• Clean Technology
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• v.28 no.4
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• pp.301-308
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• 2022

Since nanoporous silica aerogel was first synthesized in 1931, its potential as an ultra-lightweight superinsulation material has been steadily attracting attention. Silica aerogel is the best thermal insulation material to date. However, the potential applications of this lightweight material have so far been hindered by its inherent fragibility and brittleness arising from its ultra-porous nature. Although the monolithic form of silica aerogel has the best ultra-lightweight superinsulation properties, it cannot be used in this form. Instead it is used in the form of powders, particles, and blankets. However, these forms still have shortcomings. Silica aerogel is most widely applied in the form of a fiber-reinforced aerogel blanket, but this form is likely to generate dust when handled. Although silica aerogel particles have been proven to be non-toxic to humans, dust formation remains a major barrier to the widespread application of silica aerogel blankets. This paper will investigate the unique properties of silica aerogel and determine what fields it can be used in or potentially be used in due to its unique properties. In addition, we will review the important advances in silica aerogel synthesis technology and its commercialization so far, and then consider the problems that exist for its widespread commercialization in the future and how to overcome them.

• Composites Research
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• v.36 no.3
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• pp.199-204
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• 2023

A combination of a metallic mesh and an adhesive layer of metallic particle/epoxy composite was introduced as an intermediate layer to enhance the adhesion between cold-sprayed particles and fiber-reinforced composites (FRCs). Aluminum was considered for both the metallic particles in the adhesive and the metallic mesh. To predict the mechanical characteristics of the intermediate bond layer under a high strain rate, the properties of the adhesive layer needed to be calculated or measured. Therefore, in this study, the Al particle/epoxy adhesive was homogenized by using a rule of mixture. To verify the homogenization, the penetration depth, and the thickness decrease after the cold spray deposition from the undeformed surface, was monitored with FE analysis and compared with experimental observation. The comparison displayed that the penetration depth was comparable to the diameters of one cold spray particle, and thus the homogenization approach can be reasonable for the prediction of the stress level of particulate polymer composite interlayer under a high strain rate for cold spray processing.

• Korean Journal of Materials Research
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• v.11 no.7
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• pp.590-598
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• 2001

SiCp/pure Al and SiCp/2024Al MMCs were fabricated by in-situ VHP process designed specially just in this study which is composed of the vacuum hot press at range from R.T. to $500^{\circ}C$ and the continuous extrusion without canning process at $520^{\circ}C$. It was investigated the effect of SiC particle size, volume fraction and extrusion ratio on the tensile properties and micro structure in auf composites. In case of the 10:1 extrusion ratio, but SiCp/pure Al and SiCp/2024Al composites were shown a sound appearance and a good micro structure without crack of SiCp as well as uniform distribution of SiCp. However, in case of the 16:1 extrusion ratio, the number of cracked SiC particles more than increased in a higher volume fraction composite and 2024Al matrix composite compared with pure Al matrix one. The tensile strength of the composites reinforced smaller SiCp was higher than that of the bigger SiCp reinforced in same volume fraction and extrusion ratio.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.39 no.2
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• pp.129-135
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• 2015

In this experimental study, the thermal stability values of micrometer-sized silica particle-reinforced epoxy composite specimens were evaluated by measuring their thermal expansion coefficients and Young's moduli. For all specimens used in this study (from the baseline specimen to that containing 70 wt% silica filler), the thermal expansion coefficients and Young's moduli were gradually reduced down to 25% and increased up to 51%, respectively. The results of the experiment were compared with those of certain empirical models. The experimental results of the measurement of thermal expansion coefficients corresponded well with those of Kerner's model, which considers the bulk and shear moduli of the matrix and silica filler. However, the results of the measurement of Young's moduli using the empirical Mori-Tanaka model were observed to match better with those of the experiment. The comparison of the results of the experiment with those of the empirical models demonstrated that a reliable model for measuring the thermal expansion coefficients and Young's moduli of composite specimens needs to consider certain property variations in the composites in addition to volume fraction changes in the filler and matrix.

• Restorative Dentistry and Endodontics
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• v.18 no.1
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• pp.1-26
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• 1993

The purpose of this study was to investigate the effect of acid etching on the surface appearance and fracture toughness of five glass ionomer cements. Five kinds of commercially available glass ionomer cements including chemical curing filling type, chemical curing lining type, chemical curing metal reinforced type, light curing tilling type and light curing lining type were used for this study. The specimens for SEM study were fabricated by treating each glass ionomer cement with either visible light curing or self curing after being inserted into a rubber mold (diameter 4mm, depth 1mm). Some of the specimens were etched with 37% phosphoric acid for 0, 15, 30, 60, go seconds, at 5 minutes, 1 hour and 1 day after mixing of powder and liquid. Unetched ones comprised the control group and the others were the experimental groups. The surface texture was examined by using scanning electron microscope at 20 kV. (S-2300, Hitachi Co., Japan). The specimens for fracture toughness were fabricated by curing of each glass ionomer cement previously inserted into a metal mold for the single edge notch specimen according to the ASTME399. They were subjected to a three-point bend test after etching for 0, 30, 60, and 90 seconds at 5 minutes-, 1 hour-and 1 day-lapse after the fabrication of the specimens. The plane strain fracture toughness ($K_{IC}$) was determined by three-point bend test which was conducted with cross-head speed of 0.5 mm/min using Instron universal testing machine (Model No. 1122) following seven days storage of the etched specimens under $37^{\circ}C$, 100% humidity condition. Following conclusions were drawn. 1. In unetched control group, crack was present, but the surface was generally smooth. 2. Deterioration of the surface appearance such as serious dissolving of gel matrix and loss of glass particles occured as the etching time was increased beyond 15 s following Immediate etching of chemical curing type of glass ionomer cements. 3. Etching after 1 h, and 1 d reduced surface damage, 15 s, and 30s etch gave rough surface appearance without loss of glass particle of chemical curing type of glass ionomer cements. 4. Light curing type glass ionomer cement was etched by acid, but there was no difference in surface appearances according to various waiting periods. 5. It was found that the value of plane stram fracture toughness of glass ionomer cements was highest in the light curing filling type as $1.79\;MNm^{-1.5}$ followed by the light curing lining type, chemical curing metal reinforced type, chemical curing filling type and chemical curing lining type. 6. The value of plane stram fracture toughness of the chemical curing lining type glass ionomer cement etched after 5 minutes was lower than those of the cement etched after 1 hour or day or unetched (P < 0.05). 7. Light curing glass ionomer cement showed Irregular fractured surface and chemical curing cement showed smooth fractured surface.

• Journal of the Korean Recycled Construction Resources Institute
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• v.10 no.1
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• pp.111-116
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• 2022

Recently, building structures tend to be super high-rise and large-scale with the development of concrete technology. When high-rise building is constructed of reinforced concrete structure, it has a disadvantage that its own weight increases. Light weight aggregate(LWA) was developed to compensate for these shortcomings. Manufacturing concrete using these light weight aggregates has the advantage of reducing the self weight of the reinforced concrete structure, but has a disadvantage in that the strength of the concrete is reduced. In this study, an experimental study was conducted to investigate the strength characteristics of hardened cement according to the presence or absence of surface coating of lightweight aggregates. As a result, in terms of compressive strength, the surface-coated lightweight aggregate exhibited higher strength than the uncoated lightweight aggregate. Also, it was considered that this is because the interfacial voids of the surface coated lightweight aggregate mixed cement hardened body were filled with blast furnace slag fine powder particles.

• Journal of the Korean Ceramic Society
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• v.51 no.5
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• pp.392-398
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• 2014

$Al_2O_3$-SiC composites reinforced with SiC whisker ($SiC_w$) were fabricated using three different methods. In the first, $Al_2O_3-SiC_w$ starting materials were used. In the second, $Al_2O_3-SiC_w$-SiC particles ($SiC_p$) were used, which was intended to enhance the mechanical properties by $SiC_p$ reinforcement. In the third method, reaction-sintering was used with mullite-Al-C-$SiC_w$ starting materials. After hot-pressing at $1750^{\circ}C$ and 30 MPa for 1 h, the composites fabricated using $Al_2O_3-SiC_w$ and $Al_2O_3-SiC_w-SiC_p$ showed strong mechanical properties, by which the effects of reinforcement by $SiC_w$ and $SiC_p$ were confirmed. On the other hand, the mechanical properties of the composite fabricated by reaction-sintering were found to be inferior to those of the other $Al_2O_3$-SiC composites owing to its relatively lower density and the presence of ${\gamma}-Al_2O_3$ and ${\gamma}-Al_{2.67}O_4$. The greatest hardness and $K_{1C}$ were 20.37 GPa for the composite fabricated using $Al_2O_3-SiC_w$, and $4.9MPa{\cdot}m^{1/2}$ using $Al_2O_3-SiC_w-SiC_p$, respectively, which were much improved over those from the monolithic $Al_2O_3$.

• Steel and Composite Structures
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• v.35 no.5
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• pp.627-634
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• 2020

The past years were marked by an increase in the use of wood waste in civil and mechanical constructions. Date palm waste remains also one of the most solicited renewable and recyclable natural resources in the composition of composite materials. In Algeria, a great amount of this type of plant wastes accumulates every year. In order to make use of this waste, a new wood-epoxy composite material based on date palm petiole particleboard is developed. It makes use of date palm petiole particleboard as reinforcement and epoxy resin as matrix. The size of the particles reinforcement are between 1~3 mm and proportion of reinforcement used is 37%. In this work, experimental and numerical studies are conducted in order to characterize the wood fibre-epoxy plates. Firstly, experimental modal analysis test was carried out to determine Young's modulus of the elaborated material. Then, in order to validate the results, compression test was conducted. Furthermore, additional information about the shear modulus of this material is obtained by performing an experimental modal analysis to extract the first torsional mode. Moreover, a finite element model is developed using ANSYS software to simulate the vibration behaviour of the plates. The results show a good agreement with the experimental modal analysis, which confirms the values of Young's modulus and shear modulus.

• Journal of Korean Society of Water and Wastewater
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• v.24 no.3
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• pp.267-276
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• 2010

Many plants have been improved to adapt the target of the biological treatment processes changed from organics to nutrients since the water quality criteria of effluent was reinforced and included T-N and T-P for the municipal wastewater treatment plant. To meet the criteria of T-N and T-P, the conventional biological reactor such as aeration tank in activated sludge system is changed to the BNR (biological nutrient removal) processes, which are typically divided into three units as anaerobic, anoxic and oxic tank. Therefore, the solid separation process should be redesigned to fit the BNR processes in case of the application of the DAF (dissolved air flotation) process as an alternatives because the solid-liquid separation characteristics of microbial flocs produced in the BNR processes are also different from that of activated sludge system as well. The results of this study revealed that the microbial floc of the anaerobic tank was the hardest to be separated among the three steps of the unit tanks for the BNR processes. On the contrary, the oxic tank was best for the removal efficiency of nutrients as well as suspended solid. In addition, the removal efficiency of nutrients was much improved under the chemical coagulation treatment though coagulation was not indispensable with a respect to the solid separation. On the other hand, in spited that the separation time for the microbial floc from the BNR processes were similar to the typical particles like clay flocs, over $2.32{\times}10^3$ ppm of air volume concentration was required to keep back the break-up of the bubble-floc agglomerates.

• The Journal of Korean Academy of Prosthodontics
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• v.39 no.6
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• pp.682-697
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• 2001

This investigation evaluated the fracture toughness($K_{IC}$) of eight currently available core materials, and relate the fracture toughness value to fractography analysis and surface characteristics using a atomic force microscope (AFM). Single-edge notched (SEN) test specimens (n=10) and compact tension (CT) test specimens (n=10) were prepared conforming to the ASTM Standard E-399 for a high copper amalgam, three composite core materials (Core-Max II, Core Paste, Bisfil Core), two reinforced composite core materials (Ti-Core, Ti-Core Natural), a resin-modified glass ionomer core material (Vitremer), and a conventional glass ionomer core material (Ketac-Molar). The specimens were tested with an Instron Universal Testing Machine. The maximum loads were measured to calculate the fracture toughness ($K_{IC}$). Thereafter, fracture surfaces of SEN specimens of each material were investigated for fractography analysis using scanning electron microscope. And, disc-shaped specimens with 1mm thickness were fabricated for each material and were investigated under AFM for surface morphology analysis. The results were as follows: 1. Bisfil Core showed the highest mean fracture toughness regardless of test methods. 2. For the tooth-colored materials, Ti-Core Natural exhibited the highest fracture toughness. 3. Ketac Molar showed a significantly low fracture toughness when compared with the amalgam and the composite resin core materials(p<0.05). 4. The fracture toughness values obtained with the single-edge notched test, except Ketac Molar, were higher than those obtained in the compact tension test. 5. SEM revealed that the fracture surface of high fracture toughness material was rougher than that of low fracture toughness material. 6. AFM revealed that the surface particles of the composite resins were smaller in size, with a lower surface roughness than the glass ionomer core materials.