• Title/Summary/Keyword: Separation condition

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Development of a miniaturized FM transmitter with low power

  • Ryu, Jeong-Tak;Kim, In-Gyeong;Kim, Yeon-Bo;Kim, Jong-Pil
    • Proceedings of the Korea Society for Industrial Systems Conference
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    • 2008.10b
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    • pp.629-633
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    • 2008
  • Recently, there has been great interest in the application of short-range wireless communication system. In this paper, the miniaturized FM transmitter with low power is developed, and laboratory tests have been carried out. The FM transmitter uses FM radio waves to send sound from any system (MP3, PMP, PDA, MP3 Phone et.) to any nearby radio or stereo system. The transmitter is designed with $2.6cm{\times}2.6cm{\times}2.6cm$ system size. The operating voltage is 3.7 V and used the built-in storage battery. The system can use continuously during 7 hour with once charging. The transmission frequency can select one of 88.1 MHz, 88.3 MHz, or 88.5 MHz in compliance with utility condition. The channel separation ability is 40 dB. The operating temperature is $-10{\sim}+85^{\circ}C$, which use in the industry environment. Consequently, this system sis used conveniently with short distance information transmitter system at the industry field.

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Reversed-Phase Ion-Interaction Chromatography of Aromatic Sulfonic and Carboxylic Acids (방향족 슬폰산 및 카르복시산의 역상 이온-상호작용 크로마토그래피)

  • Kang Sam-Woo;Oh Hae-Beom;Lee Seung-Seok
    • Journal of the Korean Chemical Society
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    • v.32 no.2
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    • pp.113-121
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    • 1988
  • The retention mechanism and separation of various aromatic sulfonic and carboxylic acids on reversed-phase liquid chromatographic column were studied in the mobile phase containing dodecyltrimethylammonium bromide (DTAB). The retention mechanism was found to be followed the ion-interaction model where the DTAB occupies a primary layer at the stationary phase while the sample anions and other co-anions in the system compete for forming the secondary layer. The capacity factors of samples were influenced by the several factors such as pH, concentration of various organic solvents, co-anions in the mobile phase and functional groups in sample molecules. Some mixtures of organic samples were attempted to separate under optimum condition.

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A New Method on the Measurement of Catalase Activity of Panax ginseng C.A. Meyer Tissues (인삼조직에서 Catalase Activity측정에 관한 새로운 Method)

  • Yang, Deok-Cho;Chae, Quae;Yoon, Jae-Jun;Lee, Sung-Jong;Lee, Ae-Ra
    • Journal of Ginseng Research
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    • v.9 no.2
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    • pp.154-162
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    • 1985
  • We report a newassay method on the measurement of the catalase activity, whose utilzation value is considered to be remarkable in the field of plant biochemistry. We named this method as a De-Coupling method. The essence of de-coupling method is the separation between the enzyme reaction and the indicator reaction. The optimum condition of the enzyme reaction was found to be following: on addition of 1 ml of substrate (H2O2: 20mM) to the fixture of the crude extract of enzyme (volume: 0.2 ml) and the ammonium phosphate buffer (volume: 1.8 ml; 0.93 M phosphate, 1.6M NHB, 2.5 M methanol, pH 7.0). After 30, 60 and 90 seconds of the enzyme reactions are proceeded, the reactions are terminated by 25% of tai-chloro-acetate (final concentration of 5%), respectively. The precipitated materials by tai-chloro-acetate was removed by the centrifugation (2000g, 10minutes). Formaldehyde produced in the enzymatic reaction was reacted with 2ml of acetylacetone (60mM). The indicator reaction -(HANTSCH REAKT10N)- in which lutidine is formed, was proceeded for 60 minutes at $25^{\circ}C$.

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The Extraction of Palladium by Polyurethane Foam impregnated with ${\beta}$-Diphenylglyoxime (${\beta}$-디페닐글리옥심으로 침윤시킨 폴리우레탄 포움에 의한 팔라듐의 추출)

  • Sam Woo Kang;Seung Seok Lee
    • Journal of the Korean Chemical Society
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    • v.27 no.4
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    • pp.268-272
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    • 1983
  • Polyurethane foam impregnated with ${\beta}$-diphenylglyoxime has been applied to the extraction of palladium(II) from platinum(IV) and nickel(II) in aqueous solution. Palladium(II) is quantitatively extracted from $0.01{sim}0.05M$ HCl. On the other hand, platinum(Ⅳ) was slightly extracted and nickel(II) was not found to be extraction in the same experimental condition. Based on the results obtained, the selective separation, removal and recovery of Pd(II) from Pt(IV) or Ni(II) was possible by batch or elution method.

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A Study on the Present Condition and Characteristic of Appeared Contaminants on the Surface of Stone Cultural Properties-Focus on the Contaminants of Ten storied pagoda of Gyeongcheonsa (석조문화재 표면에 발생된 오염물 현황 및 특성에 관한 연구-경천사십층석탑에 발생된 오염물을 중심으로)

  • Kim, Jin-Hyung;Lee, Ju-Wan;Han, Kyoung-Soon;Do, Jin-Young
    • 보존과학연구
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    • s.24
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    • pp.29-60
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    • 2003
  • The conservation problem of stone cultural properties is widely influenced by environmental pollution nowadays as well as agingsymptoms itself. Most stone cultural properties are directly affected by air pollution such as smoke, acid-rain, etc., resulting surface separation and pulverization. In the case of Ten storied pagoda of Gyeongcheonsa, once located in the center of the Seoul, the surface shows excessive contaminant by air pollution. It is very difficult to identify chemical structure and formation system of these contaminant. Also the discoloration and stains on the surface are not pleasant to see. Through the examination of the contaminant by SEM-EDS, it is observed that the major mineral is Gypsum and many other minerals were also revealed. The contaminant layer seems to be thin and wide at the south face of pagoda and thick and narrow at the north face. This distribution pattern could provide information on the surface characteristics of pagoda. Further, the information could help to identify the relationship between geological and environmental factors and the surface patterns.

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Transport Properties of Polymer Blend Membranes of Sulfonated and Nonsulfonated Polysulfones for Direct Methanol Fuel Cell Application

  • Kim, Dong-Hwee;Kim, Sung-Chul
    • Macromolecular Research
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    • v.16 no.5
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    • pp.457-466
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    • 2008
  • The relation between the phase separated morphologies and their transport properties in the polymer blend membrane for direct methanol fuel cell application was studied. In order to enhance the proton conductivity and reduce the methanol crossover, sulfonated poly(arylene ether sulfone) copolymer, with a sulfonation of 60 mol% (sPAES-60), was blended with nonsulfonated poly(ether sulfone) copolymer (RH-2000, Solvay). Various morphologies were obtained by varying the drying condition and the concentration of the casting solution (10, 15, 20 wt%). The transport properties of proton and methanol molecule through the polymer blend membranes were studied according to the absorbed water. AC impedance spectroscopy was used to measure the proton conductivity and a liquid permeability measuring instrument was designed to measure the methanol permeability. The state of water in the blend membranes was confirmed by differential scanning calorimetry and was used to correlate the morphology of the membrane with the membrane transport properties.

Performance Characteristics of the Double-Inlet Centrifugal Blower according to the Shape of an Impeller (임펠러 형상에 따른 양흡입 원심송풍기 성능특성)

  • Lee, Jong-Sung;Jang, Choon-Man
    • The KSFM Journal of Fluid Machinery
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    • v.17 no.1
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    • pp.28-34
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    • 2014
  • This paper presents the performance enhancement of a double-inlet centrifugal blower by the shape optimization of an impeller. Two design variables, a number of blade and a length of chord, are introduced, and analyzed by a response surface method. Three-dimensional compressible Navier-Stokes equations are used to analyze the blower performance and the internal flow of the blower. Throughout the numerical simulation of the blower, blower efficiency can be increased by reducing separation flow generating from the blade leading edge of a blade pressure surface. It is noted that recirculation flow observed inside the blade passage induces low velocity region, thus increases pressure loss. Efficiency and pressure of the optimum blower are successfully increased up to 3% and 3.9% compared to those of reference blower at the design flow condition, respectively. Detailed flow field inside the blower is also analyzed and compared.

Separation and Detection of Nonchromophore Aliphatic Compounds by Reversed-Phase Liquid Chromatography using Ultraviolet-Absorbing Reagent (자외선 흡수물질을 이용한 역상 액체 크로마토그라피에 의한 비흡수 지방족 화합물들의 검출과 분리)

  • Lee Seung-Seok;Kang Sam-Woo;Oh Hae-Beom
    • Journal of the Korean Chemical Society
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    • v.35 no.4
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    • pp.397-404
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    • 1991
  • Nonchromophore compounds such as aliphatic acids, alcohols and tetraalkylammonium salts could be detected by indirect photometric detection on the revered-phase liquid chromatography. Benzyltriethylammonium bromide(BTEAB) was used as a detection reagent. Also, the retention mechanism and response of samples were investigated to the several factors such as pH, temperature, and concentration of MeOH as well as concentration of detection reagents in mobile phase. And some mixture of samples were able to be separated under optimum condition.

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Highly Selective Derivative Spectrophotometry for Determination of Nickel Using 1-(2-Pyridylazo)-2-naphthol in Tween 80 Micellar Solutions

  • Eskandari, Habibollah
    • Bulletin of the Korean Chemical Society
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    • v.25 no.8
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    • pp.1137-1142
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    • 2004
  • A spectrophotometric and first derivative spectrophotometric method was developed in aquatic Tween 80 micellar solutions for selective determination of nickel without using any pre-separation step. 1-(2-Pyridylazo)-2-naphthol (PAN), as a sensitive chromogenic complexing agent formed a red-colored Ni(II)-PAN complex in Tween 80 media with satisfactory solubility and stability. Conditions such as pH, PAN concentration, type and concentration of micellizing agent were optimized. Molar absorptivity of Ni-PAN complex was found $4.62\;{\times}\;10^4L\;cm^{?1}\;mol^{?1}$ at 569 nm, under the optimum condition. Calibration graphs were derived by zero, first and second derivative spectrophotometry at maximum wavelengths of 569, 578 and 571 nm with linear ranges of 30-1800, 20-2500 and 30-2000 ng $mL^{?1}$ , respectively. Precision as standard deviation as well as accuracy as recovery percent were in the range of 1-20 ng $mL^{?1}$, and 93.3-103.3%, respectively, for the entire of the linear ranges. Spectrophotometric detection limit was 3 ng $mL^{?1}$ and effects of diverse ions on the first derivative determination of nickel were studied to investigate selectivity of the method. Interferences of cobalt and copper on the nickel determination were prevented using o-phenanthroline as masking agent. The recommended procedures were applied to the various synthetic and stainless steel alloys, tea leaves and human hair, with satisfactory results.

Low Temperature Fluidity Test System of Composited Package Fuel Heater for Diesel Cars (디젤차량용 통합연료히터의 저온유동성 시험장치개발)

  • Jang, Young-Sung;Yoon, Dal-Hwan
    • Journal of IKEEE
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    • v.18 no.2
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    • pp.185-191
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    • 2014
  • In this paper, we have implemented the low temperature fluidity test system with the composited package fuel heater, which has tested the low temperature fluidity and start time to evaluate the performance. Then we have compared the separation and the unified fuel heater type at $+20{\sim}-30^{\circ}C$. Also, we have tested the flowing pressure and start time, power consumption of heater. By comparing the performance with several condition, the experimental results obtain an improved start time of 23% and low temperature fluidity of 19%.