• 제목/요약/키워드: SEM Image

검색결과 507건 처리시간 0.03초

$BaTiO_3$계 박막의 소결온도에 따른 미세구조와 전기적 특성 (Electrical Characteristics and Microstructure of Thin Films $BaTiO_3$ depending on The Sintering Temperature)

  • 김덕규;전장배;박춘배;송민종;강용철;박해암;소병문;김태완;강도열
    • 대한전기학회:학술대회논문집
    • /
    • 대한전기학회 1997년도 하계학술대회 논문집 C
    • /
    • pp.1573-1576
    • /
    • 1997
  • Thin films of $BaTiO_3$ system were prepared by radio frequency (rf)/dc magnetron sputtering method. We have investigated crystal structure, surface morphology and PTCR(positive-temperature coefficient of resistance) characteristics of the specimen depending on second heat - treatment temperatures. Scanning electron microscope(SEM) image of $BaTiO_3$ thin films shows that the specimen heat treated in between 900 and 1100[$^{\circ}C$] shows a grain growth. At 1100[$^{\circ}C$], the specimen stops grain-growing and becomes a crystal. A resistivity-temperature characteristics of the specimen depends on the doping concentrations of Mn.

  • PDF

플라즈마용사공정에서의 최적 조건 결정에 관한 연구 (Determination of Optimum Condition in Plasma Spraying Process)

  • 최경수;박동화
    • 한국세라믹학회지
    • /
    • 제33권2호
    • /
    • pp.155-162
    • /
    • 1996
  • A Taguchi methodology study of the plasma spraying thermal barrier coating (TBC) layer is presented. The experiment parameters were designed by a L8-style orthogonal arrays approach. A Taguchi analysis was conduc-ted through the results of the coating properties which were affected by plasma spraying parameters. Zirconia (partially stbilized with ytrria: PSZ) was sprayed on TiAl intermetallic compound substrates, The coating layer was characterized by thickness microstructure and porosity using SEM and Image analyzer. The coating quali-ties are discussed with respect to thermal barrier effect thermal cycling test6 and adhesion strength test. An optimum condition of plasma spraying process which are derived from the Taguchi analysis could be found for high quality TBC.

  • PDF

The Optimization of Gel Electrolytes on Performance of Valve Regulated Lead Acid Batteries

  • An, Sang-Yong;Jeong, Euh-Duck;Won, Mi-Sook;Shim, Yoon-Bo
    • Bulletin of the Korean Chemical Society
    • /
    • 제29권5호
    • /
    • pp.998-1002
    • /
    • 2008
  • The gel electrolytes were prepared with sulfuric acid and phosphoric acid, where hydrophilic fumed silica was used as a gelling agent. The influences of gel electrolyte on performance of the valve regulated lead acid (VRLA) batteries were investigated employing capacity tests, electrochemical impedance spectroscopy and scanning electron microscopy. The initial capacities of the sulfuric gel VRLA batteries were higher than that of phosphoric gel VRLA batteries. The sulfuric gel VRLA battery using 1.210 specific gravity of sulfuric acid with hydrophilic fumed silica exhibited the highest capacity of 0.828Ah. In the impedance measurements, the ohmic and charge transfer resistances for the phosphoric gel VRLA batteries were higher thanthat of sulfuric gel batteries. The morphology of electrodes of phosphoric gel VRLA batteries were more deteriorated in the SEM image.

Direct Growth of Graphene on Boron Nitride/Copper by Chemical Vapor Deposition

  • Jin, Xiaozhan;Park, J.;Kim, W.;Hwang, Chanyong
    • 한국진공학회:학술대회논문집
    • /
    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
    • /
    • pp.590-590
    • /
    • 2013
  • Direct growth of graphene using CVD method has been done on CVD grown boron nitride substrate. From the SEM image, we have shown that the size of grain of graphene could be clearly controlled by varying the amount of injected hydrocarbon. To convince the existence of graphene on boron nitride, XPS and Raman has been checked. Both B1s and N1s peaks in XPS spectra and the Raman peak around 1,370 $cm^{-1}$ demonstrated that boron nitride did remain after high temperature treatment during the graphene growth process. And along the graphene grain boundary, the Raman fingerprint of graphene was neatly appeared.

  • PDF

LB법에 의해서 제작된 DLPC 지질막의 캐패시턴스 특성 (The Capacitance Properities of DLPC Liquid Membrance Fabricatied by LB Method)

  • 정용호;이우선
    • 한국전기전자재료학회논문지
    • /
    • 제11권8호
    • /
    • pp.628-636
    • /
    • 1998
  • LB layers L-$\alpha$-DLPC deposited by LB method were deposited onto n-type silicon wafer as Z-type film. Films made up of 8, 16 layers of lipid with long alkyl chain and the thickness of monolayer and multiayers was determined by ellipsometry. Ut was deposited Ag and Al onto LB layers and silicon wafer for electrode and small electrode exhibit high capacitiance and low lekage current. The C-V curves of the MLS capacitor shows very high saturation value of capacitance. And cross-sectional SEM image of MLD capacitor indicated the presence of pore with Al electrode and we found that the Ag is good for electrode metal.

  • PDF

Micro FEM 해석에 의한 기포제 혼입 시멘트 페이스트의 역학적 성능 평가에 관한 연구 (A study on Mechanical Performance Evaluation of Cement Paste Using Foaming Agent by Micro FEM Analysis)

  • 김보석;우영제;이한승
    • 한국건축시공학회:학술대회논문집
    • /
    • 한국건축시공학회 2015년도 춘계 학술논문 발표대회
    • /
    • pp.55-56
    • /
    • 2015
  • This study is corroborated as a fundamental resource to develop structural lightweight paste containing silica fume as a part of cement. Paste using foaming agent is generated much foam and decreased density of paste. This study is measured at 0.8% of foaming agent dosage but over 0.8% of foaming agent dosage raise density of paste because of interconnection with foam. Also, FEM analysis using SEM image is confirmed correspondence of between Elastic modulus of experiment and FEM analysis.

  • PDF

Synthesis of Cation-Exchange Membrane by the Monomer Sorption

  • Park, Yong-Jin;Moon, Seung-Hyeon
    • 한국막학회:학술대회논문집
    • /
    • 한국막학회 2003년도 The 4th Korea-Italy Workshop
    • /
    • pp.1-4
    • /
    • 2003
  • LDPE/polystyrene cation exchange membranes were prepared through a monomer-sorption method and UV radiation polymerization. The reaction behaviors in the preparation were investigated. The membranes prepared were characterized in terms of physical and electrochemical properties. The membranes exhibited reasonable properties for an ion-exchange membrane with weight gain (Wr) of above 0.3, electrical resistance of below 1.0 Ω $\textrm{cm}^2$ and ion-exchange capacity of 1.8 meq/g-dry membrane. DSC studies and FE-SEM image revealed the formation of a homogeneous membrane. Both the current-voltage and the chronopotentiometric curves of the membranes indicated that LDPE/polystyrene membranes can be properly used at a high current density, and the surface homogeneity of cation-exchange sites in the membrane was comparable to that in a commercial membrane.

  • PDF

레이저 융제된 HTS 표면의 불균일한 변조에 대한 연구 (Study on the nonuniform modification of laser ablated HTS surface)

  • 정영식;이상렬
    • 대한전기학회:학술대회논문집
    • /
    • 대한전기학회 1996년도 추계학술대회 논문집 학회본부
    • /
    • pp.251-253
    • /
    • 1996
  • High temperature superconducting (HTS) target has been irradiated by excimer laser beam. The surface of HTS target has been changed and showed the formation of cones. The laser ablated HTS target surface has been systematically studied using a scanning electron microscope. A KrF excimer laser with a wavelength of 248 nm was used to ablate the HTS YBCO target. The size of laser beam focused on the target showed a rectangular shape of $9.7{\times}2\;mm^2$. The image of SEM shows the difference between the shapes of cones fanned at the boundary and at the center of the ablated area after 1,000 laser pulses.

  • PDF

나노 광소자 응용을 위한 알루미늄 양극산화박막 공정 (Thin film process of anodic aluminum oxidation for optoelectronic nano-devices)

  • 최재호;백하봉;김근주
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
    • /
    • pp.106-107
    • /
    • 2007
  • We fabricated anodic aluminium oxides (AAO) on Si and sapphire substrates from the electrochemical reactions of thin AI films in an aqueous solution of oxalic acid. The thin AI films have deposited on Si and Sapphire substructure by using E-beam evaporation and thermal evaporation, respectively. The formation of AAO structures has investigated from FE-SEM measurement image and showed randomly distributed phase of nanoholes instead of the periodic lattice of photonic crystals. The AAO structure on sapphire shows the double layers of nanoholes.

  • PDF

경년변화에 따른 송전용 폴리머 현수애자의 트래킹 성능평가 (Tracking Property of Polymer Suspension Insulator for Transmission line with secular variation)

  • 조한구;이운용;이유정;임기조;최인혁
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
    • /
    • pp.558-559
    • /
    • 2005
  • Recently, polymer insulators that are used for high voltage applications have some advantages such as light weight, small size, vandalism resistance, hydrophobicity and easy making process. During outdoor service of polymer insulators, the surface of the insulating material is frequently subjected to moisture and contamination that lead to dry band arcing. Their tracking resistance, erosion resistance, end sealing and shed design are very important because dry band arcing causes degradation of polymer surface. In this paper, the tracking property of polymer suspension insulator for power transmission is investigated with CEA tracking wheel test. The diagnosis of insulator sample in tracking test has been analyzed by leakage current, STRI Guide, SEM, FTIR and thermal image.

  • PDF