• Title/Summary/Keyword: Resin thickness

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Development of Heating Table Fabrication Process for the High Speed Curing Composites

  • Kim, Yun-Hae;Ha, Jin-Cheol;Lee, Jin-Woo;Park, Jun-Mu;Han, Joong-Won;Choi, Byung-Keun;Moon, Kyung-Man;Nisitani, Hironobu
    • International Journal of Ocean System Engineering
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    • v.3 no.1
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    • pp.38-43
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    • 2013
  • Wind turbine generator is, recently, becoming bigger and bigger. So, in order to produce large amounts of electricity generation, we have to consider the length and thickness of the blade. We investigated the skills of processing for making the super thickness laminate through development fabrication process for high speed curing composite heating table.

Study on the Formation of Residual Layer Thickness by Changing Magnitude and Period of UV Imprinting Pressure (UV임프린트 공정에서 임프린팅 가압력 및 가압시간에 따른 레진 잔막 두께형성에 대한 실험연구)

  • Shin, Dong-Hyuk;Jang, Si-Youl
    • Tribology and Lubricants
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    • v.26 no.5
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    • pp.297-302
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    • 2010
  • This study is focused on the resin layer formation of UV imprinting process by changing imprinting pressure and period. The mold shape is made for the process of window open over the pattern transfer area and the imprinting period is assigned as the time just before the UV light curing. The residual layer is measured by changing the imprinting period and pressure magnitude, and the measured data of residual layer provides useful information for the design of the process conditions of imprinting processes.

Surface discharge Characteristics of epoxy resin in different media (이종매질 내 에폭시수지의 연면방전특성)

  • Park, He-Rie;Lee, Jung-Hwan;Choi, Eun-Hyeok;Jang, Seung-Ho;Lee, Sang-Ho;Lee, Kwang-Sik
    • Proceedings of the Korean Institute of IIIuminating and Electrical Installation Engineers Conference
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    • 2009.10a
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    • pp.301-303
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    • 2009
  • This paper presents a basic data of the surface discharge characteristics of solid dielectric in various gas including $SF_6$ and environmentally friendly gas as Dry-Air and $N_2$ gas. Used electrodes are needle and plane. Used solid dielectric which is installed between the electrodes is made of epoxy resin and is disc form of 100[mm] diameter and 2, 3[mm] thickness. AC In same condition, we can obtain different surface dielectric strength. Increased pressure and thickness caused increased surface dielectric strength.

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Tensile Properties of Plain Weave Glass Fabric Reinforced Epoxy Resin Laminates at Low Temperatures (평직유리섬유 강화 에폭시 적층판의 저온 인장 특성)

  • Kim, Yon-Jig
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.32 no.9
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    • pp.788-795
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    • 2008
  • To understand the tensile behaviors of GFRP at low temperature, three types of specimen have been used in this study. Tensile properties and fracture mechanisms for three orthogonal orientations of plain weave glass fabric reinforced epoxy resin laminate were investigated at temperature range of about -30 to $15^{\circ}C$. The tensile properties of axial and edge type specimen decrease slightly with decreasing temperature to $-20^{\circ}C$. However, at $-30^{\circ}C$ the decreases in the tensile properties increased considerably. Below $-20^{\circ}C$, thickness type specimen showed a marked decreases in the tensile properties. It was obvious that the fracture manner of thickness type specimen was adhesive failure at above $-10^{\circ}C$ and a mixed adhesive and cohesive failure at below $-20^{\circ}C$.

Measurement of Molecular Weights of Melamine-Urea-Formaldehyde Resins and Their Influences to Properties of Medium Density Fiberboards

  • Jeong, Bora;Park, Byung-Dae
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.6
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    • pp.913-922
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    • 2016
  • This study attempted to measure molecular weight (MW) of melamine-urea-formaldehyde (MUF) resins prepared by two different synthesis methods: the one-step MUF resins were synthesized in one batch procedure, while the two-step MUF resins were prepared by a physical mixing of urea-formaldehyde (UF) resin with melamine-formaldehyde (MF) resin that had been synthesized in a separate procedure. The properties of medium density fiberboard (MDF) panels bonded with two types of MUF resins were also investigated. MWs of these MUF resins were measured using gel permeation chromatography (GPC). In addition, this study measured the MWs of one-step MUF resin during its synthesis procedure. The performance of two types of MUF resins was evaluated by determining properties of MDF panels prepared in laboratory. As the synthesis procedure progressed, both number average MW ($M_n$) and weight average MW ($M_w$) of one-step MUF resin gradually increased, while the polydispersity index (PDI) decreased. And low Mw species of the resin predominantly decreased as the synthesis step progressed. The one-step MUF resin showed greater $M_n$ and $M_w$ than those of the two-step ones even though the PDI values of both resins were very similar each other. As expected, the one-step MUF resin resulted in better properties of MDF panels than those of two-step resins. In particular, the one-step MUF resin provided better internal bond (IB) strength and thickness swelling (TS) with MDF panels than those of two-step ones, indicating better water resistance of the one-step resin. These results suggest that the preparation method of MUF resins have a great impact on the MW and final panel properties.

Curing efficiency of various resin-based materials polymerized through different ceramic thicknesses and curing time

  • Lee, Jung-Won;Cha, Hyun-Suk;Lee, Joo-Hee
    • The Journal of Advanced Prosthodontics
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    • v.3 no.3
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    • pp.126-131
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    • 2011
  • PURPOSE. The aim of this in vitro study was to examine the curing efficiency of various resin-based materials polymerized through ceramic restorations with 3 different thicknesses. Curing efficiency was evaluated by determining the surface microhardness (VHN) of the resin specimens. MATERIALS AND METHODS. Four kinds of resin materials were used. Z350 (3M ESPE $Filtek^{TM}$ Z350: A2 Shade), Z250 (3M ESPE $Filtek^{TM}$ Z250: A2 Shade) and $Variolink^{(R)}$ II (VL: Ivoclar vivadent, base: transparent) either with or without a self-curing catalyst (VLC: Ivoclar vivadent, catalyst: low viscosity/transparent) were filled into the silicone mold (10 mm diameter, 1 mm thick). They were cured through ceramic discs (IPS e.max Press MO-0 ingot ivoclar vivadent, 10 mm diameter, 0.5, 1 and 2 mm thicknesses) by LED light-curing units for 20 and 40 seconds. Vicker's microhardness numbers (VHNs) were measured on the bottom surfaces by a microhardness tester. Data were analyzed using a 3-way analysis of variance (ANOVA) at a significance level of 0.05. RESULTS. The thickness of ceramic disc increased, the VHNs of all four resin types were decreased (P<.05). The mean VHN values of the resins light cured for 40 seconds were significantly higher than that of LED for 20 seconds in all four resin materials (P<.05). VLC showed significantly higher VHN values than VL regardless of other conditions (P<.05). Z350 and Z250 showed higher values than VL or VLC (P<.01). CONCLUSION. Thinner ceramic disc with increased curing time resulted higher VHN values of all resin materials. The use of a catalyst produced a greater hardness with all polymerization methods. Restorative resin materials (Z350, Z250) showed higher VHN values than resin cement materials (VL, VLC).

Bonding of conventional provisional resin to 3D printed resin: the role of surface treatments and type of repair resins

  • Lim, Na-Kyung;Shin, Soo-Yeon
    • The Journal of Advanced Prosthodontics
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    • v.12 no.5
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    • pp.322-328
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    • 2020
  • PURPOSE. This study evaluated the shear bond strength between 3D printed provisional resin and conventional provisional resin depending on type of conventional provisional resin and different surface treatments of 3D printed resin. MATERIALS AND METHODS. Ninety-six disc-shaped specimens (Ø14 mm × 20 mm thickness) were printed with resin for 3D printing (Nextdent C&B, Vertex-Dental B. V., Soesterberg, Netherlands). After post-processing, the specimens were randomly divided into 8 groups (n=12) according to two types of conventional repair resin (methylmethacrylate and bis-acryl composite) and four different surface treatments: no additional treatment, air abrasion, soaking in methylmethacrylate (MMA) monomer, and soaking in MMA monomer after air abrasion. After surface treatment, each repair resin was bonded in cylindrical shape using a silicone mold. Specimens were stored in 37℃ distilled water for 24 hours. The shear bond strength was measured using a universal testing machine at a crosshead speed of 0.5 mm/min. Failure modes were analyzed by scanning electron microscope. Statistical analysis was done using one-way ANOVA test and Kruskal-Wallis test (α=.05). RESULTS. The group repaired with bis-acryl composite without additional surface treatment showed the highest mean shear bond strength. It was significantly higher than all four groups repaired with methylmethacrylate (P<.05). Additional surface treatments, neither mechanical nor chemical, increased the shear bond strength within methylmethacrylate groups and bis-acryl composite groups (P>.05). Failure mode analysis showed that cohesive failure was most frequent in both methylmethacrylate and bis-acryl composite groups. CONCLUSION. Our results suggest that when repairing 3D printed provisional restoration with conventional provisional resin, repair with bis-acryl composite without additional surface treatment is recommended.

Color quality evaluation of composite resins used for splinting teeth (동요치 고정에 사용되는 복합레진의 색품질 평가)

  • Jung, Ji-Hye;Cheon, Kyeong Jun;Oh, Yonghui;Chang, Hoon-Sang
    • Journal of Korean Society for Quality Management
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    • v.45 no.4
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    • pp.995-1002
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    • 2017
  • Purpose: The purpose of this study was to evaluate the color stability of composite resins used for splinting teeth by comparing a self-cure resin cement (Superbond C&B, SB), a flowable composite resin (G-aenial Universal Flo A2, GU), and a composite resin exclusively used for splinting teeth (G-Fix, GF) before and after aging in NaOCl. Methods: Resin samples were fabricated to a size of 2 mm thickness and 8.5 mm diameter and light-cured with an LED light curing unit (G-Light, n = 12). Immediately after fabrication, CIE L*a*b* values of the resin samples were measured with a spectrophotometer (CM-5) as baseline. Then, the resin samples were immersed in 5% NaOCl at $60^{\circ}C$ and the color was measured after 23 hours every day for 4 days. Data were analyzed with one-way ANOVA followed by Duncan post hoc test (p<0.05), and color differences (${\Delta}E$) of resin samples before and after NaOCl aging were also calculated. Results: For SB, there were no changes in L* and a* values but changes were observed in b* values. For GU, there were no changes in L* and b* values but in a* values. For GF, changes were observed in L*, a*, and b* values. All resin samples showed highest ${\Delta}E$ between baseline and the 1st day of NaOCl immersion. ${\Delta}E$ of SB, GU, and GF was 4.6 - 5.8, 4.9 - 7.9, and 9.9 - 16.9, respectively. GF showed highest color change during NaOCl aging. Conclusion: The results of this color quality evaluation showed that the composite resin exclusively used for splinting teeth might be more vulnerable to color change during intraoral service.

Comparison of light-transmittance in dental tissues and dental composite restorations using incremental layering build-up with varying enamel resin layer thickness

  • Rocha Maia, Rodrigo;Oliveira, Dayane;D'Antonio, Tracy;Qian, Fang;Skif, Frederick
    • Restorative Dentistry and Endodontics
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    • v.43 no.2
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    • pp.22.1-22.9
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    • 2018
  • Objectives: To evaluate and compare light-transmittance in dental tissues and dental composite restorations using the incremental double-layer technique with varying layer thickness. Materials and Methods: B1-colored natural teeth slabs were compared to dental restoration build-ups with A2D and B1E-colored nanofilled, supra-nanofilled, microfilled, and microhybrid composites. The enamel layer varied from 0.3, 0.5, or 1.2 mm thick, and the dentin layer was varied to provide a standardized 3.7 mm overall sample thickness (n = 10). All increments were light-cured to $16J/cm^2$ with a multi-wave LED (Valo, Ultradent). Using a spectrophotometer, the samples were irradiated by an RGB laser beam. A voltmeter recorded the light output signal to calculate the light-transmittance through the specimens. The data were analyzed using 1-way analysis of variance followed by the post hoc Tukey's test (p = 0.05). Results: Mean light-transmittance observed at thicker final layers of enamel were significantly lower than those observed at thinner final layers. Within 1.2 mm final enamel resin layer (FERL) thickness, all composites were similar to the dental tissues, with exception of the nanofilled composite. However, within 0.5 mm FERL thickness, only the suprananofilled composite showed no difference from the dental tissues. Within 0.3 mm FERL thickness, none of the composites were similar to the dental tissues. Conclusions: The supra-nanofilled composite had the most similar light-transmittance pattern when compared to the natural teeth. However, for other composites, thicker FERL have a greater chance to match the light-transmittance of natural dental tissues.

THE EFFECT OF HYBRID LAYER THICKNESS ON MICROTENSILE BOND STRENGTH OF THREE-STEP AND SELF-ETCHING DENTIN ADHESIVE SYSTEMS (혼성층의 두께가 three-step과 self-etching 상아질 접착제의 미세인장결합강도에 미치는 효과)

  • Lee, Hye-Jung;Park, Jeong-Kil;Hur, Bock
    • Restorative Dentistry and Endodontics
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    • v.28 no.6
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    • pp.491-497
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    • 2003
  • The purpose of this study was to evaluate the correlation between hybrid layer thickness and bond strength using confocal laser scanning microscope and microtensile bond strength test of two adhesive systems. The dentin surface of human molars. sectioned to remove the enamel from the occlusal surface. Either Scotchbond Multi-Purpose(3M Dental Product, St. Paul, MN, U.S.A) or Clearfil SE Bond (Kuraray, Osaka, Japan) was bonded to the surface. and covered with resin-composite. The resin-bonded teeth were serially sliced perpendicular to the adhesive interface to measure the hybrid layer thickness by confocal laser scanning microscope. The specimen were trimmed to give a bonded cross-sectional surface area of $1\textrm{mm}^2$, then the micro-tensile bone test was performed at a cross head speed of 1.0 mm/min. All fractured surfaces were also observed by stereomicroscope. There was no significant differences in bond strengths the materials(p>0.05). However. the hybrid layers of three-step dentin adhesive system, SM, had significantly thicker than self-etching adhesive system. CS(p<0.05). Pearson's correlation coefficient showed no correlation between hybrid layer thickness and bond strengths(p>0.05). Bond strengths of dentin adhesive systems were not dependent on the thickness of hybrid layer.