• 제목/요약/키워드: SPE-HG-ICP-AES

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Analysis of arsenic in contaminated soil SRM by two extraction methods: Ultrasonic extraction method and Microwave extraction method

  • Kim, Youn-Tae;Yoon, Hyeon;Shin, Mi-Young;Yoon, Cheol-Ho;Woo, Nam-Chil
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2004년도 임시총회 및 추계학술발표회
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    • pp.227-230
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    • 2004
  • Two extraction techniques, Ultrasonic and Microwave extraction method, were tested for the determination of arsenic in contaminated soil SRM (Montana Soil). The extraction mixture was prepared by mixing 1 M ortho-phosphoric acid and 0.1 M ascorbic acid. This extractant was known to preserve arsenic species. The appropriate extraction time was 10 min to 20 min and the recovery rate was about 80%. A coupled system, SPE-HG-ICP-AES, was used for the determination of inorganic arsenic species. The detection limit was around 2 $\mu\textrm{g}$/1 and the linearity of calibration curve was better than $R^2$=0.99.

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