• Title/Summary/Keyword: Resin composite

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High Temperature Tensile Stress Behavior of Hydrogen Vessel Composite Materials for Hydrogen Fuel Cell Bus (수소버스용 내압용기 복합재의 열적환경에 따른 기계적 물성 연구)

  • Hyunseok, Yang;Woo-Chul, Jung;Kwang Bok, Shin;Man-Sik, Kong
    • Composites Research
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    • v.35 no.6
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    • pp.425-430
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    • 2022
  • In this study, the mechanical properties of the pressure vessel composite exposed to the thermal environment were evaluated to establish the standard for high temperature static pressure test of the pressure vessel for hydrogen bus. As the tensile strength of the composite material approaches the glass transition temperature of the epoxy resin, the strength decreases due to the deterioration of the epoxy resin. In addition, it was confirmed that the tensile strength increased again due to the post-curing of the epoxy resin during long-term exposure. Therefore, the accelerated stress rupture test conditions of the pressure vessel for the hydrogen bus should be set based on the epoxy resin properties of the carbon fiber composite material.

EFFECT OF GOLD ELECTRODEPOSIT OF PD-AG, NI-CR ALLOYS ON THE COLOR OF VENERRED RESIN (Pd-Ag 및 Ni-Cr 합금의 금 전착이 전장 레진의 색채에 미치는 영향)

  • Yang, Hong-So;Park, Yeong-Joon
    • The Journal of Korean Academy of Prosthodontics
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    • v.33 no.4
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    • pp.645-661
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    • 1995
  • As the mechanical property of composite resin improved, composite resin has been widely used esthetic dentistry. In the field of esthetic dentistry, the color of prosthetic material is very important. The purpose of this study was to evaluate the color difference of specimens, by the types of alloys and gold electrodeposit. Experimental groups were as follows : Group Prec : Au-Pt alloy with no gold coating and no resin veneer. Group Semi : Pd-Ag alloy with no gold coating and no resin veneer. Group BAse : Ni-Cr alloy with no gold coating and no resin veneer. Group Gsem : Pd-Ag alloy with no gold coating and no resin veneer. Group Gbas : Ni-Cr alloy with no gold coating and no resin veneer. Group PreR : Resin veneer on the Pd-Ag alloy without gold coating. Group SemR : Resin veneer on the Pd-Ag alloy without gold coating. Group GbsR : Resin veneer on the Ni-Cr alloy with gold coating Group BasR : Resin veneer on the Ni-Cr alloy without gold coating. In this study, colors of metal surfaces and veneered resins were evaluated by the CIE $L^{*}a^{*}b$ system. The results obtained were as follows : 1. different alloy types and gold coating make the $L^{*}a^{*}b$ system. 2. The ${\Delta}E^*$ab value between groups semi and Base was less than 1.5 and there was no $a^*$ and $b^*$ value difference between groups Gsem and Gbas 3. The values of $L^*$ and $a^*$ ain groups GsemR and GbasR were so similar that the ${\Delta}E^*$ab value was as small as 0.58. 4. In resin specimens with gold coated semiprecious or base alloys showed yellower and redder deviation than the resin specimens with precious alloy. 5. The ${\Delta}E^*$ab values between goups PreR-GsemR and groups PreR-GbasR were as small as 2.68 and 2.22 respectively.

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A STUDY ON THE VOND STRENGTH OF PORCELAIN LAMINATE AND COMPOSITE RESIN CEMENTS (라미네이트 도재와 복합레진 시멘트의 결합강도에 관한 연구)

  • Kim, Sung-Il;Lim, Ho-Nam;Park, Nam-Soo
    • The Journal of Korean Academy of Prosthodontics
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    • v.29 no.1
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    • pp.91-109
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    • 1991
  • The purpose of this study were to comfirm the effects of the thickness and kinds of porcelain, etchants, illumination time, elapsed time for the measurement, and chemical cure component to the bond strength of porcelain laminate and composite resin cement, and to compare the effects between the light cured resin and the dual cured resins. The etched porcelain surface, the sectioned surface crossing porcelain and resin after bonding, and the debonded surfaces were observed by the SEM. One product of laminate porcelain powder, one light cured resin and two dual cured resins were selected. Each resin cements are lightened through the thin porcelain disc which was cut from cylindrical porcelain specimen by the diamond saw, and by the light through the porcelain disc they were bonded. Changes of thickness and kinds of porcelain, etchants, illumination time, and the elapsed time for the measurement were considered as variables for the bond strength. And the bond strength of porcelain and dual cured resins under the conditions of autopolymerization or the removal of chemical cure component were measured and compared. Bond strength were measured by shear stress. The etched surface, the cross-sectioned surface, and the debonded surface of porcelain or resin were observed by SEM. On the summary of this study, the following conclusions can be stated; 1. Bond strength of light cured resin was decreased inversely by the thickened porcelain laminate and showed the lowest value to the masking dentin porcelain among 4 kinds of porcelain powder. 2. Bond strength of autopolymerization of dual cured resin without illumination in dark chamber were from 75% to 98% to the data of dual cured resin with illumination. 3. Bond strength of dual cured resin used without chemical cured components were same to them of light cured resin. 4. Cross-sectioned surface treated by silane did not show the gap between the porcelain and resin. 5. Illumination over 80 seconds did not make the significant increase of bond strength on all kinds of resin.

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A STUDY ON MICROLEAKAGE OF COMPOSITE RESIN AFTER SURFACE TREATMENT (표면 처리방법에 따른 복합레진의 미세누출에 관한 실험적 연구)

  • Lee, Chang-Woo;Kim, Jung-Wook;Lee, Sang-Hoon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.25 no.1
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    • pp.103-115
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    • 1998
  • Adhesion of composite resin to tooth structure has been of tremendous signgicance in clinical dentistry. Due to the lack of adhesion between composite restorative resins and enamel and dentin, microleakage occurs at the tooth/restoration interface. This may lead to discoloration, secondary caries, marginal breakdown, postoperative sensitivity, and even pulpal pathology. According to extensive use of composite resin, every effort on improving bonding strength and reducing microleakage between a tooth and composite resin has been continued. This study was conducted to determine the difference in microleakage in enamel and dentin treated with air-abrasion, acid etching and combination when restored with composite resin. Class V cavities were prepared on 30 premolars. The specimens were divided into following groups. group 1:air-abrasion+Scotchbond Multi-purpose group 4 :air-abrasion+All-Bond 2 group 2:acid etching+Scotchbond Multi-purpose group 5 :acid etching+All-Bond 2 group 3:combination+Scotchbond Multi-purpose group 6 :combination+All-Bond 2 #combination:air-abrasion + acid etching The specimens were filled with Z-100 after application of Scotchbond Multi-purpose and All-Bond 2. Thermocycling was conducted by alternately dipping the specimens in $5^{\circ}C$ and $55^{\circ}C$ water for 30 seconds 500 times. 1% methylene blue was applied and the specimens were left for 24 hours at $37^{\circ}C$. After washing out the dye, the tooth was sectioned buccolingually along the axis. The sectioned surface was observed with stereoscope for dye penetration. The author has measured the microleakage in teeth prepared with air-abrasion, acid ethching and combination to study the difference in microleakage following different methods of tooth surface treatment and has come to following results. 1. In comparing microleakage between groups, group 1 and 4 showed statistically significant difference from group 2, 3, 5 and 6(p<0.05). There was no significant difference among group 2, 3, 5, 6(p>0.05) nor between group 1 and 4(p>0.05). 2. In comparing microleakage among tooth surface treatment methods, Air-abrasion group showed significantly more microleakage than acid etching group and combination(airabrasion + acid etching) group(p<0.05). Combination(acid etching+air-abrasion)group tended to show lesser microleakage than acid etching group, but this was not statistically significant(p>0.05). 3. In comparing microleakage between bonding agents, there was no statistically significant difference between Scotch bond Multi-purpose and All-Bond 2(p>0.05).

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Characteristics according to the Amount of HAp Added in Resin for Tooth Repair

  • Hwang, Sungu;Lim, Jinhyuck;Ryu, Suchak
    • Journal of the Korean Ceramic Society
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    • v.56 no.6
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    • pp.521-525
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    • 2019
  • A study was conducted to investigate the possibility of a composite material containing a composite resin as a matrix and hydroxyapatite (HAp) powder as a substitute material for tooth repair. As the content of HAp increased, hardness value (111.9 HV at 9%) increased and flexural strength (73.3 MPa at 9%) decreased. Observation of the microstructure after immersion in a simulated body fluid (SBF) solution confirmed a dense structure due to mutual coagulation and curing. It was thought that fine HAp recrystals were formed with the lapse of time, and they were entangled to form a condensation structure and had a dense structure. In addition, since the activity was shown by the ion migration on the surface of a tooth, it was highly likely that a biocompatible bond occurred during tooth contact. Therefore, it could be used as a substitute material for tooth repair.

THE RETENTION OF FULL VENEER GOLD CROWN BY CORE MATERIAL AND DENTAL CEMENT (Core와 시멘트의 종류가 전부주조금관의 유지력에 미치는 영향)

  • Ha Jum-Im;Cho Hye-Won;Dong Jin-Keun
    • The Journal of Korean Academy of Prosthodontics
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    • v.30 no.1
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    • pp.93-101
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    • 1992
  • The purpose of this study was to evaluate the effectiveness of core materials and luting agents on the retention of full veneer gold crown. The core materials used in this study was dental amalgam, and composite resin, and the luting agents were zinc phosphate cement, polycarboxylate cement, and glass ionomer cement. The obtained results were as follows. 1. In full veneer gold crown supported by composite resin core, the crown retention with zinc phosphate cement was the highest of all. 2. In full veneer gold crown supported by amalgam core, the crown retention was shown no statistical difference by luting agent. 3. There was no statistical difference in the crown retention between the full veneer gold crown supported by composite resin core and dental amalgam core.

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The effect of irradiation mode on degree of cure, shrinkage and microleakage of composite resin restoration.

  • Park, Jong-Jin;Park, Jeong-Won;Kim, Sung-Kyo
    • Proceedings of the KACD Conference
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    • 2001.11a
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    • pp.558.2-558
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    • 2001
  • The aims of this study are (1) to investigate the relation of irradiation mode, polymerization shrinkage and degree of cure of composite resin and(2) it effect on micorleakage of class V restorations. VIP(BISCO Dental Products, Schaumburg, IL, USA) and Optilux 501 (Demetron/Kerr, Danbury, CT, USA) curing lights were used for curing Z-250 composite resin following irradiation mode: VIP 200㎽d, VIP 400㎽, VIP 600㎽, pulse-delay(200㎽ 3sec, 5min wait, 600㎽ 30sec), Optilux R mode.(omitted)

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BONDING STRENGTH OF GLASS-IOMOMER CEMENT AND COMPOSITE RESIN COMBINATION (Glass ionomer cement의 상아질 결합력에 관한 연구)

  • Um, Chung-Moon;Oilo, Gudbrand
    • Restorative Dentistry and Endodontics
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    • v.19 no.2
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    • pp.633-640
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    • 1994
  • The tensile bond strength to dentin was measured for three glass-ionomer cement and composite resin combinations: two light-curing glass-ionomer cements(Vitrebond and XR - Ionomer) and one traditional glass - ionomer cement(Ketac - Bond), two adhesive systems(Scotchbond, and XR - Bonding System), and a corresponding composite resin. The bond strength of this "sandwich" was also compared with that of the same cements used in bulk. Vitredbond showed a significantly higher bond strength in bulk than did the other two cements. Of the sandwiches, the XR - Iomomer and XR - Bond combination showed a bond strength significantly higher than that of the Vitrebond and Scotchbond or Ketac- bond and Scotchbond combination. The fracture of the bond was mainly adhesive for Vitrebond, cohesive for XR - Ionomer when used in bulk and adhesive - cohesive when used in a sandwich, and cohesive for Ketac-Bond.

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The effect of irradiation mode on degree of cure, shrinkage and microleakage of composite resin restroation.

  • Park, Jong-Jin;Park, Jeong-Won;Kim, Sung-Kyo
    • Proceedings of the KACD Conference
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    • 2001.11a
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    • pp.555-555
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    • 2001
  • The aims of this study are (1) to investigate the relation of irradiation mode, polymerzition shrinkage and degree of cure of composite resin and (2) it effect on microliakage of calss V restorations. VIP(BISCO Dental Products, Schaumburg, IL, USA) and Optilux 501(Demetron/Kerr, Danbury, CT, USA) curing lights were used for curing Z-250 composite resin following irradiation mode: VIP 200㎽, VIP 400㎽, VIP 600㎽, pulse-delay(200㎽ 3sec, 5min wait, 600㎽ 30sec), Optilux C mode, Optilux R mode.(omitted)

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The Effects of Polyurethane Resin on the Water Stability of HAC/PVA Based MDF Cement Composites (Polyurethane 첨가에 의한 HAC/PVA계 MDF 시멘트 복합재료의 수분안정성 영향)

  • 박춘근;김태진;김병권;엄태형;노준석;최상흘
    • Journal of the Korean Ceramic Society
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    • v.34 no.10
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    • pp.1037-1044
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    • 1997
  • Mechanical properties and water stability of HAC/PVA based MDF cement composite were investigated using polyurethane(PU) resin, silane coupling agent and various PVA. The results were as follows ; The flexural strength of MDF cement composite increased as increasing with PVA content. Low-viscosity PVA developed higher flexural strength than high-viscosity PVA under a drying curing condition. But the strength of water immersed specimen decreased. Water stability of MDF cement improved as increasing with content of PU. Consequently, water stability of polyurethane 7% added MDF cement was about 2 times higher than that of the controlled specimen. Furthermore, the strength and water stability of diamine group based silane couling agent in using MDF cement increased and improved dramatically.

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