• 제목/요약/키워드: SEM observation

검색결과 779건 처리시간 0.024초

SEM 내 마이크로 절삭에 의한 초경합금재의 절삭 특성에 관한 연구 (Study on Cutting Characteristics of WC-Co with Micro Cutting in SEM)

  • 허성중
    • 한국정밀공학회지
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    • 제20권10호
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    • pp.74-81
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    • 2003
  • This paper describes that the micro-cutting of WC-Co using PCD (Polycrystalline Diamond) and PcBN (Polycrystalline Cubic Boron Nitride) cutting tools are performed with SEM(Scanning Electron Microscope) direct observation method. The purpose of this study is to present reasonable cutting conditions to obtain precise finished surface and machining efficiency. Summary of the results are shown below: (1) The thrust cutting forces tend to increase more than the principal forces as the depth of cut and the cuttlllg speed are increased preferably on orthogonal microcutting. (2) The tool wear in the flank face was formed larger than that in the rake face on orthogonal micro cutting. (3) The wear appearance for PCD tools is abraded by hard WC particles of the work materials, which lead diamond grain to be detached from the bond.

재습윤제의 적용이 상아질 접착에 미치는 효과 (EFFECT OF A REWETTING AGENT ON DENTIN ADHESION)

  • 조영곤;박일윤;이영곤
    • Restorative Dentistry and Endodontics
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    • 제28권1호
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    • pp.11-22
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    • 2003
  • This study compared the dentin adhesion to composite resin according to air-dry, blot dry, application of rewetting agent on air-dry or blot dry dentin surface by microleakag test and SEM observation. For microleakage test, class V cavity preparations with dentinal margins were prepared on both buccal and lingual surfaces of 40 extracted human molars. For SEM observation, occlusal dentin of 20 extracted human molars were exposed. After etched the dentin, prepared teeth were randomly divided into four groups; D group: air dry for 10-15 sec., B group: blot dry with moist cotton pellet, D-R group: air dry and rewet with Aqua-Prep F for 20 sec., B-R group: blot dry and rewet with Aqua-Prep F for 20 sec. Treated cavities and surfaces were filled or constructed using One-Step adhesives and Aelitefil composite resins. Specimens were stored in distilled water for 24 hours. For microleakage test, the specimens were thermocycled and soaked into 2% methylene blue. The specimens were sectioned longitudinally and evaluated for microleakage under steromicroscope. The data were statistically analysed by Kuskal-Wallis Test, Mann-Whitney and Wilcoxon signed ranked tests. For SEM observation, the specimens were bisectioned mesiodiatally. After decalcified and deproteinized, specimens were observed under SEM. The results of this study were as follows; 1. The microleakges on dentinal margin were the highest in D group compared with B group, D-R group, and B-R group(p<0.05). But there was no significant difference between B group, D-R group and B-R group. 2. D group showed gap and a few resin tags between dentin and composite resin. 3 B group, D-R group, and B-R groups showed close adaptation between dentin and composite resin. It showed that resin rags in B group were numerous and long, in D-R group were few and short, in B-R group were numerous and short or long. 4. Adhesive layer showed in D-R group ($10{\;}\mu\textrm{m}$) and B-R group ($3{\;}\mu\textrm{m}$) In conclusion, use of rewetting agent to dry dentin was efficient to dentin adhesion, also it did not provide reverse effect on blot dry dentin.

페이스트를 이용한 탄소나노튜브의 수직배양법 연구 (Process Development of Aligning Carbon Nanotube from the Paste)

  • 이재걸;문주호;이동구
    • 한국세라믹학회지
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    • 제39권5호
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    • pp.467-472
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    • 2002
  • 다이아몬드 연마 필름(diamond lapping film)으로 긴 탄소나노튜브를 절단하고 이를 Scanning Electron Microscope(SEM)으로 관찰했다. 절단된 탄소나노튜브를 ${\alpha}$-terpineol을 용매로 ethyl cellulose를 바인더로 사용하여 제조한 페이스트를 스크린 프린팅과 주사 사출법으로 유리 기판에 도포하였다. 스크린 프린팅으로 인쇄된 선에 존재하는 절단된 탄소나노튜브를 기판에 대해 수직 배향을 시키기 위하여 사포, 다이아몬드 연마 필름을 사용하여 마찰시키거나 접착성이 있는 테이프를 이용하여 접촉시켰다가 분리 하는 방법을 시도하였다. SEM으로 탄소나노튜브의 배향 특성을 관찰한 결과 주사 사출법과 스크린 프린팅 후 다이아몬드 연마 필름을 사용하여 후처리하는 간편한 방법으로 탄소나노튜브의 우수한 수직배양이 이루어짐을 알 수 있었다.

점토-골재 벽돌 경화에 있어 효소 사용의 효과 (Effect of Enzyme Stabilization on Hardening of Clay-rock Brick)

  • 미티키 바히루;이태식
    • 한국건설순환자원학회논문집
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    • 제5권4호
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    • pp.366-374
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    • 2017
  • 본 연구는 점토와 골재로 구성된 벽돌을 경화하는데 있어 효소 첨가제의 효과를 재료시험과 이미지 프로세싱을 통해 분석하였다. 벽돌의 강도와 밀도 시험에 사용한 벽돌 샘플의 점토/골재 중량비는 70/30, 60/40, 50/50, 40/60, 30/70이였으며, 최대 압축강도와 휨강도는 각각 5MPa와 1.25MPa으로 중량비 60/40에서 발현되었다. 또한 최대 건조단위 중량은 $2.073g/cm^3$으로 중량비 50/50에서 발현되었다. 시험 결과 전반적으로 벽돌의 강도는 효소를 첨가함으로 약 27% 향상되었다. 강도 향상을 위해서는 점토/골재 중량비 60/40, 밀도 향상을 위해서는 점토/골재 중량비 50/50에 효소를 첨가하여 벽돌을 경화하는 것이 효과적인 것으로 확인되었다. 효소 첨가 시 점토-골재 벽돌의 결합구조가 더 치밀해짐을 SEM-EDX 분석과 Matlab을 이용한 이미지 프로세싱을 통해 확인하였으며, 이를 통해 효소가 점토와 골재 간 결합구조를 형성하여 벽돌의 강도와 밀도를 향상시키는 효과가 있는 것으로 판단된다.

침탄처리된 엔진 부품의 미세조직학적 파손원인 분석 (Failure Analysis of the Carburized Engine Parts by Microstructural Observation)

  • 손경숙;이상기;정인상
    • 열처리공학회지
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    • 제18권2호
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    • pp.83-90
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    • 2005
  • Failure cause of the fractured engine parts was analyzed by microstructural observation. These parts were failed far earlier than the expected service life. By the stereoscope and SEM examinations of the fractured surface, the fracture modes have been identified as wear and fatigue failure. From the observation of microstructure and microhardness measurements of the failed gears, the probable cause for failures are internal oxidation during using and retained austenite and carbide networks due to heat-treatment, respectively. These defected structures at near surface contributed to the wear and fatigue failure.

침탄처리된 기어의 미세 조직학적 손상 원인분석 (Failure Analysis of Carburized Gears by Microstructural Observation)

  • 전해동;장성호;김경욱;국연호
    • 열처리공학회지
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    • 제27권4호
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    • pp.191-201
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    • 2014
  • The gear was made of SNC815 case-carburized, quench hardened and tempered steel. The gears were failed far earlier than the expected service life used in the industrial site. Causes of the failed gear were analyzed by microstructure observation. By the SEM and micro structure examinations, the damaged surfaces had been weared and failed by fatigue. Through microscope observation on the damaged surface, it was found that the cause of failure was determined by external overloading and the initial stage of the damage was closely related to complex contact fatigue failure. The overload and contact fatigue contributed to the early failure cause.

울산퇴적점토의 광물조성 특성 (Mineralogical Properties of the Sedimental Clay in Ulsan)

  • 민덕기;황광모;강문기;박종규
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2000년도 봄 학술발표회 논문집
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    • pp.567-574
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    • 2000
  • The purpose of this study is to examine mineralogical properties of the soft clay that is distributed widely in Samsan area, Ulsan. XRD analysis were examined to find the quantities of the clay minerals. And XRF, SEM and EDX analysis were also examined to investigate the chemical compositions and the structures of the clay. The properties of the samples from 2 sites in Samsan area were that the minerals of the clay were illite, kaolinite, chlorite, smectite and etc.. The plenty of illite has 38 to 53% of content in whole study area. And kaolinite had 18 to 30%, chlorite had 15 to 25%, and smectite had 4 to 12% of content, respectively. The results of SEM observation showed that appearances of Ulsan clay were sheet, plannar or needle form. Ulsan clay included the salt crystal of cubic and the foraminifera, which were related with the content of organ.

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