• Title/Summary/Keyword: SN2000

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Degradation Damage Evaluation of High Temperature Structural Components by Electrochemical Anodic Polarization Test (전기화학적 양극분극시험에 의한 고온 설비부재의 열화손상 평가)

  • Yu, Ho-Seon;Song, Mun-Sang;Song, Gi-Uk;Ryu, Dae-Yeong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.6 s.177
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    • pp.1398-1407
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    • 2000
  • The structural steels of power plant show the decrease of mechanical properties due to degradation such as temper embrittlement, creep damage and softening during long-term operation at high temper ature. The typical causes of material degradation damage are the creation and coarsening of carbides(M23C6, M6C) and the segregation of impurities(P, Sb and Sn) to grain boundary. It is also well known that material degradation induces the cleavage fracture and increases the ductile-brittle transition temperature of steels. So, it is very important to evaluate degradation damage to secure the reliable and efficient service condition and to prevent brittle failure in service. However, it would not be appropriate to sample a large test piece from in-service components. Therefore, it is necessary to develop a couple of new approaches to the non-destructive estimation technique which may be applicable to assessing the material degradation of the components with not to influence their essential strength. The purpose of this study is to propose and establish a new electrochemical technique for non-destructive evaluation of material degradation damage for Cr-Mo steels which is widely used in the high temperature structural components. And the electrochemical anodic polarization test results are compared with those of semi-nondestructive SP test.

Surface Modification of Synthetic Graphite as an Electrode by Fluidized-bed Chemical Vapor Deposition for Lithium Secondary Batteries (유동상 화힉증착에 의한 리튬이차전지 전극용 탄소재료의 표면개질)

  • Ryu D. H.;Lee Joong Kee;Park D. G.;Yun K. S.;Cho B. W.;Shul Y. G.
    • Journal of the Korean Electrochemical Society
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    • v.3 no.3
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    • pp.173-177
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    • 2000
  • The synthetic carbon was coated with tin oxide and copper by fluidized-bed chemical vapor deposition method. $(CH_3)_4Sn\;and\;Cu(hfac)_{2s}$ were employed as the metallic organic precursor, respectively. The modified synthetic carbons were used for lithium secondary battery anode to investigate their coating effects on electrochemical characteristics as alternative anode materials for lithium secondary batteries. The electrode which prepared by the synthetic carbons(MCMB) coated with tin oxide gave the higher capacity than that of raw material. Their capacity decreased with the progress of cycling possibly due to severe volume changes. But the cyclability was improved by coating with copper on the surface of the tin oxide coated carbon, which plays an important role as an inactive matrix buffering volume changes.

Practical Application of Lead-free Solder in Electronic Products

  • Cho Il-Je;Chae Kyu-Sang;Min Jae-Sang;Kim Ik-Joo
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2004.09a
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    • pp.93-99
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    • 2004
  • At present, LG Electronics pushes ahead to eliminate the Pb(Lead) -a hazardous material- from all products. Especially, we have performed to select the optimum standard composition of lead free alloy for the application to products for about 3 years from 2000. These days, we have the chance for applying to the mass-production. This project constructed the system for applying the lead free solders on consumer electronic products, which is one of the major products of the LG Electronics. To select the lead free solders with corresponding to the product features, we have passed through the test and applied with Sn-3.0Ag-0.5Cu alloy system to our products, and for the application to the high melting temperature composition, we secured the thermal resistance of the many parts and substrate and optimized the processing conditions. We have operated the temperature cycling test and the high temperature storage test under the standards to confirm the reliability of the products. On these samples, we considered the consequence of our decision by the operating test. For the long life time of the product, we have operated the temperature cycling test at $-45^{\circ}C-+125^{\circ}C$, 1 cycle/hour, 1000 cycles. Also we have tested the tin whisker growth about lead free plating on lead finish. We have analyzed with the SEM, EDS and any other equipment for confirming the failure mode at the joint and the tin whisker growth on lead free finish.

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Enhanced Tumor-targeted Gene Delivery by Immunolipoplexes Conjugated with the Humanized Anti-TAG-72 Fab' Fragments

  • Kim, Keun-Sik;Park, Yong-Serk;Hong, Hyo-Jeong;Kim, Kwang-Pyo;Lee, Kwang-Hyun;Kim, Dong-Eun
    • Bulletin of the Korean Chemical Society
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    • v.33 no.2
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    • pp.651-656
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    • 2012
  • Cationic immunoliposomes were prepared by conjugation of Fab' fragments of the recombinant humanized monoclonal antibody (HuCC49) against tumor-associated glycoprotein (TAG)-72 to sterically unilamella liposomes. The cationic immunoliposomes are composed of cationic lipid (O,O'-dimyristyl-N-lysyl aspartate, DMKD), cholesterol, and 1,2-dipalmitoyl-sn-glycero-3-phosphoethanolamine-N-[maleimide(polyethyleneglycol)$_{2000}$] (DPPE-PEG-maleimide) with a molar ratio of 0.5:0.47:0.03. Plasmid DNA was effectively condensed by addition of transferrin (Tf) during the formation of anti-TAG-72 PEG-immunolipoplexes (PILPs). These anti-TAG-72 PILPs were able to adhere to the surface of TAG-72-overexepressing LS174T human colon cancer cells more effectively than conventional liposomes, thereby facilitating gene delivery in vitro. Furthermore, intravenous administration of the anti-TAG-72 PILPs into the tumor-carrying mice exhibited efficient localization of the reporter gene in the tumor tissues.

Dyeing Properties Wood Dyes by Screen Printing (날염을 이용한 소목의 염색성에 관한 연구)

  • 김은경;장지혜
    • Journal of the Korean Home Economics Association
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    • v.38 no.9
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    • pp.119-130
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    • 2000
  • The purpose of this study was to confirm the possibility of screen printing with Natural dyes. The coloring matter such as sappan wood was used in order to obtain the colorant powder through the processes of extraction, low pressure concentration and the spray dry. After the screen printing on silk and cotton fabrics with colorant, K/S value changes of color and color fastness were measured. The main resets were as follows : 1. The viscosity of printing thickeners of sappan wood powder was about 15,200 cps, and the highest K/S value of the fabrics printed with sappan wood was obtained at 90$\pm$2$\^{C}$ of steaming temperature and 80 minutes of steaming time. 2. For the fabrics printed with sampan wood, adding of urea was not effective, since the more the concentration of urea increased, the more K/S values decreased. 3. For the natural dyes printing, the more the concentration of colorants increased, the more K/S values increased. In general, the K/S values of the printed fabrics were higher when treated with mordants rather than without mordants. Specifically, the λmax sappan wood was 520∼570 nm, and the K/S value was highest when treated with Cu mordant and lowest when treated with Sn. 4. Generally, the color fastness was relatively fair.

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A Study of on Minimizing the Number of V\ulcorner/V\ulcorner Pins in Simultaneous Switching Environment (동시 스위칭 환경에서 V\ulcorner/V\ulcorner Pin 수의 최소화를 위한 연구)

  • Bae, Yun-Jeong;Lee, Yun-Ok;Kim, Jae-Ha;Kim, Byeong-Gi
    • The Transactions of the Korea Information Processing Society
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    • v.7 no.7
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    • pp.2179-2187
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    • 2000
  • This paper provides a heuristic analysis technique which determines an optimal number of V\ulcorner/V\ulcorner pads meeting allowable Simultaneous Switching Noise(SN) budget, early in the design phase. Until now, in determining the number of V\ulcorner/V\ulcorner pads, designers had to simulate packaging models case by case in the design phase or roughly allocate the power/ground pins in an inaccurate way according to typical design rules. However, due to the high density and frequency trends of IC technologies, the V\ulcorner/V\ulcorner pads allocation method can affect an adverse effect on IC operations, which requires more accurate and efficient methods be devised. Thus, this paper proposes an analytic V\ulcorner/V\ulcorner pads calculation method that gives a practical help for packaging designs early in the design phase. The proposed method is applied to a design example of a 1/8x208 pin plastic quad flat package (PQFP) and the results are verified through simulation using HSPICE.

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Manufacturing Process Effect on Fatigue Properties for Copper Thin Film (구리박막의 피로특성에 관한 제조공정의 영향)

  • An, Joong-Hyok;Park, Jun-Hyub;Kim, Yun-Jae
    • Proceedings of the KSME Conference
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    • 2007.05a
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    • pp.1783-1786
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    • 2007
  • The copper film coated by Sn is often used in various applications such as LCD, Mobile Phone and etc. Especially, when the film is used as tape carrier package(TCP) of LCD panel, the film is repeatedly applied by mechanical or(and) thermal stress and then is often failed. Therefore, to guarantee the reliability of the electrical devices using the film, the tensile and fatigue characteristics of the film are important. In this study, to obtain the tensile and fatigue characteristics of the film, the specimen was fabricated by etching process to make a smooth specimen of 2000 ${\mu}m$ width, 8000 ${\mu}m$ length and 15.26 ${\mu}m$ thickness. The 2 kinds of specimen were fabricated by other manufacturing process. These specimens had values of Young's modulus(80.2GPa) lower than literature values(108${\sim}$145GPa) for bulk values, but had high values of the yield and ultimate strength as 317MPa and 437MPa, respectively. And fatigue test of load-control with 20Hz frequency was performed.

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A Kinetic Study of 2-Phenethyl p-Bromobenzenesulfonate with Substituted Pyridines Under High Pressure (II) (2-Phenethyl p-Bromobenzenesulfonate 와 치환 피리딘과의 고압반응 (제 2 보))

  • Soo-Dong Yoh;Kyung-Hwan Park;Sung-Hong Kim;Jong-Hwan Park
    • Journal of the Korean Chemical Society
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    • v.32 no.1
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    • pp.48-52
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    • 1988
  • Kinetics of the reaction of 2-phenethyl p-bromobenzenesulfonate with substituted pyridines in acetonitrile were investigated by an electric conductivity method at 1-2000 bars and $45{\sim}55{\circ}C$. The rates of these reactions were increased with raising temperatures, pressures and by changing electron-donating substitutents in pyridine. When raising pressure the Hammett reaction parameter $I{\rho}I$ and Bronsted ${\beta}$ values were increased, and isokinetic temperature observed from isokinetic relations hip between ${\Delta}H^{\neq}$ and TEX>${\Delta}S^{\neq}$ was decreased. These results indicate that the $S_N2$ characters were increased with raising pressure.

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Development and properties of jointed Bi-2223 superconductor tape

  • Kim, Jung-Ho;Ji, Bong-Ki;Park, Hyung-Sang;Kim, Ho-Jin;Oh, Seung-Jin;Kim, Joong-Seok;Joo, Jin-Ho;Nah, Won-Soo
    • 한국초전도학회:학술대회논문집
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    • v.10
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    • pp.298-303
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    • 2000
  • We evaluated the electric properties of Bi-2223 jointed tapes processed by both resistive- and supercondcuting-joint methods. For the resistive-joint, filler materials of wood metal, Pb/Sn, In, and silver paste were used, whereas, for the superconductive-joint, the lap joint method were used. In the resistive-joint tape, it was observed that the electrical properties such as current transport property, n-value, and contact resistance of the tape were significantly related to the resistivity of filler materials. On the other hand, in the superconducting-joint tape, the current transport property was dependent on the uniaxial pressure. Specifically, the current transport property varied 50 to 80% with uniaxial pressure, probably due to the irregular microstructure in the transition region.

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A clinico-statistical study of soft tissue changes of upper lip & nose following Le Fort I maxillary movement (Le Fort I 상악골이동술 후 상순과 비부의 연조직 변화에 대한 임상통계학적 연구)

  • Park, Jong-Oh;Lee, Sang-Chull
    • Maxillofacial Plastic and Reconstructive Surgery
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    • v.22 no.3
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    • pp.310-318
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    • 2000
  • The purpose of this study was to assess the soft tissue changes of upper lip & nose using 38 patients who treated with Le Fort I osteotomy for the correction of dentofacial deformities. Patients were devided into three groups. One was advancement group of maxilla(Group I, N=14), another was impaction group of maxilla(Group II, N=12) and the other was combination group(advancement & impaction)(Group III, N=12). Preop. and 1 month postop. (T1), preop. and 6 months postop.(T2) were analyzed and compared. The results obtained were as follows : 1. The upper lip thickness(UL-VP) moved anteriorly approximately 62% of the horizontal maxillary change and this was significant in the advancement group(Group I) 2. The upper lip length(Stm-Sn) and the lower border of upper lip(Stm) moved superiorly 25%, 40% of the maxillary impaction group(Group II) (P<0.05) 3. There was significancy in the upper lip thicness(UL-VP) approximately 56% of the combination group(Group III) (P<0.05) 4. The nasolabial angle decreased in all groups, but there were no significancy.

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