• Title/Summary/Keyword: SEM Image

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Influence of soft drinks supplemented calcium to enamel remineralization (칼슘보강음료가 법랑질 재광화 효과에 미치는 영향)

  • Kim, Min-Young;Lee, Hye-Jin
    • Journal of Korean society of Dental Hygiene
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    • v.8 no.3
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    • pp.13-22
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    • 2008
  • Objectives: The purpose of this study was to identify the correlation between calcium in soft drinks and enamel remineralization. Method: Six soft drinks were used in this study. These were calcium milk, normal milk, calcium yoghurt, normal yoghurt, calcium orange juice, and orange juice. Enamel specimens which 300- 400Vickers Hardness Number (VHN) were selected. These samples were immersed in each soft drink for 12 hours in an in vitro remineralization model. All specimens were processed for SEM image of the enamel surface. Results were analyzed by SPSS 13.0 package program. Results: Calcium milk was the most influential and normal yoghurt was the least to enamel surface. There was not significant difference according to calcium supplement in milk although the difference of enamel hardness was ${\Delta}f13.4$ in calcium milk, and ${\Delta}f4.7$ in normal milk (P>0.05). Other soft drinks showed a little change about calcium but they were insignificant. Demineralization effect was remarkably observed in calcium yoghurt ($-{\Delta}f269.1$) and this effect was confirmed by SEM images. In conclusion, calcium supplemented soft drinks had little influences to hardness of enamel surface.

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The Study of Asymmetrical of the Serratus Anterior and Lower Trapezius Muscles in Chronic Stroke Patients (만성 뇌졸중 환자의 앞 톱니근과 하부 등세모근의 비대칭성 연구)

  • Jeong, Ju-Ri;Lee, Wan-Hee
    • Journal of the Korean Society of Physical Medicine
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    • v.10 no.4
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    • pp.81-90
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    • 2015
  • PURPOSE: The purpose of this study was to compare the muscle architecture of serratus anterior and lower trapezius using rehabilitative ultrasound imaging (RUSI) in affected and unaffected side of chronic stroke patients. METHODS: The participants were thirty five patients with stroke hemiplegia in this study. RUSI was used to measure the muscle thickness of the serratus anterior and lower trapezius muscles. We compared the muscle thickness according to affected side and sex, determined the reliability of the measurement image. Independent t-test, intra-class correlation coefficient (ICC) and standard error of measurement (SEM) were used for statistical analysis. RESULTS: Significant difference in muscle thickness of serratus anterior was observed between affected and unaffected side (p<.001). Muscle thickness according to gender showed a significant difference in unaffected side of serratus anterior (p<.05). Compare asymmetry ratio of serratus anterior and lower trapezius muscle thickness showed a significant difference (p<.001). ICC for intra-reliability was .944~.962 in serratus anterior and .873~.925 in lower trapezius muscle thickness, respectively. SEM was .001~.004 in serratus anterior and .002~.008 in lower trapezius muscle. CONCLUSION: This study, using RUSI, showed significant difference in muscle thickness of serratus anterior in affected and unaffected side of stroke patients. RUSI is a practical tool for measuring soft-tissue thickness in the scapular region muscle of stroke.

Characteristics of Surface Grinding for Heat Treated Titanium Alloy (열처리된 티타늄 합금의 연삭가공 특성)

  • Heo, S.;Kim, W.I.;Wang, D.H.;Lee, Y.K.
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2000.10a
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    • pp.349-354
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    • 2000
  • A use of Titanium alloy as a structural material is increasing lately. Among those titanium alloys, Ti-6A1-4V alloy is the most popular one with taking 2/3 of it's market. Also, Ti-6A1-4V alloy can get the stability of organization and product measure, and the evaluation of the cutting ability and the mechanical characteristics. The point in titanium alloy work is on how treat the heat generated during grinding. Because the heat conductivity of titanium alloy is unnegligibly low, the grinding heat is accumulated in workpiece, and it cause the increasing of grinding grits' wear and the rough grinding surface. So, these characteristics in grinding of titanium alloy will change the mechanical characteristics of the titanium alloy. From this study, the mechanical characteristics of annealed Ti-6A1-4V alloy after grinding was concerned with checking out the bending strength values, and the factor of the change and the difference was analyzed after analyzing the surface roughness and the image from SEM.

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Preparation of Emulsion from Biodegradable Polymer(II) - Characteristics of paper treated as PLA and PBS emulsion - (생분해성 고분자를 이용한 발수 에멀션의 제조(II) - PLA 및 PBS 에멀션 코팅 과일봉지의 물성 비교 -)

  • Kim, Kang-Jae;Lee, Min-Hyung;Eom, Tae-Jin
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.2
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    • pp.13-20
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    • 2013
  • In this study, two biodegradable polymer(PLA, PBS) emulsions were treated on agricultural packaging paper such as fruit bagging paper. Water-repellency, mechanical properties, and SEM image with thermal aging were measured on the emulsion treated fruit bagging paper. Biodegradable polymers(such as poly lactic acid, poly butylene succinate) emulsion treated fruit bagging paper had higher water-repellency and strength than other water-repellent(such as acrylic repellent, linseed oil and paraffin wax) treated fruit bagging paper. According to FE-SEM results of polymer emulsion coated fruit bagging paper, the colloidal particles of emulsion after thermal treatment (looks like being) were adhered to the fibers. Thus, using biodegradable polymer emulsion is expected to protect a fruit for a long time.

Instrumental Analysis of the Human Hair Damaged by Bleaching Treatments - Focused on ATR FT-IRM -

  • Ha, Byung-Jo
    • Journal of Fashion Business
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    • v.12 no.6
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    • pp.23-33
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    • 2008
  • The physico-chemical characteristics by bleaching treatments were assessed by several instrumental analyses such as surface morphology, chemical structural change, color change as well as tensile strength. The change of morphological characteristic was observed through scanning electron microscope(SEM). The observation of the fine structure on hair surface by SEM showed the bleached hair had much damaged to hair cuticle, and some of cuticle surface were worn away. To investigate the chemical structural changes in hair keratin, the cross-sections of hair samples were directly analysed using Fourier transform infrared microspectroscopy(FT-IRM). The results showed the cysteic acid S=O band intensity was distinctively increased by performing the bleaching treatment. The cleavage of cystine was appeared to proceed primarily through the sulfur-sulfur (-S-S-) fission whereby cysteic acid was formed as a principal oxidation products. The distribution of amide I band in hair keratin was determined by attenuated total reflectance(ATR) FT-IR mapping image. The results showed that the outer side of hair cortex was more damaged than the inner side of the hair cortex. Also, during chemical bleaching of the hair with alkaline peroxide, the hair was turned to reddish yellow due to the oxidative degradation of eumelanin. This means the eumelanin is more unstable than pheomelanin in chemical oxidation. With bleaching, the tensile strength was also reduced as a results of the chemical oxidation.

Comparison of Yittria Stabilized Zirconia Electrolytes(YSZ) for Thin Film Solid Oxide Fuel Cell by Atomic Layer Deposition and Sputtering (원자층 증착법과 스퍼터링을 이용한 고체산화물 연료전지용 YSZ 전해질에 관한 연구)

  • Tanveer, Waqas Hassan;Ha, Seung Bum;Ji, Sanghoon;Cha, Suk Won
    • 한국신재생에너지학회:학술대회논문집
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    • 2011.11a
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    • pp.84.2-84.2
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    • 2011
  • In this research, two thin film deposition techniques, Atomic Layer Deposition and Sputtering are carried out for the fabrication of Yittria Stabilized Zirconia electrolyte for thin film Solid Oxide Fuel Cell. Zirconium to Yittrium ratio for both cases is about 1/8. Scanning Electron Microscope(SEM) image shows that the growth rate per hour for Atomic Layer Deposition is faster than for sputtering. X-ray Photo-electron Spectroscopy(XPS) shows that the peaks of both Zirconia and Yittria shift towards higher bending energy for the case of Atomic Layer deposition and thus are more strongly attached to the substrate. Later, Nyquist plot was used to compare the conductivity of Yittria Stabilized Electrolyte for both cases. The conductivity at $300^{\circ}C$ for Atomic Layer Deposited Yittria Stabilized Zirconia is found to be $5{\times}10^{-4}S/cm$ while that for sputtered Yittria Stabilized Zirconia is $2{\times}10^{-5}S/cm$ at the same temperature. The reason for better performance for Atomic Layered YSZ is believed to be the Nano-structured layer fabrication that aids in along the plane conduction as compared to the columnarly structured Sputtered YSZ.

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The Method of Thermograph using Thermoelectric Sensor Device in the Carbon fiber Thick Films (Carbon fiber 후막형 열전센서 소자를 이용한 적외선 체열진단)

  • Song, M.J.;Kim, M.H.;Ryu, S.M.;Lee, H.S.;Lee, W.J.;Park, C.B.;Choi, W.S.;Kim, T.W.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.04b
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    • pp.1-2
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    • 2008
  • Thick films of Carbon fiber were prepared by a heating element of plan shape made in Darin co.. We have investigated surface morphology of the specimen depending on second heat-treatment temperatures. X-ray diffraction patterns of Carbon fiber thick films show that the specimen heat treated below $600^{\circ}C$ was an amorphous phase and the one heat treated above $1100^{\circ}C$ forms a poly-crystallization. Scanning electron microscope(SEM) image of Carbon fiber thick films of the specimen heat treated in between 900 and $1100^{\circ}C$ shows a grain growth. At $1100^{\circ}C$, the specimen stops grain-growing and becomes a poly-crystallization.

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The Behavior of Secondary Electrons and Optimal Mounting Position of a Secondary Electron Detector in SEM with a Numerical Analysis (수치해석을 통한 SEM 챔버내의 이차전자 거동해석 및 이차전자 검출기의 최적 장착 위치 선정)

  • Boo, Kyeung-Seok;Jeon, Jong-Up
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.17 no.4
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    • pp.15-21
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    • 2008
  • Secondary electron detectors used in scanning electron microscope accept secondary electrons emitted from the specimen and convert them to an electrical signal that, after amplification, is used to modulate the gray-level intensities on a cathode ray tube, producing an image of the specimen. In order to acquire images with good qualities, as many secondary electrons as possible should be reached to the detector. To realize this it is very important to select an appropriate mounting position and angle of the detector inside the chamber of scanning electron microscope. In this paper, a number of numerical simulations are performed to explore the relationships between detection rates of secondary electrons and the values of some parameters, such as distances between the detector and sample, relative mounting positions of scintillator positioned inside the detector with respect to detector cover, two types of mounting angles of the detector. The relationships between detection rates and applied voltages to corona ring and faraday cage, and energies of secondary electrons are investigated as well.

A Study on the Electromagnetic Properties of $La_{1-x}Ca_xMnO_3$(x=0.33) grown by Floating Zone Method (FZ법에 의한 $La_{1-x}Ca_xMnO_3$(x=0.33)의 결정성장과 전자기적 물성에 대한 연구)

  • 정준기;송규정;조남희;김철진
    • Korean Journal of Crystallography
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    • v.13 no.1
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    • pp.41-47
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    • 2002
  • La/sub 1-x/Ca/sub x/MnO₃ manganese oxide were grown using the floating zone image furnace with halogen lamps as heat source. The growth condition was 4∼6 mm/hr growth rate in air atmosphere, 45∼50 rpm and 20∼25 rpm of rotation rate of feedrod and growing crystal, respectively. Characterization analyses of the crystal were carried out using XRD, SEM, and EPMA. Orientation of crystal was determined using EBSD. The electromagnetic properties were measured with Quantum Design PPMS by 4 point probe method and resulted MR value of 462% at 215 K.

Photoinduced Superhydrophilicity in TiO2 Thin Films Modified with WO3

  • Hwang, Young-Kyu;Patil, Kashinath Rangu;Kim, Hye-Kyung;Dattatraya Sathaye, Shivaram;Hwang, Jin-Soo;Park, Sang-Eon;Chang, Jong-San
    • Bulletin of the Korean Chemical Society
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    • v.26 no.10
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    • pp.1515-1519
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    • 2005
  • Tungsten oxide-modified TiO2 thin films were formed on a glass substrate by sol-gel and dip coating processes using acetyl acetone as a chelating agent. The hydrophilic properties of the thin films were investigated with illumination of UV light. The dependence of water contact angle on material composition and morphology of the film is established with SEM image and AFM profile. The surface morphology was controlled with the change of precursor concentration. 0.01 M of tungsten oxide-modified Ti$O_2$ have shown the highest hydrophilicity after UV-irradiation. The effect of composition on photoinduced hydrophilicity of the W$O_3$-Ti$O_2$ films was also investigated. The films were characterized by XRD, SEM, AFM and XPS.