• 제목/요약/키워드: SEM study

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열전자방사형 주사전자 현미경 전자광학계의 유한요소해석 (Finite Element Analysis for Electron Optical System of a Thermionic SEM)

  • 박근;정현우;김동환;장동영
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.1288-1293
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    • 2007
  • The present study covers the design and analysis of a thermionic scanning electron microscope (SEM) column. The SEM column contains an electron optical system in which electrons are emitted and moved to form a focused beam, and this generates secondary electrons from the specimen surfaces, eventually making an image. The electron optical system mainly consists of a thermionic electron gun as the beam source, the lens system, the electron control unit, and the vacuum unit. In the design process, the dimension and capacity of the SEM components need to be optimally determined with the aid of finite element analyses. Considering the geometry of the filament, a three-dimensional (3D) finite element analysis is utilized. Through the analysis, the beam emission characteristics and relevant trajectories are predicted from which a systematic design of the electron optical system is enabled. The validity of the proposed 3D analysis is also discussed by comparing the directional beam spot radius. As a result, a prototype of a thermionic SEM is successfully developed with a relatively short time and low investment costs, which proves the adoptability of the proposed 3D analysis.

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FE-SEM을 이용한 도공층 공극 구조 분석 연구 (Study on analysis of coating layer by FE-SEM image)

  • 김진우;이학래;윤혜정
    • 한국펄프종이공학회:학술대회논문집
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    • 한국펄프종이공학회 2010년도 춘계학술발표회 논문집
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    • pp.67-67
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    • 2010
  • 이미지를 이용한 도공층 구조 분석은 도공층의 실제 Morphology를 분석하여 평가하는 방법으로서 최근 세밀한 도공층 구조 분석을 위해 이 방법에 대한 많은 연구가 진행되고 있다. 특히 이러한 방법은 수은압입법(Mercury intrusion)이나 질소흡착법 (Nitrogen adsorption by BJH theory) 등과 같은 기존의 공극 특성 평가 방법과 달리 pore aspect ratio 및 orientation 등과 같은 공극 dimension을 평가할 수 있는 장점이 있다. 이러한 공극 dimension은 size distribution 및 porosity와 더불어 인쇄, 라미네이션 접착 등과 같은 Liquid interfacial 및 침투 측면에서 중요한 요소이기 때문에 이를 평가하기 위한 적합한 방법으로 인식되고 있다. 또, 원지 부분과 도공층 간의 경계를 명확하게 보여주고 Surface와 Cross-section 영역을 구분하여 평가 할 수 있어 더 명확한 평가를 가능하게 한다. 본 연구에서는 이미지 분석을 통해 도공액 구성 조건에 따른 도공층의 공극 구조 특성을 평가 하였고 일부 요소에 대해서는 수은 압입법과 비교 평가하여 이미지 분석법과의 상관성에 대해 고찰 하였다. 본 연구에서 사용된 FE (Field Emission)-SEM은 일반 SEM과 달리 전압에 의한 높은 전기장의 형성을 통해 저 가속 전압으로 이미지를 구현하는 장비로서 본 연구에서는 FE-SEM을 통해 도공층의 세밀한 Morphology와 공극 구조 이미지를 구현할 수 있었다.

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Determination of Absorbed Dose for Gafchromic EBT3 Film Using Texture Analysis of Scanning Electron Microscopy Images: A Feasibility Study

  • So-Yeon Park
    • 한국의학물리학회지:의학물리
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    • 제33권4호
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    • pp.158-163
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    • 2022
  • Purpose: We subjected scanning electron microscopic (SEM) images of the active layer of EBT3 film to texture analysis to determine the dose-response curve. Methods: Uncoated Gafchromic EBT3 films were prepared for direct surface SEM scanning. Absorbed doses of 0-20 Gy were delivered to the film's surface using a 6 MV TrueBeam STx photon beam. The film's surface was scanned using a SEM under 100× and 3,000× magnification. Four textural features (Homogeneity, Correlation, Contrast, and Energy) were calculated based on the gray level co-occurrence matrix (GLCM) using the SEM images corresponding to each dose. We used R-square to evaluate the linear relationship between delivered doses and textural features of the film's surface. Results: Correlation resulted in higher linearity and dose-response curve sensitivity than Homogeneity, Contrast, or Energy. The R-square value was 0.964 for correlation using 3,000× magnified SEM images with 9-pixel offsets. Dose verification was used to determine the difference between the prescribed and measured doses for 0, 5, 10, 15, and 20 Gy as 0.09, 1.96, -2.29, 0.17, and 0.08 Gy, respectively. Conclusions: Texture analysis can be used to accurately convert microscopic structural changes to the EBT3 film's surface into absorbed doses. Our proposed method is feasible and may improve the accuracy of film dosimetry used to protect patients from excess radiation exposure.

The Exploratory Research on Object Activity Service Evaluation Model(OA-SEM) - The Application of Retail Industry

  • Lee, Seung-Chang;Suh, Eung-Kyo;Park, Hoon-Sung
    • 유통과학연구
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    • 제14권8호
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    • pp.45-50
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    • 2016
  • Purpose - This study aimed to develop a new practical and universally applicable service quality model by improving the service quality measurement model proposed by many previous studies. Research design, data, and methodology - An in-depth analysis on what influences such service quality model had on the improvement effect of service quality, and Service Evaluation Model("SEM"), which was revised from the existing service quality measurement model, was developed. The model is divided into the two integrative categories: First, activity, that is the group of service-related activities. Next is item, the group of service-related objects. The level of service is evaluated for each category via survey questionnaire on service level evaluation. Based on the model, SEM has visibility by structuring the whole service industry. Results - For the application of the new service quality model, this study attempted to examine the appropriateness of the newly proposed service quality model by applying it to retail service field. Conclusions - As a result, the proposed service model would be a useful and applicable service quality measurement model required by many organizations. Service company can set up self check service levels. Through these results, they can look for the ways to provide better services to customers. Service users can ensure the objectivity of business plan based upon SEM.

덴탈 바이오필름에서 분리한 세균의 주사전자현미경적 관찰 및 동정 (Identification and morphology of scanning electron microscopy(sem) of bacteria isolated from dental biofilm)

  • 장계원
    • 한국치위생학회지
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    • 제8권4호
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    • pp.241-250
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    • 2008
  • In this study, specimens such as tongue, supragingival and subgingival biofilm were taken from total 20 scaling subjects who visited the oral prophylaxis practice lab at department of dental hygienics, J Health College in order to observe bacterial distributions and morphology using scanning electron microscopy(sem). as a result, this study came to the following conclusions: 1. According to observation of tongue, supragingival and subgingival biofilm through sem, it is found that there are round colonies of gram-positive cocci and gram-negative bacilli on blood agar medium. 2. The observation of bacterial morphology on dental biofilm through sem, cocci in chain cocci in cluster and bacillus(rod) respectively. 3. For tongue biofilm, it is found that a variety of bacterial species are detected, such as Granulicatolla adiacens(1), Gemella morbillorum(3), Streptococcus mitis(2), Streptococcus sanguinis(1), Aerococcus viridans (2), Streptococcus equinus(1), Leuconostoc spp.(1), Gemella haemolysans (1) and Lactococcus lactis spp.(1) respectively. 4. For supragingival biofilm, it is found that a variety of bacterial species detected, such as Aerococcus viridans(1), Gemella haemolysans(2), Leuconostoc spp.(2), Gemella morbillorum(1) and Pseudomonas fluoescens (1) respectively. 5. For subgingival biofilm, it is found that a variety of bacterial species detected, such as Leuconostoc spp.(1), Staphylococcus lugdunensis(1) and Streptococcus salivarius(1) respectively.

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An Optimized Methodology to Observe Internal Microstructures of Aloe vera by Cryo-Scanning Electron Microscope

  • Choi, Yoon Mi;Shin, Da Hye;Kim, Chong-Hyeak
    • Applied Microscopy
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    • 제46권2호
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    • pp.76-82
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    • 2016
  • Aloe vera has been used in the pharmaceutical, food and cosmetic industry for its therapeutic properties. However, there are not many current studies on the microstructure of A. vera compared to studies on the chemical constituents and health efficacy of A. vera. Therefore, we compared the morphology of an A. vera leaf using an optical microscope, a conventional scanning electron microscope (SEM) and a cryo-SEM. Especially, this study focused on observing the gel in the inner leaf of A. vera, which is challenging using standard imaging techniques. We found that cryo-SEM is most suitable method for the observation of highly hydrated biomaterials such as A. vera without removing moisture in samples. In addition, we found the optimal analytical conditions of cryo-SEM. The sublimation conditions of $-100^{\circ}C$ and 10 minutes possibly enable the surface of the inner leaf of A. vera to be observed in their "near life-like" state with retaining moisture. The experiment was repeated with A. arborescens and A. saponaria to confirm the feasibility of the conditions. The results of this study can be applied towards the basic research of aloe and further extend previous knowledge about the surface structures of the various succulent plants.

유헬스에서의 확장된 기술수용모형 적용 - 자기효능의 영향 중심 (Application of Extended Technology Acceptance Model in u-Health - Focused on the Effect of Self-Efficacy)

  • 김민철
    • 한국정보통신학회논문지
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    • 제18권12호
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    • pp.2989-2996
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    • 2014
  • 본 논문은 스마트 폰 기반의 유비쿼터스 헬스 시스템의 수용 여부에 영향을 미치는 건강 자기효능감 (health self-efficacy) 및 기술 자기효능감 (technology self-efficacy) 요인들의 영향 정도를 확장된 기술수용모형(TAM)을 통하여 분석하는데 목표를 두고 있다. 본 논문에서는 표본의 크기를 고려하여 제시된 연구 모형을 검증하기 위하여 PLS-SEM 방법론을 적용하였다. 분석 결과, 제시된 연구모형의 적합성을 확인하였고, 각 경로 계수의 통계적 유의성 또한 분석이 되었다. 결국, 기술 자기효능감인 스마트 폰 기기의 사용에 대한 쉬운 접근성만 높일 수만 있다면, 사용 의도의 가능성이 높아짐을 확인할 수 있었다.

IT중소기업의 리더십과 임파워먼트에서 MMR과 SEM 검증방법에 따른 팔로워십 조절효과분석 (The moderating effects Analysis of followership according to the MMR & SEM methods to leadership and empowerment in IT SMEs)

  • 이영신;박재성
    • 디지털산업정보학회논문지
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    • 제8권3호
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    • pp.199-212
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    • 2012
  • This study focuses on the influence of followership on leadership and empowerment, and to verify based on the control variables taken in IT SME's to enhance competitiveness through innovation and improvement plan that have been taken. Because there can be a lot of information to be taken, the laws of Moderated Regression Multiple analysis(MMR) were used. Amos, due to the moderating effect of Structural Equation Modeling(SEM) has been employed to re-verify the results seen with Moderated Regression Multiple analysis. The paper focuses on determining whether transformational leadership or transactional leadership is effective as shown by the levels of empowerment derived from these two types of leadership under study. As a result, both the Moderated Regression Multiple analysis and structural equation model searched information on transformational and followership for empowerment having moderating effects. In the Moderated Regression Multiple analysis, results showed that empowerment for leadership in business in the regulation of followership role appeared not to be seen. However, using the structural equation modeling, moderating effects have been found.

울산퇴적점토의 광물조성 특성 (Mineralogical Properties of the Sedimental Clay in Ulsan)

  • 민덕기;황광모;강문기;박종규
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2000년도 봄 학술발표회 논문집
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    • pp.567-574
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    • 2000
  • The purpose of this study is to examine mineralogical properties of the soft clay that is distributed widely in Samsan area, Ulsan. XRD analysis were examined to find the quantities of the clay minerals. And XRF, SEM and EDX analysis were also examined to investigate the chemical compositions and the structures of the clay. The properties of the samples from 2 sites in Samsan area were that the minerals of the clay were illite, kaolinite, chlorite, smectite and etc.. The plenty of illite has 38 to 53% of content in whole study area. And kaolinite had 18 to 30%, chlorite had 15 to 25%, and smectite had 4 to 12% of content, respectively. The results of SEM observation showed that appearances of Ulsan clay were sheet, plannar or needle form. Ulsan clay included the salt crystal of cubic and the foraminifera, which were related with the content of organ.

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미끄럼반복마찰의 직접관찰에 의한 TiN피막의 허용응력에 관한 연구 (A Study on the Allowable Stress of TiN Coating During Repeated Sliding Condition by In-situ System)

  • 문봉호
    • Tribology and Lubricants
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    • 제27권3호
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    • pp.147-155
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    • 2011
  • The ceramic coatings are excellent materials of cutting tools and sliding parts. To evaluate the wear characteristics of very thin ceramic coated layer, it is very important to investigate its wear process microscopically. An effective method for investigating the wear of a thin layer is the observation of wear process in microscopic detail using in-situ system. In this study, using the SEM Tribosystem as in-situ system, the microscopic wear mode of TiN coatings was investigated in repeated sliding. As results, four modes were observed for TiN coatings: Ploughing, powder formation, flake formation and coating delimitation. The observation of the microscopic wear by in-situ system can clarify the allowable stress of TiN coating.