• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2005년도 추계학술대회 논문집
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• pp.186-189
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• 2005

This paper was designed to assess the adhesive properties of hard coatings on non-nitrided and nitrided various tool steels. Estimations of adhesion were done to scratch test which is mainly used in hard coating. The critical load(Lc) between coating and substrate is defined through analysis of frictional load vs. normal load curve, signals of acoustic emission and optical observations. Coatings employed in this study are TiN, CrN and TiAlN, tools as substrates are STD11, STD61 and SKH51. It was classified to substrates with/without nitrided layer and hard coatings on substrate were deposited by arc PVD. Results showed that harder substrates and coatings give higher values of critical loads.

• Journal of electromagnetic engineering and science
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• 제4권3호
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• pp.97-101
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• 2004

Complex permittivities of reference liquids were measured by a liquid holder of slotted coaxial line with a movable probe at mobile communication frequencies. The validity of the liquid measurement system was checked by experimental tests with the reference liquids proposed in IEEE Std. 1528-200X or IEC 106/61/CDV.

• 열처리공학회지
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• 제14권1호
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• pp.8-16
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• 2001

The effects of gas composition, pressure, temperature and time on the case thickness, hardness and nitride formation in the surface of tool steels(STD11 and STD61) have been studied by micro-pulse plasma nitriding. External compound layer and internal diffusion layer and the diffusion layer were observed in the nitrided case of tool steels. The relative amounts and kind of phases formed in the nitrided case changed with the change of nitriding conditions. Generally, only nitride phases such as ${\gamma}(Fe_4N)$, ${\varepsilon}(Fe_{2-3}N)$, or $Cr_{1.75}V_{0.25}N_2$ phases were detected in the compound layer, while nitride and carbide phases such as ${\varepsilon}-nitride(Fe_{2-3}N)$, $(Cr,Fe)_{\gamma}C_3$ or $Fe_3C$ were detected in the diffusion layer by XRD analysis. The thickness of compound layer increased with the increase of nitrogen content in the gas composition. Maximum case depth was obtained at gas pressure of 200Pa.

• 한국정밀공학회지
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• 제12권4호
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• pp.100-110
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• 1995

This paper aims at reviewing the possibility of application over normal or abnormal, detection used by AE, and the characteristics of grinding processes. In this study, when WA-vitri-fied ' resinoid bond grinding wheels:36 kinds of grinding wheel and grinding depth were tuned at the surface grinding, the zone of AE signal generation is theoretically modelled and reviewed by grinding processes. The variation of grinding resistance( F$n^{9}$ $F_{t}$) and AE signal is detected in-process by the use of AE measuring system. The tests are carried out in accordance with grain size and grade of grinding wheels, and work-pieces-STD11 and STD61. According to the experiment's results, the following can be expected;as grinding time passes by, the relation of grinding depth and quantity of AE signal, observing on AE signal and grinding burn suggest the characteristics of grinding processes and evalution on the possibility of control of grinding machine, and monitoring abnormal conditions.e, and monitoring abnormal conditions.

• Asian Pacific Journal of Cancer Prevention
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• 제13권5호
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• pp.2095-2100
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• 2012

Sulforaphane (SFN) an isothiocyanate formed by hydrolysis of glucosinolates found in Brassica oleraceae is reported to possess anticancer and antioxidant activities. In this study, we isolated SFN from red cabbage (Brassica oleraceae var rubra) and evaluated the comparative antiproliferative activity of various fractions (standard SFN, extract and purified SFN) by MTT assay in human epithelial carcinoma HEp -2 and and Vero cells. Probable apoptotic mechanisms mediated through p53, bax and bcl-2 were also examined. The SFN fraction was collected by HPLC, enriched for its SFN content and confirmed. Expression of apoptosis-related proteins was detected by western blotting and RT PCR. Results showed that Std SFN and purified SFN concentration found to have closer $IC_{50}$ which is equal to 58.96 microgram/ml (HEp-2 cells), 61.2 microgram/ml (Vero cells) and less than the extract which is found to be 113 microgram/ml (HEp-2 cells) and 125 microgram/ml (Vero cells). Further studies on apoptotic mechanisms showed that purified SFN down-regulated the expression of bcl-2 (antiapoptotic), while up-regulating p53 and Bax (proapoptotic) proteins, as well as caspase-3. This study indicates that purified SFN possesses antiproliferative effects the same as Std SFN and its apoptotic mechanism in HEp-2 cells could be mediated through p53 induction, bax and bcl-2 signaling pathways.

• 열처리공학회지
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• 제6권3호
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• pp.166-177
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• 1993

Bending fatigue strength tests were made for VC coated die steels which were coated by immersing in a molten borax bath and for hardened die steels which were quenched and tempered, in order to clarify the effect of VC coating at $1000^{\circ}C$ and $1025^{\circ}C$. The material used in this investigation was a representative cold and hot die steels STD11, STD61. The results obtained are as follows. 1) The endurance limit of VC coated die steels was a little lower than that of hardened die steels. It is considered to be mainly due to the decfl.lase of hardness in the substrates. Accordingly, the endurance limit reo covered almost to the level of hardened die steels by an additional diffusion treatment. 2) The initiation point of fatigue fracture of VC coated die steels in reversed bening was on the substrate just under the VC layer. Hence, the endurance limit is corrected to the hardness of this part. 3) But, there is a considerable scatter in this relationship and the endurance limit of VC coated die steels was a little lower than that of hardened die steels with equal hardness. These results suggest that the fatigue strength of VC coated die steels is determined not only by the hardness but also by other factors. For example. the residual stress in the substrate just under VC coating layer is one of the factors besides hardness which is mainly related to the retained austenite(${\gamma}_R$).

• 열처리공학회지
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• 제7권4호
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• pp.318-327
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• 1994

According to conventional nitriding of tool steels, it was very difficult to produce a high surface hardness. This study has been conducted to investigate the influence of initial structures on the nitriding characteristics of tool steels in gas-nitrided for the improvement in surface hardness. The specimens (SACM645, STD61 steels) have been quenching and tempering at various temperature and then gas-nitrided for 30, 45 and 60hr at 500, 530 and $550^{\circ}C$ respectively in gasatmosphere of 30%$NH_3-70%N_2$ As hardness of initial structure was higher, the nitriding layer was deeper and hardness of the nitriding layer was higher. Deeper nitriding layers was due to higher diffusion rate by fine initial microstructure. Also the reason of high surface hardness was associated with formation of dispersed fine carbonitrides of nitrides.

• 한국경영과학회:학술대회논문집
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• 한국경영과학회 1997년도 추계학술대회발표논문집; 홍익대학교, 서울; 1 Nov. 1997
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• pp.133-136
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• 1997

미 국방성에서 병참 지원업무의 전산화로 시작한 CALS에 대한 관심은 현재 산업계에서도 널리 확산되고 있다. 본 연구에서는 CALS의 시작이라고도 말할 수 있는 형상관리(CM)에 관한 관련 표준들을 분석함으로서 '정보의 공유'라는 측면에서 CALS에 대한 접근을 시도하고자 한다. 형상관리는 병참지원시스템의 설계, 제조, 유지보수에 이르기까지 생명주기에 대한 모든 관리를 지원하는 방법이다. 이러한 형상관리를 위한 표준관련 문서에는 MIL-STD-2549, EIA/IS-649, MIL/HDBK-61등이 있다. 여기에서는 이런 표준관련 문서를 바탕으로 형상관리를 위한 하부 인프라 구조에는 어떠한 준비들이 필요하고 또 형상관리시스템을 실제로 구현하는 기업입장에서는 어떻게 바라보고 있는지, 실제 구현시에 고려해야 할 사항들은 어떠한 것들이 있는지에 대하여 논의해보고자 한다.

• Design & Manufacturing
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• 제8권2호
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• pp.23-29
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• 2014

Salt bath heat treatment is usually used but recently vacuum heat treatment is increased for the heat treatment of hot work die steels. The differences in two heat treatment processes were compared by testing the mechanical properties of heat treated products. With two different features of processes, mechanical properties such as hardness, tensile strength and impact strength of products show very different results. In this study salt bath heat treated products showed higher tensile strength and impact strength than vacuum heat treated products but hardness was not much different. These lower mechanical properties of vacuum heat treated products are due to differences in heating and quenching process.

• 한국재료학회지
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• 제12권8호
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• pp.676-681
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• 2002

Microstructure, mechanical properties, and oxidation resistance of TiAIN thin films deposited on quenched and tempered STD61 tool steel by arc ion plating were studied using XRD, XPS and micro-balance. The TiAIN film was grown with the (200) orientation. The grain size of TiAIN thin film decreased with increasing Al contents, while chemical binding energy increased with Al contents. When hard coating films were oxidized at $850^{\circ}C$ in air, oxidation resistance of both TiN and TiCN films became relatively lower since the surface of films formed non-protective film such as $TiO_2$. However, oxidation resistance of TiAIN film was excellent because its surface formed protective layer such as $_A12$$O_3$ and $_Al2$$Ti_{7}$$O_{15}$, which suppressed oxygen intrusion.