• 한국건축시공학회지
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• 제17권5호
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• pp.437-444
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• 2017

개량 아스팔트 방수시트 위에 폴리 우레탄 도막방수재가 도포되는 복합방수공법의 경우 시공성 향상을 위하여 도막 방수재에 유기용제를 희석해 사용하고 있지만, 유기용제가 폴리 우레탄 도막방수재의 완전 경화 전에 전부 휘발되지 못하고 시트재와 도막재 사이에 잔류하게 되고 이는 아스팔트 층을 융해시켜 방수층 손상 및 누수문제를 발생시켰다. 이에 용제에 의한 융해 문제를 개선하기 위해 내용제성이 강한 PA 필름을 개량 아스팔트 시트에 코팅(적층)하였고, 그 결과 융해에 대한 안전성을 육안을 관찰하였고, SEM 분석, EDX 분석을 통하여 PA 필름에 대한 내용제성을 정량적으로 확인하였다.

• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2010년도 춘계학술대회 논문집
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• pp.642-643
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• 2010

• 한국대기환경학회:학술대회논문집
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• 한국대기환경학회 2008년도 춘계학술대회 논문집
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• pp.144-145
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• 2008

• 한국환경과학회지
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• 제26권12호
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• pp.1333-1339
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• 2017

Coal-fired power plants emit various Particulate Matter(PM) at coal storage pile and ash landfill as well as the stack, and affect the surrounding environment. Field Emission Scanning Electron Microscopy and Energy Dispersive X-ray analyzer(FE-SEM/EDX) were used to develop identification factor and the physico-chemical analysis of PM emitted from a power plant. In this study, three samples of pulverized coal, bottom ash, and fly ash were analyzed. The pulverized coal was spherical particles in shape and the chemical composition of C-O-Si-Al and C/Si and C/Al ratios were 200~300 on average. The bottom ash was spherical or non-spherical particles in shape, chemical composition was O-C-Si-Al-Fe-Ca and C/Si and C/Al ratios were $4.3{\pm}4.6$ and $8.8{\pm}10.0$. The fly ash was spherical particles in shape, chemical composition was O-Si-Ai-C-Fe-Ca and C/Si and C/Al ratios were $0.5{\pm}0.2$ and $0.8{\pm}0.5$.

• 분석과학
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• 제23권3호
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• pp.322-329
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• 2010

총기사고에서 용의자 식별의 기초자료로 활용하기 위하여 3가지 유형의 한국형 총기인 K1A 기관단총, K2 소총, K5 권총의 뇌관화약잔사(Primer GSR)를 SEM-EDX로 분석하였다. 실내사격장에서 각 1발씩 3회 사격하여 얻은 뇌관화약잔사의 형태, 크기, 입자수 그리고 성분분석을 통한 각 입자의 원소 함량비율을 확인하였다. 뇌관화약잔사 입자는 대부분 Ba>>Pb>Sb의 함량비율을 갖고 있었지만 특정 형태의 입자에서는 Sb>Pb>Ba 혹은 Pb>Sb>Ba 등 Ba원소보다 Sb원소의 함량이 많게 나타난 입자가 발견되었다. 원소 성분비율이 차이가 나는 각 입자들을 통계처리 한 결과 사용된 탄의 종류에 따라 5.56 mm 탄을 사용한 K1A, K2 소총에서보다 9 mm 탄을 사용하는 K5권총에서 Sb원소가 Ba원소보다 함량비율이 큰 입자의 수가 3~8배 많은 것으로 확인되어 소총과 권총을 구분할 수 있었다. 또한 입자의 크기와 입자의 수에서도 역시 구분이 가능함을 확인할 수 있었다.

• 한국대기환경학회지
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• 제23권6호
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• pp.718-726
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• 2007

There are many varieties of asbestos: chrysotile, crocidolite, amosite, tremolite, actinolite, and anthophylite. These are widely used in construction materials, brake lining, textile, and so on. Even though non-asbestos fibers such as glassfiber and rockwool have manufactured because asbestos causes asbestosis, lung cancer, mesothelioma, etc., some bad effects of non-asbestos have been also reported. PCM (phase contrast microscopy) and PLM (polarized light microscopy) have been used to qualitatively analyze asbestoses. These techniques have serious drawbacks when identifying and separating various asbestoses. Recently scanning electron microscopy (SEM) equipped with energy dispersive X-ray analysis (EDX) has been known as an useful tool to analyze airborne particle since it provides physical and chemical information simultaneously. The purpose of the study was to classify both asbestos and non-asbestos fibers and finally to develop their source profiles by using the SEM/EDX. The source profiles characterized by 6 different types of asbestos fibers and 2 types of non-asbestos fibers had been developed by analyzing a total of 380 fibers. Analytical parameters used in this study were length, width, aspect ratio, and shape as physical information, and Na, Mg, Al, Si, K, Ca, Cr, Mn, Fe, and Cu as chemical information. All the parameters were intensively reviewed.

• Asian Journal of Atmospheric Environment
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• 제7권1호
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• pp.1-7
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• 2013

To establish the method for investigating the behavior of aerosol particles deposited on the leaf surface against fog water under natural conditions, scanning electron microscopy with energy-dispersive X-ray (SEM-EDX) analysis and wash water analysis by ion chromatography after the washing treatment were performed using leaves of white birch collected from low part of the tree crown and the top of the tree in Sapporo City, Hokkaido, northern Japan. Each of collected leaves was divided into two parts according to the treatment performed: leaf surface (adaxial side) was 1) untreated, and 2) washed with deionized water with a pipette. In untreated samples, many particles of various shapes, including soil particles and organic debris, were deposited on the surface. Particles containing S were found on the surface of samples collected from only low part of the tree crown. After the washing treatment, SEM-EDX analysis revealed that soil particles and particles containing S had been washed off with water, although some particles such as soil particles and organic debris still remained on the leaf surface. The major anion such as $SO{_4}^{2-}$ was detected in wash water of all samples, although the peak of S in X-ray spectra was not detected from samples collected at top of the tree. The combination of SEM-EDX analysis with wash water analysis indicated that $SO{_4}^{2-}$ was deposited on the leaf surface in dissolved state and/or in state of submicron particles. These results suggested that fog water could remove soil particles and particles containing S and $SO{_4}^{2-}$ from the leaf surfaces, but not all particles. There was no difference in sampling position in the tree crown. Our study suggested that combination with SEM-EDX analysis and wash water analysis would be effective for investigation of the behavior of particles on the leaf surface against fog water.

• 한국환경과학회지
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• 제12권4호
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• pp.469-476
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• 2003

In order to examine the pre-treatment effect of crab shell en Pb$^{2+}$ removal by crab shell in aqueous solution, acid and alkali pre-treated crab shell were used. Electron microscopy techniques such as TEM (transmission electron microscopy) and SEM (scanning electron microscopy), and EDX (energy dispersive X-ray) and FTIR (Fourier transform infrared) spectrometry techniques were used to investigate the process of Pb$^{2+}$ removal by acid and alkali pre-treated crab shell. The Pb$^{2+}$ removal by acid pre-treated crab shell was much lower than that by untreated crab shell because of the decrease of CaCO$_3$ from the crab shell. However, the Pb$^{2+}$removal by alkali pre-treated crab shell increased compared to that by untreated crab shell. The results were confirmed by TEM, SEM, EDX and FTIR.nd FTIR.

• 환경위생공학
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• 제20권3호
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• pp.17-26
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• 2005

Many researches were focused on the data which obtained from chemical bulk analysis. It is difficult to evaluate source contribution by wet type chemical bulk analysis. In this study, we have reviewed the characterization of individual particle for source identification. We analyzed by SEM/EDX methods. We have obtained average geometric particle diameter measured by optical diameter which were resulted from SEM/EDX image scan, representative physical diameter of individual particle was $3.38\;{\mu}m\;in\;A,\;3.67\;{\mu}m\;in\;B$. In the result of image analysis at each spots particles, both samples non-sphere shapes, C-rich particles. In consequence of chemical analysis of individual particle, each sampling sites some elements.

• 한국산학기술학회논문지
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• 제12권3호
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• pp.1070-1077
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• 2011

본 논문은 초음파 가공에 의한 용착성을 가공조건의 영향에 관하여 나타내었다. 한파장 혼의 최적화를 이용한 Ni-Cu 이종금속 박판의 용착성 평가는 초음파 가공 방법을 이용하여 확인된다. 초음파 가공변수 설정에 따른 인장시험을 통한 최적의 용착조건을 제시하였으며 SEM 사진과 EDX-ray 분석에 의한 용착성을 평가하였다. 실험적 연구는 초음파 가공 후 인장강도의 측정, SEM사진 분석으로 수행된다. 또한 가공시간, 가압력, 진폭의 가공변수들은 본 연구에 적용되었다.