• Title/Summary/Keyword: Scanning electron mcroscopy

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The Fabrication of Mg9Ti1-(10, 20 wt%)Ni Hydrogen Absorbing Alloys by Hydrogen Induced Mechanical Alloying and Evaluation of Hydrogenation Properties (Part I : Preparations and Characterizations of Alloys) (수소 가압형 기계적 합금화법을 이용한 Mg9Ti1-(10, 20 wt%)Ni 수소저장합금의 제조와 수소화 특성 (제 1보 : 합금제조와 특성평가))

  • Hong, Tae-Whan;Kim, Gyung-Bum;Kim, Young-Jig
    • Transactions of the Korean hydrogen and new energy society
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    • v.13 no.3
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    • pp.197-203
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    • 2002
  • The main emphasis of this study was to find an new hydrogen absorbing alloy such as Mg-Ti-Ni-H systems, and to investigate their hydrogenation properties. ($Mg_9Ti_x$)-10, 20wt%Ni-Hx systems were prepared by hydrogen induced mechanical alloying(HIMA) using Mg and Ni chips and sponge Ti. The particles synthesized were characterized by X-ray diffraction, and their morphologies were observed by means of scanning electron microscopy(SEM) with energy dispersive spectrometry (EDS). In addition, the crystal structures were analyzed in terms of their bright-/ dark field images and the selected area diffraction pattern(SADP) of transmission electron microscopy(TEM).