• Title/Summary/Keyword: SEM study

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Physico-chemical characterization of individual particles emitted from the air pollution point sources (대기 점오염원에서 배출되는 개별입자상물질의 물리화학적 특성)

  • Park Jeong-Ho;Suh Jeong-Min
    • Journal of Environmental Science International
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    • v.14 no.8
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    • pp.761-770
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    • 2005
  • Scanning electron microscopy / energy dispersive X-ray analyzer(SEM/EDX) has played an important role for evaluation the source of atmospheric particle because it is a powerful tool for characterizing individual particles. The SEM/EDX system provides various physical parameters like optical diameter, as well as chemical information for a particle-by-particle basis. The purpose of the study was to classify individual particle emitted from the point sources based on clustering analysis and physico-chemical analysis by SEM/EDX. The total of 490 individual particle were analyzed at 8 point sources including coal-fired power plant, incinerator, H-C oil boiler, and metal manufacturing industry. The main components were Si and AI in the coal-fired power plant, Cl and Na in the domestic waste Incinerator, S in the H-C oil boiler and S and Fe in the metal manufactory industry, respectively.

A Study on the design and implementation of serial communication using only one pin (단일 핀을 이용한 직렬 통신 설계 및 구현에 관한 연구)

  • Cha, Jeong-tae;Park, Sang-bong;Heo, Jeong-hwa;Jeong, Dae-seung
    • Proceedings of the Korea Information Processing Society Conference
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    • 2015.10a
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    • pp.372-374
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    • 2015
  • 최근 가전제품, 모바일 장비, 웨어러블 컴퓨터 등의 IoT 분야에서 센서 정보를 주고 받는 직렬 통신 방식이 사용된다. 기존의 SPI와 I2C 직렬 통신 방식은 클럭과 데이터 2개의 핀을 사용하여 비교적 빠른 속도로 데이터를 전송하는 방식이다. 사용되는 사물들이 점차 작아지고, 데이터 전송 정보의 양이 적어지면서 전송 속도보다는 하드웨어의 단순화가 중요한 설계요소가 되는 응용분야가 늘어나고 있다. 본 논문에서는 단일 핀을 사용하여, 데이터를 직렬로 송 수신하는 회로를 설계하고 FPGA로 구현하였다. 제안된 단일 핀 직렬 통신 프로토콜은 적은 양의 데이터를 저속으로 통신하는 IoT 제품에 적합하다.

Analysis of Deposited Dust Particles using SEM/EDX (SEM/EDX 분석법을 이용한 침착먼지에 대한 분석사례)

  • Ha, Eun-Ji;Park, Jeong-Ho
    • Journal of Environmental Science International
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    • v.30 no.3
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    • pp.279-287
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    • 2021
  • In this study, the composition and morphology of deposited dust particles with size ranging from a few to tens ㎛ were investigated using SEM/EDX (scanning electron microscopy with energy dispersive x-ray spectrometer). Then deposited dust particles were classified into 8 groups: quartz, aluminosilicates, ca-rich, Fe/Ti oxide, carbon-rich, industrial particle, Fe-rich, and biogenic particle. The sources of deposited dust were high in the order of aluminosilicates 41% > biogenic 18% > Fe-rich 11% > quartz and C-rich 8% > industrial 7% > Fe/Ti oxide 5% > Ca-rich 1%. In particular, the ratio of biogenic particles was relatively high due to influence of pollen. The ratio of carbon-rich was 11% at YM site, 10% at MD site, and 4% at MO site, and the site close to the large emission source was high.

Analysis of composition and microstructure of diatom frustules in mud on the coast of Boryeong- city, South Korea

  • Mi Kyung Bok;Chung Hwa Chin;Hee Jung Choi;Ju Hyun Ham;Byung Soo Chang
    • Applied Microscopy
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    • v.52
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    • pp.12.1-12.8
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    • 2022
  • The microstructure of diatom frustules found in mud sediments along the coast of Boryeong- city, South Korea, was observed using a scanning electron microscopy (SEM), and the constituent elements of diatoms were analyzed using energy-dispersive X-ray spectroscopy (EDS). Diatom frustules and clay minerals were present in the SEM images of the mud powder. High-magnification SEM images revealed that the surface of the frustules contained identically shaped circular pores, measuring 1 ㎛ in diameter, arranged at regular intervals. This study revealed that the diatom shell fragments in the mud powder ranged in size from 3 to 30 ㎛, with an average thickness of approximately 2.5 ㎛. The elements Si, Al, Fe, K, Na, Mg, and Ti were detected while analyzing the frustule constituents, with Si being the primary component with the highest content.

The Service Recovery Strategies, Customer Satisfaction, Customer Loyalty

  • Kim, Gye-Soo
    • International Journal of Quality Innovation
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    • v.8 no.1
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    • pp.76-86
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    • 2007
  • This paper reports on a study investigating key attributes of service recovery strategies in internet shopping mall. In theses day, service recovery has received important attention in the service operation management literature. Service recovery involves those actions designed to resolve problems, alter negative attitudes of dissatisfied consumers and to ultimately retain these customers. The study examined that service recovery strategies (apology, compensation) impact on the customer satisfaction. And customer satisfaction impacts on customer loyalty with SEM (Structural Equation Modeling). This study can be used a strategic implication for internet shopping mall managers to develop successful service recovery strategies.

Busan Housing Market Dynamics Analysis with ESDA using MATLAB Application (공간적탐색기법을 이용한 부산 주택시장 다이나믹스 분석)

  • Chung, Kyoun-Sup
    • The Journal of the Korea Contents Association
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    • v.12 no.2
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    • pp.461-471
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    • 2012
  • The purpose of this paper is to visualize the housing market dynamics with ESDA (Exploratory Spatial Data Analysis) using MATLAB toolbox, in terms of the modeling housing market dynamics in the Busan Metropolitan City. The data are used the real housing price transaction records in Busan from the first quarter of 2006 to the second quarter of 2009. Hedonic house price model, which is not reflecting spatial autocorrelation, has been a powerful tool in understanding housing market dynamics in urban housing economics. This study considers spatial autocorrelation in order to improve the traditional hedonic model which is based on OLS(Ordinary Least Squares) method. The study is, also, investigated the comparison in terms of $R^2$, Sigma Square(${\sigma}^2$), Likelihood(LR) among spatial econometrics models such as SAR(Spatial Autoregressive Models), SEM(Spatial Errors Models), and SAC(General Spatial Models). The major finding of the study is that the SAR, SEM, SAC are far better than the traditional OLS model, considering the various indicators. In addition, the SEM and the SAC are superior to the SAR.

Evaluations of Microstructure and Hydrogenation Properties on $Mg_2NiH_x$ ($Mg_2NiH_x$ 수소저장합금의 미세결정구조 및 수소화 특성평가)

  • Seok, Song;Shin, Kyung;Kweon, Soon-Yong;Ur, Soon-Chul;Lee, Young-Geun;Hong, Tae-Whan
    • Transactions of the Korean hydrogen and new energy society
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    • v.16 no.3
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    • pp.238-243
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    • 2005
  • Mg and Mg-based alloys are most important hydrogen storage materials. It is a lightweight and low-cost materials with high hydrogen storage capacity. However, the formation of hydride at high temperature, the deterioration effect, the hydriding and dehydriding kinetics are bad factor for application. In this study, Mg and Ni have been produced by hydrogen induced mechanical alloying(HIMA) process. The raw materials, Mg(purity 99.9%) chip and Ni(purity 99.95%) chip was prepared by using a planetary ball mill apparatus(FRITSCH pulverisette 5). The balls to chips mass ratio(BCR) are 30:1. The hydrogen pressure induced 2.0MPa and milling times were 12, 24, 48, 72, 96 hours with a rotating speed of 200rpm. X-ray diffraction(XRD) analysis was made to characterize the crystallite size and misfit strain. The crystallite size measured by laser particle size analysis(PSA). Microstructure changes were investigated by scanning electron microscopy(SEM) and the transmission electron microscopy(TEM). The hydrogen storage properties were evaluated by using an Sivert's type automatic pressure-composition-therm(PCT) apparatus.

Cryo-SEM Methodology of Arabidopsis thaliana Stem Using High-Pressure Freezing (고압동결고정을 이용한 애기장대 줄기의 cryo-SEM 분석법)

  • Choi, Yun-Joung;Lee, Kyung-Hwan;Je, A-Reum;Chae, Hee-Su;Jang, Ji-Hoon;Lee, Eun-Ji;Kweon, Hee-Seok
    • Applied Microscopy
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    • v.42 no.2
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    • pp.111-114
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    • 2012
  • The scanning electron microscopy is an ideal technique for examining plant surface at high resolution. Most hydrate samples, however, must be fix and dehydrate for observation in the scanning electron microscope. Because the microscopes operate under high vacuum, most specimens, especially biological samples, cannot withstand water removal by the vacuum system without morphological distortion. Cryo-techniques can observe in their original morphology and structure without various artifacts from conventional sample preparation. Rapid cooling is the method of choice for preparing plant samples for scanning electron microscopy in a defined physiological state. As one of cryo-technique, high-pressure freezing allows for fixation of native non-pretreated samples up to $200{\mu}M$ thick and 2 mm wide with minimal or no ice crystal damage for the freezing procedure. In this study, we could design to optimize structural preservation and imaging by comparing cryo-SEM and convention SEM preparation, and observe a fine, well preserved Arabidopsis stem's inner ultrastructure using HPF and cryo-SEM. These results would suggest a useful method of cryo-preparation and cryo-SEM for plant tissues, especially intratubule and vacuole rich structure.

Observation of Shrinkage Features of Cross Sectional Surface of Wood by LV-SEM (저진공주사현미경(LV-SEM)을 이용한 목재횡단면의 수축거동관찰)

  • Kang, Chunwon;Matsumura, Junji;Kang, Wook
    • Journal of the Korean Wood Science and Technology
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    • v.36 no.3
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    • pp.17-23
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    • 2008
  • The purpose of this study is to estimate the shrinkage of wood by LV-SEM (Low-Vacuum Scanning Electron Microscope) which can observe wetted wood sample. The shrinkage of small sample specimen by the dehumidification in the specimen chamber was investigated and compared with that of normal wood specimen. The observation of cross sectional surface of wood from wetted condition to dried condition can be achieved in about twenty minutes by means of the dehumidification in the specimen chamber of LV-SEM. The volumetric shrinkage of earlywood was almost the same as that of latewood. The shrinkage of SEM observation specimen was similar to that of normal wood specimen. From the correlation of the shrinkages between SEM observation specimen and normal wood specimen, it is surmised that the shrinkage of wood is more strictly dominated by shrinkage of latewood than that of earlywood.