• Title/Summary/Keyword: Shape Treatment

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Preparation of Green-Light Emitting BAM:Mn Phosphor Particles by High Temperature Spray Pyrolysis (고온 분무열분해 공정에 의한 녹색 발광의 BAM:Mn 형광체 합성)

  • Ju Seo Hee;Koo Hye Young;Kim Do Youp;Kang Yun Chan
    • Korean Journal of Materials Research
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    • v.15 no.8
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    • pp.496-502
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    • 2005
  • Green-light emitting $BaMgAl_{10}O_{19}:Mn^{2+}$ (BAM:Mn) phosphor particles were prepared by spray Pyrolysis. The effect of reactor temperature and flow rate of carrier gas in the spray Pyrolysis on the morphology, crystallinity and photoluminescence characteristics under vacuum ultraviolet were investigated. The morphology of the as-Prepared Particles obtained by spray Pyrolysis had spherical shape and non-aggregation characteristics regardless of the reactor temperature. The spherical shape of the as-prepared Particles obtained by spray pyrolysis at low temperature disappeared after Post-treatment. On the other hand the as-Prepared Particles obtained by spray Pyrolysis at $1600^{\circ}C$ maintained spherical shape and non-aggregation characteristics after post-treatment at $1400^{\circ}C$ for 3 h under reducing atmosphere. The BAM:Mn Phosphor Particles Prepared by spray Pyrolysis at different reactor temperatures had pure crystal structure and high photoluminescence intensities under vacuum ultraviolet after post-treatment. BAM:Mn phosphor particles prepared by spray Pyrolysis at low How rate of carrier gas had complete spherical shape and filed morphology and high photoluminescence intensity after post-treatment under reducing atmosphere.

The Effect of Heat Treatment on the Tensile Properties of TiNi/6061Al Composites (TiNi/6061Al 복합재료의 인장특성에 미치는 열처리의 영향)

  • Park, Sung-Ki;Shin, Soon-Gi;Lee, Jun-Hee
    • Korean Journal of Materials Research
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    • v.13 no.1
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    • pp.64-68
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    • 2003
  • The 1.6 vol% and 2.5 vol% TiNi/6061Al composites were fabricated by permanent mold casting for investigating the effect of heat treatment on tensile strength for composites. The tensile strength without T6 treatment at 293 K was increased with increasing the volume fraction of TiNi fiber and at 363 K the higher the pre-strain, the higher the tensile strength. The tensile strength of the composite with $T_{6}$ treatment at 293 K was found to increase with increasing both the amount of pre-strain and the volume fraction of TiNi fiber and was higher than that without $T_{6}$ treatment. It should be noted that the tensile strength 2.5vol%TiNi/6061Al composites rolled at a 38% reduction ratio was the maximum value of 298 MPa. The tensile strength of composites decreased with increasing the reduction ratio over 38% because of the rupture of TiNi fiber.

A Study on the Infrared Local Heat Treatment of Curved Line for Aluminum Alloy Sheet (알루미늄 판재의 성형성 향상을 위한 적외선 국부 열처리법의 곡선형태 적용에 관한 연구)

  • Lee, E.H.;Yang, D.Y.
    • Transactions of Materials Processing
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    • v.27 no.2
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    • pp.87-92
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    • 2018
  • Auto industries have tried to employ lightweight alloys to improve the fuel efficiency of manufactured vehicles, as the environmental concern becomes an important issue. Even though the aluminum alloy is one of the most appropriate lightweight alloys for auto parts, the low formability of an aluminum alloy has been an obstacle to its application. In order to resolve the low formability problem, a recent study (Lee et al., 2017 [1]) showed that the infrared (IR) local heat treatment can improve the formability with a reduction of heating energy. However, the aforementioned study was limited to only a linear line heating. Since many of the available auto parts as applicable to vehicle manufacturing have a curved line shape, the heating experiments for a curved line should be studied. The possibility of building IR lamps having complex shapes is an advantage of the IR lamp, since it can control the heating shape. This work conducted the IR local heat treatment for the curved line. The experimental results show that the IR local heat treatment can improve the formability of the aluminum alloy for curved line. Additionally, it is shown that the IR local heat treatment also reduces the heating energy when it is compared with the furnace heating which heats a blank as a whole. A numerical simulation with a stress-based forming limit diagram also supports the experimental results.

Fabrication and Interface Properties of TiNi/6061Al Composite (TiNi 형상기억합금을 이용한 복합재료의 제조 및 계면 특성)

  • Kim, Sun-Guk;Lee, Jun-Hui
    • Korean Journal of Materials Research
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    • v.9 no.4
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    • pp.419-427
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    • 1999
  • TiNi shape memory alloy was shape memory heat-treated and investigated its mechanical properties with the variation of prestrain. Also 6061 Al matrix composites with TiNi shape memory alloy fiber as reinforcement have been fabricated by Permanent Mold Casting to investigate the microstructures and interface properties. Yield stress of TiNi wire was the most high in the case of before heat-treatment and then decreased as increasing heat-treatment time. In each heat-treatment condition, the yield stress of TiNi wire was not changed with increasing the amount of prestrain. The interface bonding of TiNi/6061Al composite was fine. There was a 2$\mu\textrm{m}$ thickness of diffusion reaction layer at the interface. We could find out that this diffusion reaction layer was made by the mutual diffusion. The diffusion rate from Al base to TiNi wire was faster than that of reverse diffusion and the amount of the diffusion was also a little more than that of reverse.

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Characterization of Shape Memory Alloy Springs by Beat Treatment Condition (열처리 조건에 따른 형상기억합금 스프링의 특성변화)

  • Kim, Myung-Soon;Na, Seung-Woo;Lee, Sang-Hoon;Lee, Seung-Ki
    • Proceedings of the KIEE Conference
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    • 1996.07c
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    • pp.1985-1987
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    • 1996
  • Shape memory alloy springs have been fabricated and annealed at $400^{\circ}C$, $450^{\circ}C$ and $500^{\circ}C$ in atmosphere and in nitrogen gas. The optimal heat treatment condition in view of maximum generated force has been decided by the iso-thermal test with variation of annealing condition. Experimental results show that the heat treatment with high temperature in nitrogen gas is desirable for high generated force and can be used for the design of shape memory alloy springs.

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The Shape Design of Shot Ball to Improve the Reliability of Surface Treatment (표면가공의 신뢰성향상을 위한 쇼트볼의 형상설계)

  • 이승호
    • Journal of the Korean institute of surface engineering
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    • v.35 no.6
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    • pp.357-362
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    • 2002
  • In this study, to improve the effect of the surface treatment, the shape design of shot ball is proposed. The fatigue effects of shot peening by the cut wire shot ball and the rounded cut wire shot ball are compared. The rotary bending and tensile fatigue tests are conducted on a spring steel to evaluate fatigue lives. The residual compressive stresses by the rounded cut wire shot ball is higher than by the rounded cut wire shot ball. This consequently increase the fatigue life and the reliability of surface treatment. Thus, to obtain optimum, repeatable and reliable shot peening effect the shape of the shot ball must be round.

Helical coil springs property in Cu-Zn-Al shape memory alloy (Cu-Zn-Al 형상기억합금의 코일스프링 특성)

  • Kwon, Hee-Kyung;Choi, Chang-Soo;Chung, In-Sang
    • Journal of the Korean Society for Heat Treatment
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    • v.9 no.3
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    • pp.187-197
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    • 1996
  • In this study, the properties of coil spring made by Cu-Zn-Al and B added shape memory alloys are investigated. The measurement of recovery displacement and energy with increasing weight, and thermocycling properties have been studied using displacement measuring device. Transformation temperature and phase change by thermocycling have been also investigated by DSC and X-ray diffractometer. Grain size of the alloy is refined from 1.2mm to $400{\mu}m$ by 0.06wt% of B addition. The maximum recovery energy of the coil spring for B added alloy is larger than that of no B added alloy, it is because of grain refinement. And shape memory ability of the coil spring by thermocycling decrease with increasing thermocycling after thermocycle under load. The degradation of shape memory properties of coil spring by thermocycling is improved by B addition.

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Shape Control of Automotive Flexible Plate in Press Quenching (프레스 퀜칭 공정에 의한 자동차 Flexible Plate의 형상 제어 연구)

  • Park, I.H.;Jeong, W.C.
    • Journal of the Korean Society for Heat Treatment
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    • v.21 no.4
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    • pp.189-198
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    • 2008
  • The production of automotive chassis parts requiring both high hardness and good shape-holdability is better realized by using press quenching technology, comprising the austenitizaton and the subsequent press quenching in a specially designed stamping tool. The effect of press quenching mold shape on the hardness distribution, bending height, and degree of planeness of automotive flexible plate during press quenching and tempering has been investigated. The preferable shape of the projections of punch and die in contact with the flexible plate was close to oval to improve the flow of cooling oil, leading to the higher hardness. The press quenching mold with three separate parts was more effective to control the dimensional change due to thermal deformation during press quenching. Some decrease in the bending height during tempering may be related to some recovery of the residual stress at $400^{\circ}C$.

Effect of Composition in Cu-Al-Mn Shape Memory Alloys on the Shape Memory Properties and Cold Workability (Cu-Al-Mn계 형상기억합금에서 조성이 형상기억특성 및 냉간가공성에 미치는 영향)

  • Park, Jong Bae;Park, Hyun Gyoon
    • Journal of the Korean Society for Heat Treatment
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    • v.27 no.2
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    • pp.59-64
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    • 2014
  • Cu-Al-Mn shape memory alloys of a variety of composition were characterized in terms of shape memory properties and cold workability. Cold workability tested by cold rolling indicated that the alloys solution treated in the ${\alpha}+{\beta}$ region have a higher ductility than those solution treated in the ${\beta}$ region. Also it is known that cold workability increased with the decrease in Al content in the ${\beta}$ region. This seems to be resulted from the fact that Mn addition causes to expand ${\beta}$ region toward lower Al content and lower order-disorder transition temperature, consequently, ${\beta}$ of excellent workability being frozen even at room temperature. Experimental results regarding shape memory showed that the properties were better with a higher Al contents at a given Mn content, which is closely related with martensitic transformation. It is also shown that super elasticity limit was enhanced with decrease in the yield strength of alloys because a lower yield strength seems to initiates slip at the lower applied stress.

Transformation Behavior on Heat Treatment Condition in Grain-Refined Cu-Zn-Al Shape Memory Alloy (결정립 미세화된 Cu-Zn-Al 형상기억합금의 열처리 조건에 따른 변태거동)

  • Kang, J.W.;Jang, W.Y.;Yang, G.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.4
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    • pp.34-43
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    • 1991
  • A small amount of misch metal and/or Zr was added as a dopant to 70.5wt----Cu-26wt----Zn-3.5wt----Al shape memory alloy in order to study the effect of grain refinement and heat treatments on the transformation behavior, stabilization of martensite, and shape memory ability. It was found that the addition of misch metal and Zr was very effective for reducing the grain size. The fracture mode has been changed from intergranular brittle fracture to ductile fracture with void formation and coalescence by the addition of misch metal and Zr. Aging of the ${\beta}$-phase decreases the $M_s$ temperature, but that of the martensite phase increases the $A_s$ temperature. The hysteresis of transformation temperature ${\Delta}T(A_s-M_s)$ has an increasing tendancy by grain refinement. The crystal structure of martensite was identified as monoclinic structure. As the grain size decreased, martensite stabilization more easily occured and the shape, memory ability has been reduced by the grain size refined.

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