• 한국진공학회:학술대회논문집
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• 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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• pp.313-313
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• 2013

For high-performance TFT (Thin film transistor), poly-crystalline semiconductor thin film with low resistivity and high hall carrier mobility is necessary. But, conventional SPC (Solid phase crystallization) process has disadvantages in fabrication such as long annealing time in high temperature or using very expensive Excimer laser. On the contrary, MIC (Metal-induced crystallization) process enables semiconductor thin film crystallization at lower temperature in short annealing time. But, it has been known that the poly-crystalline semiconductor thin film fabricated by MIC methods, has low hall mobility due to the residual metals after crystallization process. In this study, Ni metal was shallow implanted using PIII&D (Plasma Immersion Ion Implantation & Deposition) technique instead of depositing Ni layer to reduce the Ni contamination after annealing. In addition, the effect of external magnetic field during annealing was studied to enhance the amorphous silicon thin film crystallization process. Various thin film analytical techniques such as XRD (X-Ray Diffraction), Raman spectroscopy, and XPS (X-ray Photoelectron Spectroscopy), Hall mobility measurement system were used to investigate the structure and composition of silicon thin film samples.

• 분석과학
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• 제33권1호
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• pp.11-22
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• 2020

When extracting semi-volatile components of herbal medicines using hot water vapor, some substances may react with water vapor or oxygen, and some volatile substances may be lost, when using an organic solvent extraction method has the disadvantage that it may contain a non-volatile material and residual organic solvent. In addition, it is inefficient to separate semi-volatile substances from herbal medicines into each single component and conduct biological activity research for each component to determine the effective ingredient, and some components may be lost in the separation process. In this study, semi-volatile substances evaporated under two pressure-reduced conditions in Chinese herbal medicines such as Cnidii Rhizoma, Aucklandiae Radix and Amomum Fructus were separated by cooling with liquid nitrogen. Those were analyzed by gas chromatography-mass spectrometry (GC-MS) to identify the components, and this method may be used to study biological activities at the cellular level. The substances separated under reduced pressure, essential oil obtained by simultaneous distillation extraction (SDE) method and substances by using solid phase micro-extraction (SPME) from Cnidii Rhizoma, Aucklandiae Radix and Amomum Fructus were analyzed by GC-MS. In the case of Cnidii Rhizoma and Aucklandiae Radix, there were some differences among the essential oil components obtained by SDE and those identified by low temperature capture (CT) and SPME method, these were believed to be produced by some volatiles reacting with water or oxygen at the boiling point temperature of water.

• 한국환경농학회지
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• 제24권2호
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• pp.98-105
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• 2005

Groundwater sampled from 24 tube wells of three districts namely Sherpur, Gaibandha and Naogaon in Bangladesh was appraised for their water quality for irrigation and agro-based industrial usage. All waters under test were slightly alkaline to alkaline (pH = 7.2 to 8.4) in nature and were not problematic for crop production. As total dissolved solid (TDS), all groundwater samples were classified as fresh water (TDS<1,000 mg/L) in quality. Electrical conductivity (EC) and sodium adsorption ratio (SAR) values reflected that waters under test were under medium salinity (C2), high salinity (C3) and also low alkalinity (S1) hazard classes expressed as C2S1 and C3S1. As regards to EC and soluble sodium percentage (SSP), groundwater samples were graded as good and permissible in category based on soil properties and crop growth. All water samples were free from residual sodium carbonate (RSC) and belonged to suitable in category. Water samples were under soft moderately hard, hard and very hard classes. Manganese, bicarbonate and nitrate ions were considered as major pollutants in some water samples and might pose threat in soil ecosystem for long-term irrigation. For most of the agro-based industrial usage, Fe and Cl were considered as troublesome ions. On the basis of TDS and hardness, groundwater samples were not suitable for specific industry. Some water samples were found suitable for specific industry but none of these waters were suitable for all industries. The relationship between water quality parameters and major ions was established. The correlation between major ionic constituents like Ca, Mg, K, Na, $HCO_3$ and Cl differed significantly. Dominant synergistic relationships were observed between EC-TDS, SAR-SSP, EC-Hardness, TDS-Hardness and RSC-Hardness.

• 한국식품과학회지
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• 제28권5호
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• pp.870-876
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• 1996

가시발새우 껍질을 부가가치가 높은 자원으로 활용하기 위하여, 이들로부터 키틴과 키토산을 제조하여 물리화학적 특성을 살펴 보았다. 가시발새우 껍질에서 추출한 키틴의 일반성분은 질소 6.84%, 지방 0.57%, 회분 0.32%였으며, 수율은 15.7%였다. 키토산은 질소함량이 7.52%였으며 지방과 회분함량은 각각 0.13%와 0.33%였다. 그리고 탈아세틸화도는 67.5%, 분자량은 $9.1{\times}10^5$이었으며 수율은 75%를 나타내었다. 키틴 및 키토산의 잔류 아미노산은 각각 2.64mg/g과 1.39mg/g 검출되었고, 그 중 lysine이 가장 높게 나타났다. 한편 키틴과 키토산의 IR 스펙트럼과 고체상태 $^{13}C-NMR$ 스펙트럼 data는 분자구조를 확인하는데 도움이 되었다.

• 청정기술
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• 제12권3호
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• pp.151-156
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• 2006

염색폐수 처리를 위해 세라믹 정밀여과막 (MF)과 고분자 한외여과막 (UF)의 복합공정을 적용, 색도 및 유기물 (TOC) 제거율을 통해 공정을 최적화하고, 염색폐수의 분리효율을 조사하였다. 막 회복을 통한 운전 효율향상을 위해 역세척과 화학세정을 수행한 결과, 역세척에 의한 정밀여과막은 2분 주기로 1초 동안 역세척하였을때 투과수량이 10.3% 증가하였고, 한외여과막은 0.1% 수산화나트륨 용액으로 화학세정하였을 때 97%의 회복률을 나타내었다. 이때, 유기물, 색도, 부유물질(SS)의 제거율은 각각 84.6%, 97.4% 및 100%를 나타내었다. 분 복합공정의 적용은 염색폐수의 색도와 유기물 제거에 효과적임을 확인할 수 있었다.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2010년도 제39회 하계학술대회 초록집
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• pp.157-157
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• 2010

Vertical-structure light-emitting diodes (V-LEDs) by laser lift-off (LLO) have been exploited for high-efficiency GaN-based LEDs of solid-state lightings. In V-LEDs, emitted light from active regions is reflected-up from reflective ohmic contacts on p-GaN. Therefore, silver (Ag) is very suitable for reflective contacts due to its high reflectance (>95%) and surface plasmon coupling to visible light emissions. In addition, low contact resistivity has been obtained from Ag-based ohmic contacts annealed in oxygen ambient. However, annealing in oxygen ambient causes Ag to be oxidized and/or agglomerated, leading to degradation in both electrical and optical properties. Therefore, preventing Ag from oxidation and/or agglomeration is a key aspect for high-performance V-LEDs. In this work, we demonstrate the enhanced thermal stability of Ag-based Ohmic contact to p-GaN by reducing the thermal compressive stress. The thermal compressive stress due to the large difference in CTE between GaN ($5.6{\times}10^{-6}/^{\circ}C$) and Ag ($18.9{\times}10^{-6}/^{\circ}C$) accelerate the diffusion of Ag atoms, leading to Ag agglomeration. Therefore, by increasing the additional residual tensile stress in Ag film, the thermal compressive stress could be reduced, resulting in the enhancement of Ag agglomeration resistance. We employ the thin Ni layer in Ag film to form Ni/Ag mutli-layer structure, because the lattice constant of NiO ($4.176\;{\AA}$ is larger than that of Ag ($4.086\;{\AA}$). High-resolution symmetric and asymmetric X-ray diffraction was used to measure the in-plane strain of Ag films. Due to the expansion of lattice constant by oxidation of Ni into NiO layer, Ag layer in Ni/Ag multi-layer structure was tensilely strained after annealing. Based on experimental results, it could be concluded that the reduction of thermal compressive stress by additional tensile stress in Ag film plays a critical role to enhance the thermal stability of Ag-based Ohmic contact to p-GaN.

• Journal of the Korean Wood Science and Technology
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• 제16권4호
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• pp.3-9
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• 1988

Infrared (IR) spectroscopic techniques for the analysis of wood samples and the absorbance spectra of solid woods were presented. KBr pellets were prepared by throughly mixing approximately 300 mg of dried KBr and 1 mg of finely milled wood powder extracted with ethanol-cyclohexane previously. This mixture was made into a transparent disc by means of a pellet-making die (10 ton/$cm^2$ for 10 min). This IR techniques were applied for the analysis of archaeological wood samples. The most notable difference in the IR spectra between the recent and the archaeological waterlogged woods is that the absorption band centered at $1,730cm^{-1}$ was significantly diminished in the waterlogged ones. Total loss of absorption in $1,730cm^{-1}$ might be mainly due to the result of hemicellulose degradation. Another feature indicated by IR spectral comparision are that the degraded waterlogged wood samples showed 1) the increased intensity of the 1,600, 1,500 and $1,270cm^{-1}$ due to the residual lignin and the increased intensity at 1,470 and $1,425cm^{-1}$ due to the degradation of hemicellulose and 2) to the emergence of single band around $1,050cm^{-1}$ instead of three bands at 1,110, 1,060 and $1,040cm^{-1}$ in recent wood due to the degradation of cellulose crystalline. It was revealed from the IR examinations that the first change of wood in the waterlogged situation was the lysis of hemicellulose and the second the lysis of cellulose. It was also suggested that IR spectroscopy could serve a fast method for the investigation on the chemical characteristics of archaeological wood samples.

• 한국해양학회지
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• 제28권2호
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• pp.86-100
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• 1993

ADI(Alternating Direction Implicit) 유한차분법을 사용하여 3차원 경합 해수유 동 모델 BACHOM-3을 개발하였다. 본 모델을 장방형 내만에서 하나의 결점을 갖는 정상 파에 적용하여 해석해와 비교하였으며, 그 결과 해석해와 잘 일치하였다. 모델의 현지 적용성과 수영만의 해수유동을 조사하기 위해 모델을 수영만에 적용하여 대조기 평수 시 현지관측결과와 비교하였으며, 그 결과 현지 관측결과와 비교적 잘 일치하였다. 만 중앙부의 제 1층(수심 0∼2 m)과 제 2층(수심 2∼5 m)에서 조석잔차류는 시계방향으로 회전하는 순환류가 나타났으며, 또한 낙조류가 창조류보다 강하게 나타났다. 계산된 유속분포에 의하면, 표층과 저층 사이에 유속의 위상차가 나타나며, 표층으로 갈수록 위상의 지연이 나타났다. 그리고, 본 모델을 홍수시와 바람 효과를 고려한 흐름 장의 계산에도 적용하였다. 해양에서 육지로 바람이 불 때 표층에서는 풍향에 대응하는 유 속분포를 나타냈으나, 저층의 육지경계부근에서는 풍향과 반대방향의 흐름이 나타났 다.

• 한국구조물진단유지관리공학회 논문집
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• 제16권5호
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• pp.88-97
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• 2012

본 연구에서는 비내진 교각의 내진성능과 휨-전단 거동을 파악하고자 형상비 4.5인 정사각형의 중실 및 중공단면 철근콘크리트 교각실험체를 제작하여 일정한 축력하에서 변위비 등급을 증가시켜 가면서 횡하중을 가력하는 실험을 수행하였다. 본 연구는 철근콘크리트 교각의 한정연성 내진설계를 위한 실험적 기초자료의 제공과 함께 성능단계별 교각성능 및 손상평가를 위한 정량적 수치와 경향을 제공하기 위한 것이며, 파괴거동, 극한변위, 극한드리프트비율, 변위연성도, 응답수정계수, 등가점성감쇠비, 잔류변형지수, 유효강성, 철근 변형률 등의 주요 내진성능 인자들에 대한 분석결과와 비선형 해석 결과를 나타내었다.

• 자원환경지질
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• 제33권4호
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• pp.249-260
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• 2000

한국 남부에서 섭입 해구의 방향과 나란히 쌍으로 발달한 화산대가 발견된다. 경상분지와 영동-광주 함몰대의 화산암류는 거의 나란한 양상을 보이며, 이들은 각각 동일한 섭입 체계에 따르는 첫 번째 화산대, 두 번째 화산대이다. 경상분지와 영동-광주 함몰대 화산암류의 불호정성 원소 함량은 호를 가로지르는 변화를 뚜렷하게 보인다. 즉, 첫 번째 화산대 (경상분지 및 남해안 도서지역)용암들의 불호정성 원소 함량은 두 번째 화산대 (영동-광주 함몰대)에 비해 더욱 결핍되며 두 번째 화산대에서 더욱 증가하는 경향을 보인다. 이와 같이 호를 가로지르는 변화를 보이는 것은, 탈수과정 동안 유체상과 공존하는 고체상의 차이에 기인한 것으로 보인다. 두 번째 화산대의 불호정성 원소의 함량, Zr/Y 비, Rb/K 비는 첫 번째 화산대에 비해 더 깊은 깊이에서 더 적은 정도의 부분 용융, 그리고 용융 과정에서의 잔류 석류석에 기인할 것이다.