were examined by x-ray photoelectron spectroscopy. As the amount of fuel increased during the synthesis, the $LaFeO_3$ powders became amorphous with a large plate-like shape. It was found that the O 1s spectra were composed of two types of photoelectrons by deconvolutioning the spectra. Photoelectrons with higher binding energy come from adsorbed oxygen ($O^-$) whereas those with lower energy come from lattice oxygen ($O^{2-}$). The ratio of adsorbed and lattice oxygen increased as the ratio of the fuel and nitrate (${\Phi}$) increased. The binding energy of both types of oxygen increased as ${\Phi}$ increased due to the formation of carbonates.

Compensation of Relation Formula between Luffing Wire Tension and Overturning Moment in a Crawler Crane Considering the Deflection of Boom (크롤러 크레인에서 붐의 처짐을 고려한 러핑와이어 장력과 전도모멘트 사이의 관계식 보정)

  • Jang, Hyo-Pil;Han, Dong-Seop
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.10 no.4
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    • pp.44-49
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    • 2011
  • The crawler crane, which consists of a lattice boom, a driving system, and movable vehicle, is widely used in a construction site. It needs to be installed an overload limiter to prevent the overturning accident and the fracture of structure. This research is undertaken to provide the relation formula for designing the overload limiter as follows: First the relation formulas between the wire-rope tension and the hoisting load or the overturning ratio according to the luffing angle and length of a lattice boom are established. Secondly the derived formulas are corrected by using the compensated angle considering the deflection of boom through the finite element analysis. The stiffness analysis is carried out for 30-kinds of models as a combination of 6-kinds of luffing angle and 5-kinds of length of boom. Finally the shape design of a stick type load cell, which is the device to measure the wire-rope tension, is performed. 5-kinds of notch radius and 5-kinds of center hole radius are adopted as the design parameter for the strength analysis of the load cell.

Oscillatory Josephson-Vortex Resistance in Stacks of $Bi_{2}Sr_{2}CaCu_{2}O_{8+x}$ Intrinsic Josephson Junctions

  • Choi Jae-Hyun;Bae Myung-Ho;Lee Hu-Jong;Kim Sang-Jae
    • Progress in Superconductivity
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    • v.7 no.1
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    • pp.17-21
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    • 2005
  • We report the oscillation of the Josephson vortex-flow resistance in the rectangular stacks of $Bi_{2}Sr_{2}CaCu_{2}O_{8+x}$(Bi-2212) intrinsic Josephson junctions (IJJs). Apiece of Bi-2212 single crystal containing a few tens of IJJs was sandwiched between two gold electrodes and fabricated into a rectangular shape with the typical lateral size of about $1.5{\times}10\;{\mu}m^2$, using e-beam lithography and focused ion-beam etching techniques. In a tesla-range magnetic field applied in parallel with the junction planes, the oscillation of the Josephson vortex flow resistance was observed at temperatures near 60 K. The oscillation results from the interplay between the triangular Josephson vortex lattice and the potential barrier at the boundary of a single crystal. The oscillatory magnetoresistance for different bias currents, external magnetic fields, and the tilt-angles provides useful information on the dynamics of the coupled Josephson-vortex lattice system.

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Syntheses and Properties of the High-Tc Superconductive Bi_{2-x}Mo_xSr_2Ca_2Cu_3O_y$ System

  • Keu Hong Kim;Jong Tae Lim;Seung Koo Cho;Byoung Chan Kwak;Don Kim;Jae Shi Choi
    • Bulletin of the Korean Chemical Society
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    • v.11 no.1
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    • pp.25-28
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    • 1990
  • The superconducting properties have been studied for high-Tc superconductors of the $Bi_{2-x}Mo_xSr_2Ca_2Cu_3O_y$ system (x = 0.03-0.30). The crystal structure is pseudo tetragonal with the average lattice parameters a = 5.38 ${\AA}$, b = 5.44 ${\AA}$ and c = 30.6 ${\AA}$. All samples exhibit superconductivity with Tc offset at 79 K and Tc onset at 90-115 K. The Tc onset point decreases with increasing x, but the Tc offset points are nearly the same for all samples. Scanning electron micrographs show a special growth behavior of the grains with a plate shape. It is suggested that the decrease in Tc onset points with substitution of Mo for Bi is due to the decrease in lattice parameters and to the p-orbital of Mo. It is concluded that Mo does not play a crucial role in the superconducting transition of the $Bi_2Sr_2Ca_2Cu_3O_y$ system.

The formation mechanism of grown-in defects in CZ silicon crystals based on thermal gradients measured by thermocouples near growth interfaces

  • Abe, Takao
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.4
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    • pp.402-416
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    • 1999
  • The thermal distributions near the growth interface of 150nm CZ crystals were measured by three thermocouples installed at the center, middle (half radius) and edge (10nm from surface) of the crystals. The results show that larger growth rates produced smaller thermal gradients. This contradicts the widely used heat flux balance equation. Using this fact, it is confirmed in CZ crystals that the type of point defects created is determined by the value of the thermal gradient(G) near the interface during growth, as already reported for FZ crystals. Although depending on the growth systems the effective length of the thermal gradient for defect generation are varied, we defined the effective length as 10n,\m from th interface in this experiment. If the G is roughly smaller than 20C/cm, vacancy rich CZ crystals are produced. If G is larger than 25C/cm, the species of point defects changes dramatically from vacancies to interstitials. The experimental results after detaching FZ and CZ crystals from the melt show that growth interfaces are filled with vacancies. We propose that large G produces shrunk lattice spacing and in order to relax such lattice excess interstitials are necessary. Such interstitials recombine with vacancies which were generated at the growth interface, nest occupy interstitial sites and residuals aggregate themselves to make stacking faults and dislocation loops during cooling. The shape of the growth interface is also determined by te distributions of G across the interface. That is, the small G and the large G in the center induce concave and convex interfaces to the melts, respectively.

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Three Dimensional Last Data Generation System Utilizing Cross Sectional Free Form Deformation (단면 분할 FFD를 이용한 3D 라스트 데이터 생성시스템 개발)

  • Kim, Si-Kyung;Park, In-Duck
    • Journal of Institute of Control, Robotics and Systems
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    • v.11 no.9
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    • pp.768-773
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    • 2005
  • A new approach for human foot modelling and last design based on the cross sectional method is presented in this paper. The proposed last design method utilizes the dynamic trimmed parametric patches for the foot 3D data and last 3D data. The cross section a surface of 3D foot for the 3D last, design modeling of free form geometric last shapes. The proposed last design scheme wraps the 3D last data surrounding the measured 3D foot data with the effect of deforming the last design rule The last design rule of the FFD is constructed on the FFD lattice based on foot-last shape analysis. In addition, the control points of FFD lattice are constructed with cross sectional data interpolation methods from the a finite set of 3D foot data. The deformed 3D last result obtained from the proposed FFD is saved as a 3D dxf foot data. The experimental results demonstrate that the last designed with the proposed scheme has good performance.

Optimum Design of a Composite T-tail Configuration for Maximum Flutter Speed Using Genetic Algorithm (유전자 알고리즘을 이용한 T-형 복합재료 날개의 플러터 속도 최적설계)

  • Alexander, Boby;Oh, Se-Won;Kim, Dong-Hyun
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.11a
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    • pp.173-178
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    • 2005
  • In this paper, an efficient and robust analysis system for the flutter optimization of laminated composite wings has been developed using the coupled computational method based on the genetic algorithm. General three-dimensional doublet-lattice method is efficiently used to compute generalized aerodynamic forces of T-tail configuration in the frequency domain. Structural dynamic analyses of laminated composite T-tail models are conducted using finite clement method. The classical P-k flutter analysis technique is applied to effectively solve the aeroelastic governing equations in the frequency domain. Optimum design studies using genetic algorithm have been conducted in order to obtain maximum flutter stability of a composite T-tail configuration. The results show that flutter stability can be significantly increased using composite materials with proper optimum design concepts even for the same weight and shape condition. In the view point of engineering design, it is also importantly shown that the optimization of the vertical wing part is highly effective comparing to the optimization of horizontal wing part.

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