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Synthesis of Copper Nanoparticle by Multiple Thermal Decomposition and Electroless Ag Plating (복합적 열분해법을 이용한 구리 나노분말의 합성 및 무전해 은도금에 관한 연구)

  • PARK, JEONGSOO;KIM, SANGHO;HAN, JEONGSEB
    • Transactions of the Korean hydrogen and new energy society
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    • v.28 no.1
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    • pp.70-76
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    • 2017
  • To synthesize copper nanoparticle a thermal decomposition was adopted. And to solve the problem of surface oxidation of the synthesized copper powder an electroless Ag plating method was used. The size and shape of synthesized Cu nanoparticle were affected by the size of copper oxalate used as a precursor, reaction solvent, reaction temperature and amount of reducing agent. Especially reaction solvent is dominant factor to control shape of Cu nano-particle which can have the shapes of sphere, polygon and rod. In case of glycerol, it produced spherical shape of about 500 nm in size. Poly ethylene produced uniform polygonal shape in about 700 nm and ethylene glycol produced both of polygon and rod having size range between 500 and 1500 nm. The silver coated copper powder showed a high electrical conductivity.

Automatic Detection Algorithm of Radiation Surgery Area using Morphological Operation and Average of Brain Tumor Size (형태학적 연산과 뇌종양 평균 크기를 이용한 감마나이프 치료 범위 자동 검출 알고리즘)

  • Na, S.D.;Lee, G.H.;Kim, M.N.
    • Journal of Korea Multimedia Society
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    • v.18 no.10
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    • pp.1189-1196
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    • 2015
  • In this paper, we proposed automatic extraction of brain tumor using morphological operation and statistical tumors size in MR images. Neurosurgery have used gamma-knife therapy by MR images. However, the gamma-knife plan systems needs the brain tumor regions, because gamma-ray should intensively radiate to the brain tumor except for normal cells. Therefore, gamma-knife plan systems spend too much time on designating the tumor regions. In order to reduce the time of designation of tumors, we progress the automatical extraction of tumors using proposed method. The proposed method consist of two steps. First, the information of skull at MRI slices remove using statistical tumors size. Second, the ROI is extracted by tumor feature and average of tumors size. The detection of tumor is progressed using proposed and threshold method. Moreover, in order to compare the effeminacy of proposed method, we compared snap-shot and results of proposed method.

Twin Spray Characteristics Between Two Impinging F-O-O-F Type Injectors

  • Kang, Shin-Jae;Lee, Eun-Sang;Kwon, Ki-Chul;Oh, Je-Ha;Yu, Myoung-Jong
    • Journal of Mechanical Science and Technology
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    • v.16 no.5
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    • pp.732-742
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    • 2002
  • This paper presents twin spray characteristics of two impinging F-O-O-F type injectors in which fuel and oxidizer impinge on each other to atomize under the various conditions. The droplet size and velocity in the impinging spray flow field were measured using PDPA. The droplet size and velocity were investigated at the mixture ratios of 1.5, 2.0, 2.47 and 3.0 for four injectors in which two single F-O-O-F injectors were arranged at the intervals of 20.8, 31.2, 41.6 and 62.4mm respectively. In general, the arithmetic mean diameter, SMD and standard deviation of droplet size in the interaction area (X=0 and Y=0mm) were smaller, while the axial velocity in the interaction area was slightly higher. An empirical correlation is obtained for the (D$\_$10/)$\_$D//(D$\_$10/)$\_$c/ value under the assumptions of two identical droplets and these with different size and velocity. The droplets with low Weber numbers below 40 have possibility to coalesce, while those over 40 tend to disintegrate after impingement in the interaction area.

The Influence of Surface Modification of Gold Nanoparticles Supported on TiO2 in the Catalytic Activity of CO Oxidation

  • Park, Da-Hee;Reddy, A.S.;Eah, Sang-Kee;Park, Jeong-Young
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.213-213
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    • 2011
  • Gold catalysts supported on TiO2 have shown a unique catalytic behavior on CO oxidation, depending on surface effects. Particle size has an influence on the surface activity. To make monodisperse Au nanoparticles, organic capping ligands, such as alkylthiols, were used by a "greener" synthesis method [1,2] and Au nanoparticles were deposited on TiO2. However, organic capping ligands must be removed for high catalytic activities by the Au nanoparticles without changing the Au size [3]. We used UV ozone treatment to decompose thiol ligands. The samples have been characterized by X-ray photoelectron spectroscopy to examine the surface modification by UV ozone treatment. We show the size distribution of the gold nanoparticles by light scattering analysis and transmission electron microscopy. Au/TiO2 have been prepared using the wetness impregnation method. The catalytic performance of CO oxidation over Au supported on TiO2 under oxidizing reaction conditions (40 Torr CO and 100 Torr O2) were tested. The results show that the catalytic activity depends on particle size and the time of UV ozone exposure, which suggests the role of sulfur bonding in determining the catalytic activity of Au/TiO2 catalysts.

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Factors Affecting Financial Leverage: The Case of Vietnam Firms

  • NGUYEN, Chi Dieu Thi;DANG, Hong Thuy Thi;PHAN, Nghi Huu;NGUYEN, Trang Thuy Thi
    • The Journal of Asian Finance, Economics and Business
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    • v.7 no.11
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    • pp.801-808
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    • 2020
  • The purpose of the study is to find the factors that influence the financial leverage of Vietnam firms. The dependent variable is the financial leverage and the independent variables are firm size, asset structure, liquidity, growth opportunities, profitability, and firm age. The data are collected from Vietnam firms' annual financial reports in the period from 2010 to 2019. The study uses a sample of 448 Vietnam listed firms in the period. We also employ a panel regression model with pooled OLS and fixed effect to analyze the firms' financial data. The results of the model showed that financial leverage (FL) has a negative relationship with some factors such as asset structure (AS), liquidity (LQ), growth opportunities (GRW), profitability (ROA), and firm age (AGE) in the fixed effect regression. It means that when liquidity, profitability, and firm age increase, firms' financial leverage will decrease. While firms' financial leverage has still a positive relationship with the firm size (SIZE) in the model. As a result, when firm size increases, financial leverage will increase, too. The results showed that models are fit for the research and can be used to predict future findings. It is also useful for enterprises, financial advisors, investors, as well as the financial managers.

A study on spray characteristics of the triplet impinging stream type injector for liquid rocket (액체 로켓용 충돌형 Triplet 인젝터의 미립화 특성에 관한 연구)

  • Park, Sung-Young;Kim, Seon-Jin;Park, Seung-Woon;Kim, Yoo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.20 no.3
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    • pp.1005-1014
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    • 1996
  • An experimental investigation has been carried out to examine the influence of injector design variables and operating conditions on the resultant drop size for triplet impinging streams injectors. The variables studied in this investigation are pressure drop, impinging angle, orifice length to diameter ratio, and impinging point distance. Droplet-size data are obtained using water as the propellant simulant by Malvern Particle Analyzer System. Drop size decreases with increasing impinging angle and pressure drop while other injector parameters remain constant at the same point. But it is found that there is no noticeable droplet-size change which results from change in orifice length to diameter ratio or impinging point distance within the investigated range.

Reusing Search Window Data and Exploiting Early Termination in Variable Block Size Motion Estimation (가변 블록 크기 움직임 추정 기법에서 탐색 영역 데이터의 재사용과 조기 중단 기법의 적용)

  • Park, Taewook;Hur, Ahrum;Lee, Seongsoo
    • Journal of IKEEE
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    • v.20 no.1
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    • pp.111-114
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    • 2016
  • In HEVC, motion estimation is performed independently for each variable block size. So it requires several times of search window data, and also it is difficult to exploit early termination. In this paper, a new method is proposed to exploit search window data and early termination in variable block size. When applied to TZS algorithm, it reduces pixel comparison and search window data accesses to 1/3.7 ~ 1/2.9 with negligible image quality degradation.

A Video Cache Replacement Scheme based on Local Video Popularity and Video Size for MEC Servers

  • Liu, Pingshan;Liu, Shaoxing;Cai, Zhangjing;Lu, Dianjie;Huang, Guimin
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • v.16 no.9
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    • pp.3043-3067
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    • 2022
  • With the mobile traffic in the network increases exponentially, multi-access edge computing (MEC) develops rapidly. MEC servers are deployed geo-distribution, which serve many mobile terminals locally to improve users' QoE (Quality of Experience). When the cache space of a MEC server is full, how to replace the cached videos is an important problem. The problem is also called the cache replacement problem, which becomes more complex due to the dynamic video popularity and the varied video sizes. Therefore, we proposed a new cache replacement scheme based on local video popularity and video size to solve the cache replacement problem of MEC servers. First, we built a local video popularity model, which is composed of a popularity rise model and a popularity attenuation model. Furthermore, the popularity attenuation model incorporates a frequency-dependent attenuation model and a frequency-independent attenuation model. Second, we formulated a utility based on local video popularity and video size. Moreover, the weights of local video popularity and video size were quantitatively analyzed by using the information entropy. Finally, we conducted extensive simulation experiments based on the proposed scheme and some compared schemes. The simulation results showed that our proposed scheme performs better than the compared schemes in terms of hit rate, average delay, and server load under different network configurations.

A Study on the Shelf Sediments from Korea Strait through Decomposition of Size Curves into Normal Components (입도곡선의 정규성분 분해에 의한 대한해협의 대륙붕 퇴적물 연구)

  • KONG Young Sae;KIM Hee Joon;MIN Geon Hong;LEE Chi Won
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.29 no.3
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    • pp.386-392
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    • 1996
  • A numerical method based on genetic algorithms was introduced to characterize the grain-size distribution more effectively. This technique was proved significant particularly for multimodal size distributions, as was verified for samples from Korea Strait continental shelf. Sediment samples collected from the Korea Strait continental shelf revealed that $96\%$ of the grain-size distributions were multimodal. Therefore, the use of grain-size parameters was not the ideal method. As an alternative method, the decomposition of sue curves into elementary normal component curves was used. Means and standard deviations of 593 decomposed normal components were calculated by a numerical method from 268 size curves of Korea Strait sediments. The mean values of decomposed normal components showed peaks at $1\~3\phi\;and\;7\~9\phi$ size classes. The plot of mean and standard deviation values of the coarse fraction normal components on the map showed a characteristic areal distribution. The characteristic distribution was found to derive from underlying Pleistocene sediment on the basis of sea bottom geologic distribution of the area. The method of decomposition into normal components was found to be more effective than the analysis using traditional grain-size parameters in investigation of multimodal size distribution of Korea Strait shelf sediment.

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Size Measurement of Radioactive Aerosol Particles in Intense Radiation Fields Using Wire Screens and Imaging Plates

  • Oki, Yuichi;Tanaka, Toru;Takamiya, Koichi;Osada, Naoyuki;Nitta, Shinnosuke;Ishi, Yoshihiro;Uesugi, Tomonori;Kuriyama, Yasutoshi;Sakamoto, Masaaki;Ohtsuki, Tsutomu
    • Journal of Radiation Protection and Research
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    • v.41 no.3
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    • pp.216-221
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    • 2016
  • Background: Very fine radiation-induced aerosol particles are produced in intense radiation fields, such as high-intensity accelerator rooms and containment vessels such as those in the Fukushima Daiichi nuclear power plant (FDNPP). Size measurement of the aerosol particles is very important for understanding the behavior of radioactive aerosols released in the FDNPP accident and radiation safety in high-energy accelerators. Materials and Methods: A combined technique using wire screens and imaging plates was developed for size measurement of fine radioactive aerosol particles smaller than 100 nm in diameter. This technique was applied to the radiation field of a proton accelerator room, in which radioactive atoms produced in air during machine operation are incorporated into radiation-induced aerosol particles. The size of $^{11}C$-bearing aerosol particles was analyzed using the wire screen technique in distinction from other positron emitters in combination with a radioactive decay analysis. Results and Discussion: The size distribution for $^{11}C$-bearing aerosol particles was found to be ca. $70{\mu}m$ in geometric mean diameter. The size was similar to that for $^7Be$-bearing particles obtained by a Ge detector measurement, and was slightly larger than the number-based size distribution measured with a scanning mobility particle sizer. Conclusion: The particle size measuring method using wire screens and imaging plates was successfully applied to the fine aerosol particles produced in an intense radiation field of a proton accelerator. This technique is applicable to size measurement of radioactive aerosol particles produced in the intense radiation fields of radiation facilities.