• Title/Summary/Keyword: Sample testing

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Effect of particle size and scanning cup type for near infrared reflection on the soil property measurement

  • Ryu, Kwan-Shig;Cho, Rae-Kwang;Park, Woo-Churl;Kim, Bok-Jin
    • Near Infrared Analysis
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    • v.1 no.2
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    • pp.35-39
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    • 2000
  • The purpose of this research was to find out suitable soil sample preparation and sample holding tools for NIR reflection radiation for estimating soil components. NIR reflectance was scanned at 2nm intervals from 1,100 to 2,500nm with an InfraAlyzer 500(Bran+Luebbe Co.). Coarse(2.0mm) and fine(0.5mm) soil sample and various sample holding tools were used to obtain mean diffuse reflection of the soil for the calibration and validation of the calibration set in estimating moisture, organic matter and total nitrogen of the soils. Multiple linear regression was used to obtain the best correlation of NIR spectroscopy method. Correlation of NIR spectroscopy method. Correlation of NIR spectra for finely and coarsely sized soil did not show much difference. The standard errors of prediction(SE) using different types of sample holding tools for organic matter, total nitrogen and soil moisture were better than 0.765, 0.041 and 0.63% respectively. From the results it can be concluded that NIR spectroscopy with flow type cell could be used as a fast routine testing method in quantitative determination of organic matter, total nitrogen and soil moisture.

Two-sample chi-square test for randomly censored data (임의로 관측중단된 두 표본 자료에 대한 카이제곱 검정방법)

  • 김주한;김정란
    • The Korean Journal of Applied Statistics
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    • v.8 no.2
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    • pp.109-119
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    • 1995
  • A two sample chi-square test is introduced for testing the equality of the distributions of two populations when observations are subject to random censorship. The statistic is appropriate in testing problems where a two-sided alternative is of interest. Under the null hypothesis, the asymptotic distribution of the statistic is a chi-square distribution. We obtain two types of chi-square statistics ; one as a nonnegative definite quadratic form in difference of observed cell probabilities based on the product-limit estimators, the other one as a summation form. Data pertaining to a cancer chemotheray experiment are examined with these statistics.

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Feasibility Study on Detection of Crack in Bovine Incisor Using Active Thermography (보빈 치아 균열의 적외선 열화상 검사 가능성에 관한 실험적 연구)

  • Kim, Woo-Jae;Yang, Seung-Yong;Kim, No-Hyu
    • Journal of the Korean Society for Nondestructive Testing
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    • v.31 no.5
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    • pp.508-515
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    • 2011
  • Bovine incisor was investigated using active infrared thermography(IRT) to visualize crack on bovine teeth. An artificial crack was carefully created in bovine incisor sample by compression load of universal tensile machine. While applying a sinusoidal heat wave to the cracked bovine incisor through halogen lamp, consecutive digital infrared images was captured from the sample surface at a frequency synchronized with heat excitation. Phase information of thermal image was calculated by four-point correlation method and processed to produce the phase image of bovine incisor. This phase image showed clearly the crack on the incisor, which was hardly detected in traditional passive thermography.

Index Properties and Undrained Shear Strength of the Pusan Clays by Fall Cone Test (부산점토의 Fall Cone Test에 의한 지수 및 강도특성)

  • ;;Pham Huy Giao
    • Proceedings of the Korean Geotechical Society Conference
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    • 2000.11a
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    • pp.391-398
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    • 2000
  • The index properties of cohesive soils play an important role to examine entire tendency of soil properties. Especially, the Atterberg limits have a good correlation with compression and shear strength of cohesive soils. However, these values strongly depend on their testing methods. In this study, for Pusan clays the Atterberg limits were peformed under different conditions; for example, four kinds of specimen preparation, two kinds of testing equipment, and four kinds of estimating method. And a laboratory vane test was peformed to compare the undrained shear strength with that of the fall cone test. As experimental results, the value of liquid limit performed for oven-dried sample, followed in ASTM D4318, underestimated by about 10% compared to those of another three methods, irrespective to the used equipments. But the value of plastic limit was not influenced by sample preparation methods and equipments. The liquid limits by one-point methods(Leroueil et al., 1996; Nagaraj et al., 1981) were agreed well with those of different methods. Finally, the undrained shear strength by laboratory vane test was relatively larger than that of fall cone test, and the relationship between both showed a bad trend.

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Microstructure and Processing of Bioactive Ceramic Composites as Dental Implants (치과 임플란트용 bioactive 세라믹 복합재료의 제조와 미세조직)

  • Kim, Bu-Sob
    • Journal of Technologic Dentistry
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    • v.25 no.1
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    • pp.21-28
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    • 2003
  • The purpose of this study was to process bio-active glass ceramic composite, reinforced with sapphire fibers, by hot press. Also to study the interface of the matrix and the sapphire fiber, and the mechanical properties. Glass raw materials melted in Pt crucible at 1300$^{\circ}C$ during 3.5 hours. The melt was crushed in ball mill and then crushed material, ground and sieved to $<40{\beta}{\mu}m$. Sapphire fibers cut (30mm) and aligned. Powder and fibers hot pressed. The micrographs show good bonding between the matrix and the fiber and no porosity in the glass matrix. This means ideal fracture phenomena. Glass is fractured before the fiber. This is indication of good fracture strength. EDXS showing aluminum rich phase and crystalline phase. Bright field image of the matrix showing crystalline phase. Also diffraction pattern of TEM showing the crystalline phase and more than one phase. Strength of the samples was determined by 3 point bend testing. Strength of the 10vol% sample was approximately 69MPa, while strength of the control sample is 35MPa. Conclusions through this study as follow: 1. Micrographs show no porosity in the glass matrix and the interface. 2. The interface between the fiber and the glass matrix show no gaps. 3. Fracture of the glass indicates characteristic fiber-matrix separation. 4. Presence of crystalline phase at high processing temperature. 5. Sapphire is compatible with bioactive glass.

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4:2:1 compromise plans using Min-Max method (Min-Max 방법을 적용한 4:2:1 절충적 계획)

  • 최재혁;강창욱
    • Journal of Korean Society of Industrial and Systems Engineering
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    • v.21 no.47
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    • pp.1-10
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    • 1998
  • Testing high reliability devices under nomal operating condition is difficult, because the devices are not likely to fail in the relatively short time available for tests. For most applications it is necessary to accelerate the causes of failure by increasing a stress above its nomal value. Previous accelerated life test(ALT) plans have shown how to find optimum allocation, lowest stress and sample size subject to minimizing the variance of mean life estimator. In these ALT plans, the highest acceptable test-stress was assumed to be specified in advance by the experimenter but there is no guidance for selecting it. This assumption is, however, inappropriate for many applications. Testing devices at too-high stress levels can invalidate the extrapolation model, or introduce failure mechanisms that are not anticipated under nomal operating conditions. In this paper, we propose new 4:2:1 compromise plans using Min-Max method to minimize this risk and present minimized test-stress levels(max, middle, min), and find sample allocation based on Min-Max 4:2:1 compromise plans. In result, we compare previous 4:2:1 compromise plans specified maximum test-stress with Min-Max 4:2:1 compromise plans minimized maximum test-stress.

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Implementation of Statistical Significance and Practical Significance Using Research Hypothesis and Statistical Hypothesis in the Six Sigma Projects (식스시그마 프로젝트에서 연구가설과 통계가설에 의한 통계적 유의성 및 실무적 유의성의 적용방안)

  • Choi, Sung-Woon
    • Journal of the Korea Safety Management & Science
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    • v.15 no.1
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    • pp.283-292
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    • 2013
  • This paper aims to propose a new steps of hypothesis testing using analysis process and improvement process in the six sigma DMAIC. The six sigma implementation models proposed in this paper consist of six steps. The first step is to establish a research hypothesis by specification directionality and FBP(Falsibility By Popper). The second step is to translate the research hypothesis such as RHAT(Research Hypothesis Absent Type) and RHPT(Research Hypothesis Present Type) into statistical hypothesis such as $H_0$(Null Hypothesis) and $H_1$(Alternative Hypothesis). The third step is to implement statistical hypothesis testing by PBC(Proof By Contradiction) and proper sample size. The fourth step is to interpret the result of statistical hypothesis test. The fifth step is to establish the best conditions of product and process conditions by experimental optimization and interval estimation. The sixth step is to draw a conclusion by considering practical significance and statistical significance. Important for both quality practitioners and academicians, case analysis on six sigma projects with implementation guidelines are provided.

Estimation of the Number of Sources Based on Hypothesis Testing

  • Xiao, Manlin;Wei, Ping;Tai, Heng-Ming
    • Journal of Communications and Networks
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    • v.14 no.5
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    • pp.481-486
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    • 2012
  • Accurate and efficient estimation of the number of sources is critical for providing the parameter of targets in problems of array signal processing and blind source separation among other such problems. When conventional estimators work in unfavorable scenarios, e.g., at low signal-to-noise ratio (SNR), with a small number of snapshots, or for sources with a different strength, it is challenging to maintain good performance. In this paper, the detection limit of the minimum description length (MDL) estimator and the signal strength required for reliable detection are first discussed. Though a comparison, we analyze the reason that performances of classical estimators deteriorate completely in unfavorable scenarios. After discussing the limiting distribution of eigenvalues of the sample covariance matrix, we propose a new approach for estimating the number of sources which is based on a sequential hypothesis test. The new estimator performs better in unfavorable scenarios and is consistent in the traditional asymptotic sense. Finally, numerical evaluations indicate that the proposed estimator performs well when compared with other traditional estimators at low SNR and in the finite sample size case, especially when weak signals are superimposed on the strong signals.

Significant Parameters for Assessing Soil Contaminant-Leaching to Groundwater and Determining Soil Sample Size in Field Survey

  • Jeong, Seung-Woo;An, Youn-Joo
    • Environmental Engineering Research
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    • v.13 no.2
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    • pp.73-78
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    • 2008
  • For a given soil-contaminated site, a level of soil contamination is characterized and decisions on risk may be made from the risk assessment. The study evaluated critical design factors for the determination of sample size in the sampling design plan and the assessment of soil contaminant- leaching to groundwater. Two variables, the minimum relative detectable difference (T) and coefficient of variation (CV) were evaluated for the sample size determination. The minimum number of samples can be appropriately determined by CV under a T value greater than or equal to 0.2. Soil-contaminant leaching to groundwater was evaluated by using the Soil Screening Level equation of U.S. Environmental Protection Agency and the Risk Based Screening Level equation of American Society for Testing and Materials, with the same input parameters. The groundwater concentrations estimated from soil contaminant concentrations were significantly affected by the Darcy velocity of groundwater and the organic content of soil.

Applications on p-values of Chi-Square Distribution

  • Hong, Chong Sun;Hong, Sung Sick
    • Communications for Statistical Applications and Methods
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    • v.9 no.3
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    • pp.877-887
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    • 2002
  • In this paper, behaviors and properties of p-values for goodness-of-fit test are investigated. With some findings on the p-values, we consider some applications to determine sample size of a survey research using the regression equation based on a pilot study data. Regression equations are obtained by the well-known least squared method, and we find that regression lines could be formulated with only two data points, alternatively. For further studies, this works might be extended to t distributions for testing hypotheses about population mean in order to determine sample size of a prospective study. Also similar arguments could be explored for F test statistics.