• Transactions of the Korean Society of Mechanical Engineers A
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• v.35 no.2
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• pp.169-174
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• 2011

Acoustic emission (AE) signals were detected and analyzed in real time during the polymerization shrinkage of composite resin restoration in an artificial dental ring with a class I cavity. Most AE hit events were observed in the initial curing period of the 1st region with high contraction rate. The range of the $2^{nd}$ region for the stainless steel specimen was shorter than that for the PMMA specimen but longer than that for the human dentin specimen. AE hit events showed a blast-type signal having an amplitude in the range of 25.45 dB and a frequency band of 100.200 kHz or 240.300 kHz. These values of amplitude and frequency indicated the fracture of resin or of the adhesive layer.

• Restorative Dentistry and Endodontics
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• v.48 no.2
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• pp.13.1-13.11
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• 2023

Objectives: Natural extracts have been investigated as a biomimetic strategy to mechanically strengthen the collagen network and control the biodegradation of extracellular matrix. This study evaluated the effect of epigallocatechin-3-gallate (EGCG) on abfraction lesions prior to the composite resin. Materials and Methods: The sample consisted of 30 patients (aged between 28 and 60 years) with abfraction lesions located in 2 homologous premolars. The teeth were randomly assigned according to dentin treatment: 0.02% EGCG solution or distilled water (control). After enamel acid etching, the solutions were applied immediately for 1 minute. The teeth were restored with Universal Adhesive (3M) and Filtek Z350 XT (3M). Analyzes were done by 2 independent examiners using modified USPHS (retention, secondary caries, marginal adaptation, and postoperative sensitivity) and photographic (color, marginal pigmentation, and anatomical form) criteria at baseline (7 days) and final (18 months). The data analysis used Friedman and Wilcoxon signed-rank tests (α = 0.05). Results: At baseline, all restorations were evaluated as alpha for all criteria. After 18 months, restorations were evaluated as alpha for secondary caries, color, and marginal pigmentation. There was significant difference between baseline and 18 months (p = 0.009) for marginal adaptation and postoperative sensitivity (p = 0.029), but no significant difference were verified between treatments (p = 0.433). The EGCG group had a restoration retention rate of 93.3%, while the control group had 96.7%. Conclusions: The application of EGCG solution on abfraction lesions did not significantly influence the survival of the restorations based on clinical and photographic criteria.

• The Journal of the Korean dental association
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• v.51 no.11
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• pp.604-609
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• 2013

Crown fractures are relatively common trauma to anterior teeth, and should be restored immediately in most cases. For those who suffer from unfortunate traumatic episode, the best treatment option should be minimally invasive approach. In the presence of fractured tooth fragment, reattachment procedure creates positive emotional response in the patient and simplifies the procedure and maintenance of the patient's original tooth anatomy and occlusion. Without fractured tooth fragment, next conservative option could be direct composite restoration which is based on minimal invasion concept. This article proposes simple and very conservative techniques that anyone can do in daily practice.

• Composites Research
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• v.12 no.2
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• pp.62-69
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• 1999

During fatigue loading of composite materials, damage accumulation can be monitored by measuring their material properties. In this study, fatigue modulus is used as the damage index. Fatigue life of composite materials may be predicted analytically using damage models which are based on fatigue modulus and resultant strain. Damage models are propesed as funtions of applied stress level, number of fatigue cycle and fatigue life. The predicted life was comparable to the experimental result obtained using E-glass fiber reinforced epoxy resin materials and pultruded glass fiber reinforce polyester composites under two-stress level fatigue loading.

• Journal of the Korean Ceramic Society
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• v.35 no.5
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• pp.421-428
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• 1998

The effect of silane coupling agents on the water stability of HAC/PVA based MDF cement composites which were modified with urethane and epoxy resin were studied as a function of the functional groups and addition amount of silane coupling agent. According to the composition of polymer matrix the silanes with different functional groups showed the different effectiveness. In case of the only PVA matrix the silane with vinyl functional group was more effective than other silanes. When the epoxy resin was added the silane of epoxy-methodxy group enhanced the flexural strength of dry and wet state more than other. In case of urethane-added MDF cement the silane of diamine group was effective and enhanced the water sta-bility fo MDF cement composite more and more as the addition amount of silane increased, Especially in case of warm-presed composite the effect of silane was enhanced By addition of 2wt% of silane with 야-amine group the flexural strength of urethane-added composites were enhanced by 20% more in dry state 40-70% in wet state in accord with the porosity analysis. The flexural strength of the poxy resin-added MDF cement composite was increased by addition of 1wt% and 2wt% silane of epoxy-methoxy group However the addition of 4wt% of silane decreased the flexural strength of dry and wet state by formation of closed pore in the polymer matrix.

• The Journal of Advanced Prosthodontics
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• v.9 no.4
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• pp.257-264
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• 2017

PURPOSE. To evaluate the adhesion to CAD/CAM feldspathic blocks by failure analysis and shear bond strength test (SBSt) of different restorative systems and different surface treatments, for purpose of moderate chipping repair. MATERIALS AND METHODS. A self-adhering flowable composite (Vertise Flow, Kerr) containing bi-functional phosphate monomers and a conventional flowable resin composite (Premise Flow, Kerr) applied with and without adhesive system (Optibond Solo Plus, Kerr) were combined with three different surface treatments (Hydrofluoric Acid Etching, Sandblasting, combination of both) for repairing feldspathic ceramics. Two commercial systems for ceramic repairing were tested as controls (Porcelain Repair Kit, Ultradent, and CoJet System, 3M). SBSt was performed and failure mode was evaluated using a digital microscope. A One-Way ANOVA (Tukey test for post hoc) was applied to the SBSt data and the Fisher's Exact Test was applied to the failure analysis data. RESULTS. The use of resin systems containing bi-functional phosphate monomers combined with hydrofluoric acid etching of the ceramic surface gave the highest values in terms of bond strength and of more favorable failure modalities. CONCLUSION. The simplified repairing method based on self-adhering flowable resin combined with the use of hydrofluoric acid etching showed high bond strength values and a favorable failure mode. Repairing of ceramic chipping with a self-adhering flowable resin associated with hydrofluoric acid etching showed high bond strength with a less time consuming and technique-sensitive procedure compared to standard procedure.

• Restorative Dentistry and Endodontics
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• v.44 no.1
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• pp.1.1-1.12
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• 2019

Objectives: The aim of this in vitro study was to test the effect of 2 finishing-polishing sequences (QB, combining a 12/15-fluted finishing bur and an EVO-Light polisher; QWB, adding a 30-fluted polishing bur after the 12/15-fluted finishing bur used in the QB sequence) on 5 nanotech-based resin composites (Filtek Z500, Ceram X Mono, Ceram X Duo, Tetric Evoceram, and Tetric Evoceram Bulk Fill) by comparing their final surface roughness and hardness values to those of a Mylar strip control group (MS). Materials and Methods: Twelve specimens of each nanocomposite were prepared in Teflon moulds. The surface of each resin composite was finished with QB (5 samples), QWB (5 samples), or MS (2 samples), and then evaluated (60 samples). Roughness was analysed with an optical profilometer, microhardness was tested with a Vickers indenter, and the surfaces were examined by optical and scanning electron microscopy. Data were analysed using the Kruskal-Wallis test (p < 0.05) followed by the Dunn test. Results: For the hardness and roughness of nanocomposite resin, the QWB sequence was significantly more effective than QB (p < 0.05). The Filtek Z500 showed significantly harder surfaces regardless of the finishing-polishing sequence (p < 0.05). Conclusions: QWB yielded the best values of surface roughness and hardness. The hardness and roughness of the 5 nanocomposites presented less significant differences when QWB was used.

• Restorative Dentistry and Endodontics
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• v.45 no.4
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• pp.55.1-55.12
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• 2020

Objectives: This study investigated the effects of physically damaged and resin-contaminated tips on radiant emittance, comparing them with new undamaged, non-contaminated tips using 3 pieces of spectrophotometric laboratory equipment. Materials and Methods: Nine tips with damage and/or resin contaminants from actual clinical situations were compared with a new tip without damage or contamination (control group). The radiant emittance was recorded using 3 spectrophotometric methods: a laboratory-grade thermopile, a laboratory-grade integrating sphere, and a portable light collector (checkMARC). Results: A significant difference between the laboratory-grade thermopile and the laboratory-grade integrating sphere was found when the radiant emittance values of the control or damaged/contaminated tips were investigated (p < 0.05), but both methods were comparable to checkMARC (p > 0.05). Regardless of the method used to quantify the light output, the mean radiant emittance values of the damaged/contaminated tips were significantly lower than those of the control (p < 0.05). The beam profile of the damaged/contaminated tips was less homogeneous than that of the control. Conclusions: Damaged/contaminated tips can reduce the radiant emittance output and the homogeneity of the beam, which may affect the energy delivered to composite restorations. The checkMARC spectrophotometer device can be used in dental offices, as it provided values close to those produced by a laboratory-grade integrated sphere spectrophotometer. Dentists should assess the radiant emittance of their light-curing units to ensure optimal curing in photoactivated, resin-based materials.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2003.04a
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• pp.196-201
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• 2003

When the structures are used in cold regions, the mechanical properties and dimension stability of the blade will be changed. The proposal of this study is to test the durability of the structures in cold regions. It is necessary to select the most comfortable materials and fabrication processes for more stable structures in cold regions. To select the most comfortable materials and processes, the static strength has to know through the tensile static tests at the severe condition as cold regions. First, the tensile static specimens made by RIM (Resin injection molding) process & vacuum bagging process with reinforcement materials and resin. Tensile static tests were carried out on three laminate lay-ups (carbon prepreg, carbon fiber dry fabric) at different test temperature($24^{\circ}C$, $-30^{\circ}C$), determining properties such as the mechanical strength, stiffness and strain to failure. At different test temperature, in order to test the tensile strengths of these specimens used the low temperature chamber. Next, the results of this test were compared with each other. Finally, the most comfortable materials and fabrication processes can select based on these results. The results show the changes in the static behavior of three laminate lay-ups at different test temperatures. At low temperatures, the static strengths are higher than the ones at room temperature.

• Composites Research
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• v.26 no.3
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• pp.182-188
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• 2013

The purpose of this study was to measure the volumetric polymerization shrinkage kinetics and stress of a silorane-based dental restorative composite and compare it with those of conventional methacrylate-based dental composites. Two methacrylate-based composites (Z250, Z350 flowable) and one silorane-based composite (P90) were investigated. The volumetric polymerization shrinkage of the composites during light curing was measured using a laboratory-made volume shrinkage measurement instrument based on the Archimedes' principle, and the polymerization stress was also determined with the strain gage method. The shrinkage of silorane-based composites (P90) was the lowest, and that of Z350 flowable was the highest. Peak polymerization shrinkage rate was the lowest in P90 and the highest in Z350 flowable. The time to reach peak shrinkage rate of P90 was longer than those of the methacrylate-based composites. The polymerization shrinkage stress of P90 was lower than those of the methacrylate-based composites.