• Title/Summary/Keyword: Scanning electron micrographs

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Performance evaluation of β-glucan treated lean clay and efficacy of its choice as a sustainable alternative for ground improvement

  • Kumara, S. Anandha;Sujatha, Evangelin Ramani
    • Geomechanics and Engineering
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    • v.21 no.5
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    • pp.413-422
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    • 2020
  • The choice of eco-friendly materials for ground improvement is a necessary way forward for sustainable development. Adapting naturally available biopolymers will render the process of soil stabilization carbon neutral. An attempt has been made to use β-glucan, a natural biopolymer for the stabilization of lean clay as a sustainable alternative with specific emphasis on comprehending the effect of confining stresses on lean clay through triaxial compression tests. A sequence of laboratory experiments was performed to examine the various physical and mechanical characteristics of β-glucan treated soil (BGTS). Micro-analysis through micrographs were used to understand the strengthening mechanism. Results of the study show that the deviatoric stress of 2% BGTS is 12 times higher than untreated soil (UTS). The micrographs from Scanning Electron Microscopy (SEM) and the results of the Nitrogen-based Brunauer Emmett Teller (N2-BET) analysis confirm the formation of new cementitious fibres and hydrogels within the soil matrix that tends to weld soil particles and reduce the pore spaces leading to an increase in strength. Hydraulic conductivity (HC) and compressibility reduced significantly with the biopolymer content and curing period. Results emphases that β-glucan is an efficient and sustainable alternative to the traditional stabilizers like cement, lime or bitumen.

Die-sinking Electrical Discharge Machining with Ultrasonic Emission for Ceramic Matrix Composite (초음파 진동 부가에 의한 세라믹 복합체의 형조방전가공)

  • Wang, Duck-Hyun;Woo, Jeong-Yun;Yun, Jon-Do
    • Journal of the Korean Society for Precision Engineering
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    • v.16 no.8
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    • pp.9-15
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    • 1999
  • Die-sinking electrical discharge machining(EDM) for conductive ceramic matrix composite(CMC) of Tic/$Al_2O_3$ was experienced with addition of ultrasonic emission, and the results were compared with ones obtained by the EDM only. From this experimental study, the values of material removal rate(MRR) and surface roughness($R_{max}$), scanning electron microscope(SEM) micrographs, and weibull probability distribution of bending strength for the specimens were obtained and compared. The trend of MRR was found to be increased slightly with the current and the duty factor for both EDM only and EDM with ultrasonic emission. The MRR values were found to be increased for EDM with ultrasonic emission. The SEM micrographs of EDMed surface by under various operating conditions showed less micro cracks in various places. Although smaller bending strength value was obtained by EDMed surface with ultrasonic emission by weibull probability distribution analysis of bending strength.

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An Electrochemical Approach for Fabricating Organic Thin Film Photoelectrodes Consisting of Gold Nanoparticles and Polythiophene

  • Takahashi, Yukina;Umino, Hidehisa;Taura, Sakiko;Yamada, Sunao
    • Rapid Communication in Photoscience
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    • v.2 no.3
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    • pp.79-81
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    • 2013
  • A novel method of fabricating polythiophene-gold nanoparticle composite film electrodes for photoelectric conversion is demonstrated. The method includes electrodeposition of gold and electropolymerization of 2,2'-bithiophene onto an indium-tin-oxide (ITO) electrode. First, electrodeposition of gold onto the ITO electrode was carried out with various repetition times of pulsed applied potential (0.25 s at -2.0 V vs. Ag/AgCl) in an aqueous solution of $HAuCl_4$. Significant progress of the number density of deposited gold nanoparticles was confirmed from scanning electron micrographs, from 4 (1 time) to 25% (15 times). Next, electropolymerization of 2,2'-bithiophene onto the above ITO electrode was performed under controlled charge condition (+1.4 V vs. Ag wire, 15 $mC/cm^2$). Structural characterization of as-fabricated films were carried out by spectroscopic and electron micrographic methods. Photocurrent responses from the sample film electrodes were investigated in the presence of electron acceptors (methyl viologen and oxygen). Photocurrent intensities increased with increasing the density of deposited gold nanoparticles up to ~10%, and tended to decrease above it. It suggests that the surplus gold nanoparticles exhibit quenching effects rather than enhancement effects based on localized electric fields induced by surface plasmon resonance of the deposited gold nanoparticles.

On the Composites of Poly(ethylene terephthalate) with a Liquid Crystalline Polyester (액정 폴리에스테르와 폴리(에틸렌 테레프탈레이트)의 복합재료 연구)

  • Choi, Jae-Kon;Bang, Moon-Soo;Han, Chul
    • Applied Chemistry for Engineering
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    • v.8 no.1
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    • pp.76-83
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    • 1997
  • Blends of thermotropic liquid crystalline polymer(TLCP) with poly(ethylene terephthalate) (PET) were prepared by the coprecipitation from a common solvent. The blends were processed through a capillary die at $287^{\circ}C$ to produce a monofilament. Morphology and mechanical, thermal properties of blends and composites were examined by differential scanning calorimetry(DSC), tensile test, optical microscopy and scanning electron microscopy. Crystallization kinetics of the blends were investigated by the isothermal DSC method. The Avrami analyses were applied to obtain the information on the crystal growth geometry and factors controlling the rate of crystallization. In the blends, liquid crystalline phase did not reveal any significant macrophase separation and thermal degradation at the processing temperature. From scanning electron micrographs of cryogenic fracture surfaces of extruded fibers, the TLCP domains were found to be more or less finely dispersed with $0.1{\mu}m$ to $0.2{\mu}m$ in size. Interfacial adhesion between the TLCP and matrix polymer was excellent. Tensile strength and modulus of TLCP/PET in-situ fiber composites were enhanced with increasing draw ratio and LCP content.

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Measurement of residual stress of steel filaments by using focused ion beam and digital image correlation (집속 이온빔과 디지털 화상 관련법를 이용한 고 탄소 미세 강선의 잔류 응력 측정)

  • Yang, Y.S.;Bae, J.G.;Kang, K.J.;Park, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.05a
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    • pp.241-245
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    • 2007
  • The residual stress in axial stress in the axial direction of the steel filaments has been measured by using a method based on the combination of the focused ion beam (FIB) and high resolution strain mapping program (VIC-2D). That is, the residual stress was calculated from the measured displacement field before and after the introduction of a slot along the steel filaments. The displacement was obtained by the digital correlation analysis of high-resolution scanning electron micrographs, while the slot was introduced by FIB milling with low energy beam. The present measurement revealed that the residual stress within 8% of the magnitude was persistent in the steel filaments fabricated.

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The Effect on the Wear-Corrosion Behavior of Ductile Cast Iron in the Various pH Environments (구상흑연주철재의 마멸-부식특성에 미치는 pH의 영향)

  • 임우조;박동기
    • Tribology and Lubricants
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    • v.19 no.1
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    • pp.31-35
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    • 2003
  • This paper reports the studies on the wear-corrosion behavior of ductile cast iron in the various pH environments. In the variety of pH solutions, corrosion and wear-corrosion loss of GCD 600 were investigated. Also, the anodic polarization test of GCD 600 using potentiostat/galvanostat was carried out. And rubbed surface of GCD 60 using scanning electron micrographs after immersion and wear-corrosion test was examined in the environment of various pH values. The main results are as following In alkali zone, the wear-corrosion loss of GCD 600 increases, but corrosion loss decreases. The unevenness and crack of wear-corrosion surface in neutral zone becomes duller than that in alkali zone. As the corrosive environment is acidified, wear-corrosion behavior of GCD 600 with passing immersion time becomes sensitive.

Achene wall anatomy and surface sculpturing of Launaea Cass. (Compositae: Cichorieae) with notes on their systematic significance

  • Zareh, Momen Mustafa;Faried, Ahmed Mohamed;Mohamed, Mona Hassan
    • Korean Journal of Plant Taxonomy
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    • v.46 no.2
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    • pp.187-198
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    • 2016
  • This is the first study to deal in-depth with the achene ultra-structure of the genus Launaea Cass. in Egypt. It focuses on 12 taxa belonging to 10 species of this genus. The achene wall anatomy and surface sculpturing of those taxa were studied using scanning electron microscopy (SEM). Important aspects of the investigated taxa based on the achene characters as well as SEM micrographs of the achene surface and anatomical sections are given. Main and secondary costa of the inner achenes are used for easy differentiation between L. intybacea and L. massauensis.

Adsorptivities and Particle Surface Properties of the Activated Carbon Made from Rice-chaff (왕겨로부터 제조한 활성탄의 입자표면특성과 흡착력)

  • Lee, Dong-Sun;Lee, Myung-Hwan;Lee, Yoon-Joong;Ahn, Moon-Gyu
    • YAKHAK HOEJI
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    • v.32 no.3
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    • pp.187-193
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    • 1988
  • An activated carbon which showed big adsorption capacities of iodine, potassium permanganate and phenol was prepared from the Korean ricechaff. By scanning electron micrographs and IR spectra, it was observed that the organic components in the rice-chaff were decomposed to carbon dioxide and vapor by the pyrolysis and the activation, that activated carbon particles had carbon-carbon structures with a lot of microporosity. The adsorption capacities of iodine, potassium permanganate and phenol were determined. The adsorption isotherm of phenol was well fitted in Freundlich's equation.

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Wear Characteristics of Submerged-Arc Cladding (서브머지드 아크 클래딩에 의한 표면 피복층의 마모특성)

  • 김권흡;강용규;권오양;육선평
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2002.05a
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    • pp.844-847
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    • 2002
  • This paper is to investigate the wear behavior of submerged-arc clad materials by the wear test with a ball-on-disk type wear testing machine in air. The specimens were clad with Stoody105 alloy wire on a carbon steel (SM45C) substrate by submerged-arc cladding process under different welding parameters. The wear behavior of the cladding through ball-en-disk test has been studied under the wear load from 5N to 16N and sliding speed from 8cm/s to 35cm/s. The weight of the specimen loss was measured. Scanning electron micrographs of the worn surface show a layer of oxide film formed on the worn surface. Oxidation wear mechanism controls the wear process. The spalling of the oxide is caused by the repeated rubbing fatigue mechanism.

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Effects of Cutting Direction on the Laser Machining Characteristics of Wood (절삭방향(切削方向)이 목재(木材)의 레이저절삭특성(切削特性)에 미치는 영향(影響))

  • Lee, Hyoung-Woo
    • Journal of the Korean Wood Science and Technology
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    • v.24 no.4
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    • pp.87-92
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    • 1996
  • When cutting 2.0cm-thick red oak and hard maple with an air-jet-assisted carbon-dioxide laser of 2kW output power, maximum feed speed at the point of full penetration of the beam decreased with increasing the angle between grain and cutting direction. Feed speed averaged 3.75 and 3.38 meters per minute for red oak and hard maple, respectively. Gray-level of laser-cut surfaces were analyzed by image analysis system. The highest gray level of laser-cut surface was obtained when red oak was cut parallel to grain by laser. Surface profiler was used to scan the sawn and laser-cut surfaces. Center line average roughnesses of laser-cut surfaces were higher than those of sawn surfaces. Scanning electron micrographs showed the cell walls which were melted by laser.

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