• 한국세라믹학회지
• /
• 제32권9호
• /
• pp.1009-1018
• /
• 1995

(Ti.Si)C composite powders were synthesized by SHS method using microwave energy. Compositional and structural characterization of the powder were carried out by using scanning electron microscopy and X-ray diffraction. The average particle size of the synthesized (Ti.Si)C composite powders was smaller than that of the starting materials. From the results of the temperature profile, combustion temperature and velocity were decreased with increasing Si molar ratio. With increasing C molar ratio combustion temperature and velocity did not change. (Ti.Si)C composite was sintered at 185$0^{\circ}C$ for 60 min by using hot-pressing with 30 MPa. The best properties were obtained from the sintered specimen whose composition was 1 : 1 : 1.9 molar ratio of Ti : Si : C. The sintering density, flexural strength and vickers hardness of the sintered body were 4.71 g/㎤, 423 MPa and 21 GPa, respectively.

• 한국세라믹학회:학술대회논문집
• /
• 한국세라믹학회 2004년도 추계총회 및 연구발표회 초록집
• /
• pp.97.2-97.2
• /
• 2004

• 한국재료학회지
• /
• 제18권3호
• /
• pp.153-158
• /
• 2008

Fe-aluminides have the potential to replace many types of stainless steels that are currently used in structural applications. Once commercialized, it is expected that they will be twice as strong as stainless steels with higher corrosion resistance at high temperatures, while their average production cost will be approximately 10% of that of stainless steels. Self-propagating, high-temperature Synthesis (SHS) has been used to produce intermetallic and ceramic compounds from reactions between elemental constituents. The driving force for the SHS is the high thermodynamic stability during the formation of the intermetallic compound. Therefore, the advantages of the SHS method include a higher purity of the products, low energy requirements and the relative simplicity of the process. In this work, a Fe-aluminide intermetallic compound was formed from high-purity elemental Fe and Al foils via a SHS reaction in a hot press. The formation of iron aluminides at the interface between the Fe and Al foil was observed to be controlled by the temperature, pressure and heating rate. Particularly, the heating rate plays the most important role in the formation of the intermetallic compound during the SHS reaction. According to a DSC analysis, a SHS reaction appeared at two different temperatures below and above the metaling point of Al. It was also observed that the SHS reaction temperatures increased as the heating rate increased. A fully dense, well-bonded intermetallic composite sheet with a thickness of $700\;{\mu}m$ was formed by a heat treatment at $665^{\circ}C$ for 15 hours after a SHS reaction of alternatively layered 10 Fe and 9 Al foils. The phases and microstructures of the intermetallic composite sheets were confirmed by EPMA and XRD analyses.

• Steel and Composite Structures
• /
• 제24권5호
• /
• pp.561-568
• /
• 2017

Steel frames are widely used in steel structures. Exiting steel structures may be needed to strengthen for various reasons. Carbon Fiber Reinforced Polymers (CFRP) is one of the materials that are used to strengthen steel structures. Most studies on strengthening steel structures have been done on beams and steel columns. No independent study, to the researcher's knowledge, has studied the effect of CFRP strengthening on steel frames. This study explored the use of CFRP composite on retrofitting square hollow section (SHS) steel frames, using numerical investigations. Ten Finite Element (FE) models, which were strengthened with CFRP sheets, were analyzed under different coverage length, number of layers, and location of CFRP composite. One FE model without strengthening was analyzed as a control FE model to determine the increase of the ultimate load in the strengthened steel frames. ANSYS software was used to analyze the SHS steel frames. The results showed that the coverage length and the number of layers of CFRP composite have a significant effect on increasing the ultimate load of the SHS steel frames. The results also showed that the location of CFRP composite had no similar effect on increasing the ultimate load and the amount of mid span deflection of the SHS steel frames.

• 대한간호학회지
• /
• 제26권3호
• /
• pp.591-604
• /
• 1996

The surgical hand scrub (SHS) is the single most important procedure in the prevention of post-operative wound infections and yet it remains the most violated of all infection control procedures. The purpose of this study was to gain an overview of SHS habits in operative th atre personnel and to determine knowledge and attitudes to identify whether there is a need for improvement. The subjects for this study included 79 doctors and 94 nurses working in the operative th atres of four hospitals in Incheon City and Kyungki Province. Related data were collected from July 25 to August 10, 1995 by the author. The data were analyzed using descriptive stat-istics and Chi-squre test. The results of the study are summarized as follows : 1. Nurses felt that they conducted SHS for a longer period of time than doctors did(X=20.1, P=.005). 2. Nurses and doctors had some knowledge of slip-ping rings off fingers and the length of nails, but they lacked knowledge on the duration of SHS, handwashing after an operation and on manicure. 3. There were many reasons given for insufficient SHS included : 1) because they were so busy (38%). 2) brushes were too harsh(19.7%). 3) operations were very simple(18.7%). 4) surgical latex gloves provide functional barrier(11.6%). 5) SHSs were troublesome(7.4%) 6) there were no clocks near the sinks(2.5%) and 7) the operative patients were administered antibiotics after operartion(2.1%). 4. Most of nurses and doctors considered SHS to be important in prevention against post operative infections. 5. Nurses were found to do a thorough SHS, but residents were found to neglect SHS. 6. Considering prevention against postoperative infections, most nurses and doctors considered aseptic techniques, environment-sanitary management and SHS more important than the use of antibiotics, the resistance of patients or the method of operation. 7. Half of the nurses and doctors(54.3%) considered surgical latex gloves to function well as a barrier. 8. Half of the nurses (56.4%) and doctors(51.9%) learned SHS as part of the curriculum in their school education and the rest(nurses : 95.7%, doctors : 74.7%) learned SHS as part of their In Service Education. In conclusion, these findings suggest a need to develop an educational program on surgical hand scrub and hospital infection control for surgical personnels, to install clocks near the hand scrub sinks, to consider a violation report for negligent surgical hand scrubs, and to develop a soft brush for hand scrubs in order to increase performance of the surgical hand scrub.

• Structural Engineering and Mechanics
• /
• 제66권4호
• /
• pp.439-444
• /
• 2018

This paper presents a numerical study on the behavior of continuous hollow steel beam strengthened using carbon fiber reinforced polymers (CFRP). Most previous studies on the CFRP strengthening of steel beams have been carried out on the steel beams with simple boundary conditions. No independent study, to the researcher's knowledge, has studied on the CFRP strengthening of square hollow section (SHS) continuous steel beam. However, this study explored the effect of the use of adhesively bonded CFRP flexible sheets on the behavior of the continuous SHS steel beams. Finite Element Method (FEM) has been employed for modeling. Eleven specimens, ten of which were strengthened using CFRP sheets, were analyzed under different coverage length, the number of layers, and the location of CFRP composite. ANSYS software was used to analyze the SHS steel beams. The results showed that the coverage length, the number of layers, and the location of CFRP composite are effective in increasing the ultimate load capacity of the continuous SHS steel beams. Application of CFRP composite also caused the ductility increase some strengthened specimens.

• 한국세라믹학회지
• /
• 제32권1호
• /
• pp.11-16
• /
• 1995

High reaction heat evolved from the oxidation of Al was used to synthesize SiC, which might be difficult to be formed by SHS. Al2O3-SiC composite powder was easily manufactured using KNO3 as an ignition and reaction catalyst. Unreacted Si and C were observed after reaction dependent upon the composition of starting powders, reaction atmosphere and relative densities of compacted bodies. The unreacted carbon could be removed by calcining at $600^{\circ}C$ and the remaining Si could be removed by dissolving in NaOH solution. The final powder particles were smaller than 1${\mu}{\textrm}{m}$ in size.

• 한국세라믹학회지
• /
• 제32권8호
• /
• pp.865-872
• /
• 1995

Ultra-fine $\beta$-SiC powders were fabricated by self-propagating high temperature synthesis process (SHS) using microwave oven. The flexural strength, fracture toughness, and hardness of hot pressed sample at 200$0^{\circ}C$ for 60 min using synthesized SiC powders, which had 2 wt% of Al2O3 and 2.5 wt% of B4C content, showed 438 MPa, 4.15MPa.m1/2 and 28 GPa, respectively. The highest strength, fracture toughness, and hardness of composites containing 4wt% of Al2O3, which had highest relative density of 99.9%, showed 458 MPa, 4.6MPa.m1/2 and 36.2 GPa, respectively.

• 한국결정학회지
• /
• 제9권1호
• /
• pp.44-47
• /
• 1998

가정용 2.45GHz 마이크로파 오븐을 사용하여 A1 금속분말과 SiO2 분말간에 SHS방법에 의하여 산화/환원 반응을 통한 Al2O3 분말과 Si분말간의 복합체를 얻을 수 있었다. 분말간의 반응을 일으키기 위한 온도까지 승온시키기 위하여는 SiC 분말을 susceptor로 이용한 마이크로파 복합가열(Microwave Hybrid Heating)방법을 사용하여 분당 100℃의 승온 속도로 가열하였으며 반응은 850℃ 근처에서 일어났으며 가열 속도는 반응이 시작되면서 분당 200℃ 이상의 온도상승이 일어나면서 원하는 반응을 얻을 수 있었다.

• 한국음향학회:학술대회논문집
• /
• 한국음향학회 2000년도 학술발표대회 논문집 제19권 2호
• /
• pp.141-144
• /
• 2000

본 논문에서는 악기음의 음고 추정을 위해 많이 사용되어지는 것으로 알려진 SHS 방법과 P&G 방법의 조합 및 개선을 통하여 좀더 신뢰도가 높은 음고 추정 방법을 제안한다 P&G 방법의 경우 잡음에 의한 주파수 조합의 오염에 민감한 단점이 있는데 주파수 조합을 선택함에 있어 SHS 방법을 사용하여 잡음에 의한 주파수 조합의 오염을 비교적 무시할 만한 수준으로 낮출 수 있었다. 또한 P&G 방법에 있어 배음 행렬 개념을 도입하여 음고 추정시 가장 빈번히 발생하는 오류인 옥타브 에러(octave error)를 최소화하였다. 또한 본 알고리즘을 여러 악기 음에 적용한 결과, 기존 방법에 비해 더 나은 성능을 보였다.