• 제목/요약/키워드: SEM Micrographs

검색결과 137건 처리시간 0.023초

A New Species of the Rarely Known Genus Apolethon(Copepoda, Harpacticoida, Laophontidae) from Brackish Waters of Korea

  • Lee, Ji-Min;Chang, Cheon-Young
    • Animal cells and systems
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    • 제12권4호
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    • pp.249-259
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    • 2008
  • A new laophontid copepod species, Apolethon articulatus n. sp., is described from the estuaries and salt marshes in South Korea. Apolethon articulatus is similar to the three congeneric species currently known in sharing the character combination of the elongate first endopodal segment of leg 1 with inner seta and the expansion of second endopodal segments of legs 2-4 with decrease in the number of setae on them. However, A. articulatus differs from them by the separate exopod of female leg 5 and the armature of mandibular palp with 6 setae. Description and taxonomic accounts of the new species are presented herein with detailed illustrations and SEM micrographs. As the true identity of the rarely known genus has not been clarified yet, a revised generic diagnosis is provided with a key to the species hitherto known in the genus.

Laser Ablated Carbon Thin Film from Carbon Nanotubes and Their Property Studies

  • Sharon, Maheshwar;Rusop, M.;Soga, T.;Afre, Rakesh A.
    • Carbon letters
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    • 제9권1호
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    • pp.17-22
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    • 2008
  • A carbon nanotube (CNT) of diameter ~20 nm has been synthesized by spray pyrolysis of turpentine oil using Ni/Fe catalyst. Pellet of CNTs has been used as a target to produce semiconducting carbon thin film of band gap 1.4 eV. Presence of oxygen pressure in the pulse laser deposition (PLD) chamber helped to control the $sp^3/sp^2$ ratio to achieve the desired band gap. Results are discussed with the help of Raman spectra, SEM TEM micrographs and optical measurements suggest that semiconducting carbon thin film deposited by PLD technique has retained its nanotubes structure except that its diameter has increased from 20 nm to 150 nm.

Template Synthesis of $Ni(OH)_2$ nanowires by Electrochemical Process

  • Zhang, Wentao;Beili, Pang;Lee, Hong-Ro
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 한국표면공학회 2008년도 추계학술대회 초록집
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    • pp.68-68
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    • 2008
  • There are several methods for oxide coating on metals, such as aluminum or carbon nanotubes(CNTs). Usually CVD method is introduced for various oxide coating on CNTs. Another method is electrochemical method which use potential-pH diagram for oxide coating on metal or CNTs. In this experiment, electrochemical coating parameter for oxide coating on aluminum template modified by acids and hydrogen peroxide ($H_2O_2$) were examined. SEM micrographs displayed clearly $Ni(OH)_2$ coating on template. For confirmation of electrochemical method application to EDLC electrode material fabrication, EDS spectrum was analyzed.

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Preparation of Silica Core-Hybrid Pigment via Sol-Gel Process and It's Application for Inkjet Dispersion Ink (졸-겔법을 이용한 실리카 핵을 가지는 하이브리드 안료의 제조와 잉크젯 분산 잉크로서 응용)

  • Jeon, Young-Min;Kim, Jong-Gyu;Gong, Myoung-Seon
    • Korean Journal of Materials Research
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    • 제16권10호
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    • pp.599-605
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    • 2006
  • N-(3-triethoxysilylpropyl)-1,4-diaminoanthrquinone-2,3-dicarboximide (TESP-DADI), an organic blue pigment, has been prepared and incorporated into silica solid matrix reacting triethyl orthosilicate (TEOS) via sol-gel method. Morphology and microstructure of resulting hybrid pigment were studied employing SEM and TEM. The micrographs and particle size distributions showed that uniform pigment can be obtained employing TEOS-based sol-gel method forming silica core. Particle size distribution of dispersed pigment in water was examined using the technique of dynamic light scattering. The ensuing pigment dispersion ink was subjected to various physicochemical evaluation such as viscosity, surface tension, inkjet stability, storage stability, and color change as inkjet ink using spectrophotometric, and microscopic techniques.

Changes of Emulsifying and Foaming Properties of Soy Protein with an Calcium , HCI and Microbial IJ-3 Strain Enzyme

  • Park, Yang-Won;Kim, Young-Jeon
    • Preventive Nutrition and Food Science
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    • 제1권1호
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    • pp.53-58
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    • 1996
  • The characterstics of the soy protein curd(eczyme-, HCI- and Ca-surd) were shown by scanning electron micrographs and gel electrophoreis. The emulsion stability of enzyme-curd showed high value in the range of pH 2~10and wide range of temperature(20~8$0^{\circ}C$). While at the isoelectric point(pH5.0), the emulsion stability of the HCI-and Ca-curd was decreased remarkably, and the emulsion stability of temperature was reduced quickly to the 60% and 40% at the 4$0^{\circ}C$. The foam stability of enzyme-curd was slightly higher than that HCI-and CA-curd in all ranges of pH and temperature. The feature of SEM of enzyme-cured produced degradation products faster than that of the HCI- and Ca-curd.

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Role of class-C fly Ash in the Development of Strength & Microstructure of Fly Ash-GGBS Geopolymer

  • Sasui, Sasui;Kim, Gyu Yong;Lee, Sang Kyu;Son, Min jae;Hwang, Eui Chul;Nam, Jeong Soo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 한국건축시공학회 2020년도 봄 학술논문 발표대회
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    • pp.79-80
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    • 2020
  • The class-C fly ash (FA) and ground granulated blast-furnace slag (GGBS) based geopolymer activated in NaOH (4M) was studied regarding compressive strength, porosity, microstructure and formation of crystalline phases. The class-C FA and GGBS blends resulted in reduced strength and increased porosity of the matrix with the increase in FA content. The unreactivity of calcium in blends was observed with increasing FA content leading to strength loss. it is evident from XRD patterns that calcium in FA did not contribute in forming CSH bond, but formation of crystalline calcite was observed. Furthermore, XRD analyses revealed that reduction in FA leads to the reduction in crystallinity and SEM micrographs showed the unreactive FA particles which hinder the formation of denser matrix.

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Morphological Studies of Developmental Stages of Oculotrema hippopotami (Monogenea: Polystomatidae) Infecting the Eye of Hippopotamus amphibius (Mammalia: Hippopotamidae) Using SEM and EDXA with Notes on Histopathology

  • Rubtsova, Nataliya Yu.;Heckmann, Richard A.;Smit, Willem J.;Luus-Powell, Wilmien J.;Halajian, Ali;Roux, Francois
    • Parasites, Hosts and Diseases
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    • 제56권5호
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    • pp.463-475
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    • 2018
  • The present study was performed to observe histopathological effects of Oculotrema hippopotami Stunkard, 1924 infection in the eye of Hippopotamus amphibius, as well as to reveal new details of morphology and structural features of this monogenean and its comparison between 2 age stages of the parasite. This was done using both light and scanning electron microscopy, energy dispersive X-ray analysis (EDXA) and histopathology. The presence of a mixture of different generations (adult and sub-adult) in one host individual is common for Oculotrema Stunkard, 1924 in contrast to Polystoma Zeder, 1800. New metrical and graphical information obtained for adults and sub-adults compared with the previous studies. Here we show the presence of genital papillae in adults, metrical data on the distal part of the vas deferens. SEM micrographs of sperm ejaculatory structures and information about the flattened dorsal side of the body provided for the first time. Histopathological changes, such as necrosis and hemorrhage in host tissues as a result of O. hippopotami attachment structures are described. Structural analysis of different body parts of O. hippopotami of both age groups are also included. We show qualitative differences in the presence of hardening ions (S, P, Ca) in attachment structures (oral and haptor suckers) that increase with the age of the worm. The presence of sub-adults and adults on the same host, together with high levels of infection without high pathogenicity may account for Oculotrema being one of the most successful parasites among the Monogenea.

Superconducting Properties of the Mg-Bi(Pb)SrCaCuO (110 K Phase) Composite System focusing on the Microstructure (Mg가 혼합된 Bi(Pb)SrCaCuO(110 K 상) 고온초전도체의 미세구조에 따른 초전도 특성 변화에 대한 연구)

  • 이정화;최봉수;이민수
    • Journal of the Korean Ceramic Society
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    • 제40권6호
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    • pp.530-538
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    • 2003
  • Samples with the nominal composition, B $i_{1.84}$P $b_{0.34}$S $r_{1.91}$C $a_{2.03}$C $u_{3.06}$ $O_{10+}$$\delta$/ (110 K phase) high $T_{C}$ superconductors containing MgO as an additive were fabricated by a solid-state reaction method. Samples with 5~50 wt% MgO were sintered at 820~86$0^{\circ}C$ for 24 h. The structural characteristics, critical temperature and grain size of the samples with different MgO contents were analyzed by XRD and SEM. As the MgO content increased, the intensity of MgO peaks and ratio of Bi-2212 phase in superconductors were intensified and the proportion of the phase transition from Bi-2223 to Bi-2212 was increased.d.creased.d.

Adsorption and Biological Properties of Ni-treated PAN Based Activated Carbon Fiber (Ni가 처리된 PAN계 활성탄소섬유의 흡착특성과 생물학적 특성)

  • Oh, Won-Chun
    • Analytical Science and Technology
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    • 제13권2호
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    • pp.194-199
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    • 2000
  • The study on the adsorption, the surface properties and the antibacterial effects of the Ni-treated PAN based activated carbon fibers was carried out. In the adsorption study on the Ni-treated PAN based ACFs, Type I isotherms for N1-N3 and Type II-Type III isotherms for N4-N6 were obtained, respectively. Futhermore, their adsorbed volumes slowly were decreased with the increase in the mole concentration of Ni on the treated PAN based ACFs. From the BET equation, the specific surface areas of the Ni-treated PAN based ACFs were in the range of $692.58-895.24m^2/g$. The micropore volumes obtained from ${\alpha}_s$-method using common-t value were $0.19-0.56cm^3/g$. The surfaces of PAN based ACFs partially blocked by metal after the treatment were observed from the SEM micrographs. Finally, from the antibacterial effects using Shake flask method against E. coli, the percentage of the effects was 92.5-100% and the antibacterial effect was increased with the increase in mole concentration of Ni treated.

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Confinement effectiveness of Timoshenko and Euler Bernoulli theories on buckling of microfilaments

  • Taj, Muhammad;Khadimallah, Mohamed A.;Hussain, Muzamal;Mahmood, Shaid;Safeer, Muhammad;Al Naim, Abdullah F.;Ahmad, Manzoor
    • Advances in concrete construction
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    • 제11권1호
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    • pp.81-88
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    • 2021
  • Rice Husk Ash (RHA) geopolymer paste activated by sodium aluminate were characterized by X-ray diffractogram (XRD), scanning electron microscope (SEM), energy dispersion X-Ray analysis (EDAX)and fourier transform infrared spectroscopy (FTIR). Five series of RHA geopolymer specimens were prepared by varying the Si/Al ratio as 1.5, 2.0, 2.5, 3.0 and 3.5. The paper focuses on the correlation of microstructure with hardened state parameters like bulk density, apparent porosity, sorptivity, water absorption and compressive strength. XRD analysis peaks indicates quartz, cristobalite and gibbsite for raw RHA and new peaks corresponding to Zeolite A in geopolymer specimens. In general, SEM micrographs show interconnected pores and loosely packed geopolymer matrix except for specimens made with Si/Al of 2.0 which exhibited comparatively better matrix. Incorporation of Al from sodium aluminate were confirmed with the stretching and bending vibration of Si-O-Si and O-Si-O observations from the FTIR analysis of geopolymer specimen. The dense microstructure of SA2.0 correlate into better performance in terms of 28 days maximum compressive strength of 16.96 MPa and minimum for porosity, absorption and sorptivity among the specimens. However, due to the higher water demand to make the paste workable, the value of porosity, absorption and sorptivity were reportedly higher as compared with other geopolymer systems. Correlation regression equations were proposed to validate the interrelation between physical parameters and mechanical strength. RHA geopolymer shows comparatively lower compressive strength as compared to Fly ash geopolymer.