• 제목/요약/키워드: SEM observation

검색결과 779건 처리시간 0.019초

로렌츠 SEM을 이용한 동적자구 모양의 관찰 (Observation of Dynamic Domain Patterns using Lorentz SEM)

  • 김영학
    • 한국자기학회지
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    • 제5권5호
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    • pp.885-891
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    • 1995
  • 로렌트 SEM을 이용하여 동적자구 모양의 관찰에 대한 검토가 50 Hz ~ 10 kHz의 주파수 범위에서 수행되었다. 동적자구 모양의 관찰은 여자주파수와 SEM의 주사주파수의 정수 배와의 사이에 미소한 차를 두고 관찰하는 방법이며, 이 관찰 방법에 따라서 시뮬레이션하여 시뮬레이션한 모양과 관찰모양을 비교 검토하였다. 또한 더욱 높은 주파수에서 동적자구 모양을 관찰하기 위해서는 SEM의 주사주파수의 안정화에 대한 필요한 것을 알았다.

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저진공주사현미경(LV-SEM)을 이용한 목재횡단면의 수축거동관찰 (Observation of Shrinkage Features of Cross Sectional Surface of Wood by LV-SEM)

  • 강춘원;마츠무라 준지;강욱
    • Journal of the Korean Wood Science and Technology
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    • 제36권3호
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    • pp.17-23
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    • 2008
  • 목재의 수축거동을 짧은 시간 내에 세포수준에서 관찰하기 위하여 목재를 함수상태로 관찰할 수 있는 저진공 주사전자현미경(Low-Vacuum Scanning Electron Microscopy)의 경통 내에서 습윤상태의 소형시편을 탈습시켜 건조시키면서 횡단면에서의 목재수축거동을 관찰하였다. 또한 동일한 개체에서 수축율 시험편을 제작하여 실제목재의 수축율을 측정하여 비교하였다. 경통 내의 탈습은 약 20여 분 정도에 완료되어 짧은 시간 내에 목재의 수축과정을 관찰하는 것이 가능하였으며, 수축율 시험편의 수축율과 현미경 내의 탈습에 의한 소시험편의 수축율은 비슷하였다. 목재의 수축율에 기여하는 춘재와 추재의 수축율에 대한 개개의 관찰이 가능하였으며 양자의 수축량은 거의 비슷하게 나타나는 것을 알 수 있었다. 목재의 수축과 세포벽수준에서의 수축을 비교해보면, 목재의 수축은 춘재보다 추재에 의해 좌우되는 사실을 알 수 있었다.

Characterization of Burned Architectural Woods by Fire Using SEM-EDXS and Computerized Tomography

  • Lee, Hyun-Mi;Hwang, Won-Joung;Lee, Dong-Heub;Son, Dong-Won
    • Journal of the Korean Wood Science and Technology
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    • 제42권5호
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    • pp.516-522
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    • 2014
  • Old architectural wood materials damaged by a fire were evaluated on the basis of wood species and scanning electron microscopy (SEM) observation of wood tissues in combination with energy dispersive X-ray spectroscopy (EDXS) analysis. Results of SEM observation showed that tracheid wall thickness of burned parts was very thin compared with undamaged and sound wood, and tylosoid in the resin canals disappeared after the exposure to fire. SEM-EDXS analysis indicated that carbon and oxygen peaks occurred in the original energy band, and the carbon peak was higher than that of the oxygen in the burned part. A computerized tomography was also undertaken to investigate the carbonization layer formed by fire and possible internal defects.

초경합금재의 전자현미경(SEM)내 마이크로 절삭 (Micro-cutting of Cemented Carbides with SEM)

  • 허성중
    • 한국정밀공학회지
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    • 제20권9호
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    • pp.55-62
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    • 2003
  • This paper investigates the micro-cutting of cemented carbides using PCD (polycrystalline diamond) and PCBN (polycrystalline cubic boron nitride) cutting tools are performed with SEM direct observation method. The purpose of this study is to make clear the cutting mechanism of cemented carbides and the fracture of WC particles at the plastic deformation zone in orthogonal micro-cutting. And also to achieve systematic understanding, the effect of machining parameter on chip formation and machined surface was studied, including cutting speed, depth of cut and various tool rake angle. Summary of the results are shown below. (1) Three type of chip formation process have been proposed by the results of the direct observation in orthogonal micro-cutting of cemented carbide materials. (2) From the whole observation of chip formation, primary WC particles are crushed and/or fine grained in the shearing deformation zone. A part of them are observed to collide directly with a cutting edge of tool by following the micro-cutting. (3) Surface finish, surface morphology and surface integrity is good to obtain by cutting with PCD cutting tool compared with PCBN. (4) The machined surface has the best quality near the low cutting speed of 10${\mu}m$/sec with a cutting depth of 10 ${\mu}m$ using 0$^\circ$ rake angle and 3$^\circ$ flank angle in this condition, but it was found that excessively low speed, for example the extent of 1 ${\mu}m$/sec, is not good enough to select for various reason.

Viola속 식물의 원형질체 및 융합세포의 전자현미경 관찰 (Electron Microscopic Observations of Protoplast and Fusion Cell of Viola Species)

  • 정용모;임현희;손병구;서정해;정정한;권오창
    • 생명과학회지
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    • 제7권4호
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    • pp.282-288
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    • 1997
  • To obtain a basic information on the development of Genus Viola, ultrastructure and electrofusion process between the two protoplasts from wild Viola callus cells and pansy mesophyll cells were observed with a scanning electron microscopy(SEM) and transmission electron microscopy(TEM). In the ultrastructural observation of wild viola callus protoplasts and pansy mesophyll protoplasts using SEM, their cell walls were removed completely. A knob-like formation was observed on the enlarge surface of viola callus protoplasts. On the surface of pansy mesophyll protoplasts net-like chloroplasts were observed. In SEM observation of pansy mesophyll protoplasts, chloroplasts devoid of membrane were observed on the surface the protoplasts. Pearl chain was formed by applying AC field of 200 V/cm at 1.0 MHz for 43 sec. The lysis of plasma membranes and fusion process occurred by applying a 1,600 V/cm DC pulse twice for 1 sec. After 1-2 hours of a DC pulse application, it was observed that the two protoplasts were fused completely into one cell. In TEM observation of the fused cell, many small vacuoles were located in the fusion area of the two protoplasts. Indeed, two distinct regions were observed during fusing process; in one region, a nucleus was found, while in the other region, both nucleus and nucleous were found.

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격음노출 후 기니픽 달팽이관 내유모세포 부동섬모에 관한 SEM(전자투사식현미경) 관측 (SEM Observation for the Damage of Inner Hair Cell Stereocilia of Guinea Pig Cochlea after Loud Tone Exposure)

  • Jarng Soon Suck
    • The Journal of the Acoustical Society of Korea
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    • 제24권1E호
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    • pp.1-6
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    • 2005
  • The inner hair cell stereocilia of the guinea pig cochlea was examined under a scanning electron microscope (SEM) after loud tone exposure onto the ear drum of the animal. Before and after guinea pigs were exposed to intensive and continuous tone such as 106 dB SPL in intensity, the functioning of the cochlea was monitored by N1-N2 audiograms. The structural damage of the stereocilia of inner hair cells (IHCs) and outer hair cells (OHCs) was examined using the SEM in x 1500 magnification. The comparison between the functional change of the cochlea and the structural damage of the IHC stereocilia is done by means of photographic observation. It can be shown that the functional change might be related to the structural damage of the IHC stereocilia after intensive acoustic trauma.

초음파 가공에 의한 Ni-Cu 박판의 용착 특성 평가 (Evaluation on Welding Characteristic of Ni-Cu Sheet by Ultrasonic Machining)

  • 백시영;장성민
    • 한국산학기술학회논문지
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    • 제12권3호
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    • pp.1070-1077
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    • 2011
  • 본 논문은 초음파 가공에 의한 용착성을 가공조건의 영향에 관하여 나타내었다. 한파장 혼의 최적화를 이용한 Ni-Cu 이종금속 박판의 용착성 평가는 초음파 가공 방법을 이용하여 확인된다. 초음파 가공변수 설정에 따른 인장시험을 통한 최적의 용착조건을 제시하였으며 SEM 사진과 EDX-ray 분석에 의한 용착성을 평가하였다. 실험적 연구는 초음파 가공 후 인장강도의 측정, SEM사진 분석으로 수행된다. 또한 가공시간, 가압력, 진폭의 가공변수들은 본 연구에 적용되었다.

치석의 주사전자현미경 관찰 및 세균동정에 관한 연구 (A study of dental calculus scanning electron microscopic by observation bacteria identification)

  • 장계원
    • 한국치위생학회지
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    • 제7권2호
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    • pp.189-196
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    • 2007
  • A study of the J health college dept of dental hygiene practice vistant a total of 35 supragingival calculus and subgingival calculus picking SEM observation and bacteria identification of the result are followings. 1. As observed by dental calculus SEM, the surface roughness appeared as peaks, valleys, and pits. 2. About bacteteria morphology blood agar plate small green zone partial hemolysis colony streptococcus observation 3. Isolated colony gram stain gram are positive display 4. Supragingival calculus at Lactococcus lactis spp. Leuconostoc spp. Streptococcus mitis, Aerococcus viridans bacteria 1, 3, 3, 16 species detection 5. Subgingival calculus at Aerococcus viridans, Leuconostoc spp. bacteria 5, 1 species detection.

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미끄럼반복마찰의 직접관찰에 의한 TiN피막의 허용응력에 관한 연구 (A Study on the Allowable Stress of TiN Coating During Repeated Sliding Condition by In-situ System)

  • 문봉호
    • Tribology and Lubricants
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    • 제27권3호
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    • pp.147-155
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    • 2011
  • The ceramic coatings are excellent materials of cutting tools and sliding parts. To evaluate the wear characteristics of very thin ceramic coated layer, it is very important to investigate its wear process microscopically. An effective method for investigating the wear of a thin layer is the observation of wear process in microscopic detail using in-situ system. In this study, using the SEM Tribosystem as in-situ system, the microscopic wear mode of TiN coatings was investigated in repeated sliding. As results, four modes were observed for TiN coatings: Ploughing, powder formation, flake formation and coating delimitation. The observation of the microscopic wear by in-situ system can clarify the allowable stress of TiN coating.