• 제목/요약/키워드: Reference Material

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자연해수를 이용한 해수 중 영양염 분석용 표준물질 개발 (Development of Reference Material Using Natural Seawater for Nutrient Analysis in Seawater)

  • 노태근;강동진;김은수;강성현;조성록;이정무;박은주;문초롱
    • 한국해양학회지:바다
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    • 제20권1호
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    • pp.29-35
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    • 2015
  • 해수 중 용존 영양염은 해양 내 물질순환을 이해하는 가장 기초적인 자료로 전 지구적 환경변화를 감지하는데 필수 생지화학 성분으로 그 중요성이 인식되고 있다. 분석능력이 다양한 연구자들에 의해서 상이한 시공간에서 측정된 용존 영양염 자료의 상호 비교를 위해 영양염 표준물질의 필요성이 증가하고 있다. 본 연구는 경기도 시화호 내측연안, 울진의 인근 연안 표층수와 동해 울릉분지 표층과 1500m에서 채취된 해수를 여과, 멸균하여 제조한 영양염 표준물질의 균질성과 안정성에 대하여 다루었다. 본 연구에서 제작된 영양염 표준물질은 해외에서 제조되는 영양염 표준물질과 유사한 균질성을 가지고 있다. 제조 후 3-13개월 동안 영양염 농도가 일정한 방향으로 감소하거나 증가하는 경향이 관측되지 않았으며 이 보다 더 긴 기간 동안의 안정성은 지속적인 모니터링이 필요하다.

동위원소희석-질량분석법을 이용한 화장품 크림 중 히드로코르티손 인증표준물질 개발 연구 (A study on the development of hydrocortisone certified reference material in cosmetic cream using isotope dilution-mass spectrometry)

  • 이채홍;허지선;정은지;김현아;엄민영
    • 분석과학
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    • 제37권3호
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    • pp.166-173
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    • 2024
  • 스테로이드는 혈관 확장을 조절하여 일시적인 피부결 향상 및 미백 효과가 있으나, 장기간 사용 시 부작용이 발생하여 국내의 화장품에는 사용할 수 없는 원료로 지정 및 관리 중이며, 지속적으로 기능성 화장품에서 검출되어 회수 및 판매 중지 등과 같은 이슈가 발생하고 있다. 본 연구는 스테로이드의 종류인 히드로코르티손의 분석을 위한 인증표준물질의 개발에 목적을 두고 실험을 수행하였다. 크림형 화장품 매질의 후보표준물질을 제조하였으며 ISO Guide 35의 절차에 따라 수행하였다. 동위원소희석-질량분석법(ID-MS)을 적용하여 균질성, 단기 안정성, 장기 안정성 평가를 수행하였으며, 소급성 연결을 위해 미국국립표준기술연구소(NIST)의 일차표준물질을 사용하여 인증값을 결정하였다. 향후 KOLAS로부터 ISO 17034에 따라 인증표준물질로 인정 후 국제 표준물질 데이터베이스(COMAR)에 등록하여 국내·외 관련 산업계 및 시험기관에 보급할 예정이다.

A LINKING METHOD OF INFORMATION FACTORS FOR ADOPTING STANDARD MATERIALS INTO APARTMENT HOUSING CONSTRUCTION

  • Geun-Soo Park;Seok-Ho Lim
    • 국제학술발표논문집
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    • The 3th International Conference on Construction Engineering and Project Management
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    • pp.1148-1154
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    • 2009
  • This study focus on the suggestion of application manual using assembling reference plane design & standard finish material basis upon material classification code. We see it will function as a tool of a linkage between building design and construction standarization in order to enlarge the applicability of house building material that is produced by the module plan. For a estabilishing of this condition, it is neccessary to link the standardization's result of material--design--construction field. According to this neccessity, we are going to suggest information factor that can make relative business manager easily approach to the standardization practical task.

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제로에너지빌딩의 기술 패키지 구성을 위한 성능 기준 및 성능 측정 방법에 관한 연구 (A Study on the Performance Measuring Methods and Standard for the Technical Package in Zero Energy Building)

  • 성욱주;임민엽;김석현;조수
    • 한국건축친환경설비학회 논문집
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    • 제12권6호
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    • pp.543-556
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    • 2018
  • Zero energy building was attended for energy consumption minimization by the energy saving technology about building heating and cooling energy consumption and the renewable energy production facility. So the government has supported the zero energy building supply for decreasing green gas emissions. The study about inventory of zero energy building has many proceeding. That inventory need the information of material and equipment. So information of material and equipment about zero energy building must be included for the zero energy building realization. Actually the database of zero energy building inventory construction through the inventory established studies has difficult because the database need many information. In this study, author proposed the test methods and performance reference for upload at inventory. It was constructed to material - module - package. Also the author analyzed the construction of the technical package for zero energy building. The author separated performance category to the energy performance for energy analysis and other performance for confirmed the durability, stability and etc. This performance category proposed the table. The test methods of material and equipment in the passive package and active package proposed to the international standard and korea standard basically korea standard. Also the performance reference was proposed to korea legal standard and various standard by this study results. And the authors proposed the table of performance value, test methods, performance reference. By result of this study, the test methods and performance reference will be used the basic data for inventory of zero energy building.

SRM의 안정된 발전을 위한 지령전류 제한에 관한 연구 (Reference Current Limitation Strategy for Stable Generation of SRM)

  • 강유정;박성준;안진우
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 춘계합동학술대회 논문집
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    • pp.6-10
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    • 2002
  • A Switched Reluctance Generator attracts much attention because of high efficiency, simple controllability, with traction drive. But the theories that have been adopted as SRG control methods up to the present are complicated. This paper proposes reference current limitation strategy for stable generation of SRM. The proposed method is verified by simulation and experiments.

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ABS 중 phthalates 가소제 CRM 개발에 대한 연구 (A study on the development of phthalate plasticizers CRM in ABS resin)

  • 정정설;박정우;유석;권성일;홍성택;선일식;박천민;최창휴
    • 분석과학
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    • 제25권5호
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    • pp.273-283
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    • 2012
  • 현재 RoHS 및 REACH, CPSC 등에서 phthalates 가소제를 유해물질로 분류하여 규제하고 있는 실정이다. 이러한 국제환경규제에 대응하기 위해 phthalates 가소제 정량분석용 ABS 인증표준물질을 개발하였으며 인증 대상물질은 DMP, DEP, DBP, BBP, DEHP, DnOP이다. 후보물질은 전기 전자제품에 많이 사용되고 있는 ABS 수지에 phthalates 가소제 6가지 물질을 혼합한 후 쌍축압출기(twin screw extruder)를 이용하여 압출, 냉각, 펠렛, 건조의 과정을 거쳐 제조하였으며 ISO Guide 35의 절차에 따라 인증하였다. 동위원소희석 질량분석법(ID-GC/MS)을 이용하여 균질성, 단기안정성 및 장기안정성을 평가하였으며, 소급성 확립을 위해 한국표준과학연구원(KRISS)의 일차표준물질을 이용하여 인증값을 결정하였다. 향후 인증표준물질로서 인증을 받은 후, 국제 표준물질 데이터베이스(COM AR:code of reference material)에 등록하고 국내 외 산업체 및 시험기관에 보급할 예정이다.

기준저항 보상회로를 이용한 비냉각형 볼로미터 검출회로의 설계에 관한 연구 (A Study on the Design of a ROIC for Uncooled Bolometer Thermal Image Sensor Using Reference Resistor Compensation)

  • 유승우;곽상현;정은식;황상준;성만영
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2008년도 하계학술대회 논문집 Vol.9
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    • pp.148-149
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    • 2008
  • As infrared light is radiated, the CMOS Readout IC (ROIC) for the microbolometer type infrared sensor detects voltage or current when the resistance value in the bolometer sensor varies. One of the serious problems in designing the ROIC is that resistances in the bolometer and reference resistor have process variation. This means that each pixel does not have the same resistance, causing serious fixed pattern noise problems in sensor operations. In this paper, Reference resistor compensation technique was proposed. This technique is to compensate the reference resistance considering the process variation, and it has the same reference resistance value as a bolometer cell resistance by using a comparator and a cross coupled latch.

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초고압용 피뢰기 산화아연소자의 전기적 특성 평가 (Evaluation of Electrical Characteristics of Metal Oxide Varistors for Surge Arresters)

  • 조한구;윤한수;김석수;한세원
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2005년도 춘계학술대회 논문집
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    • pp.46-49
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    • 2005
  • This paper presents the electrical characteristics of metal oxide varistors for lightning surge arresters. ZnO varistors were fabricated with typical ceramic production methods and two types of varistors were also prepared to be compared. The nominal discharge current and line discharge class of those varistors are $10kA(8/20{\mu}s)$ and class 3, respectively. The diameter of varistors manufactured and prepared were in the range of 61.6~65.0mm and the thickness of those were in the range of 27~42.52mm. The reference and residual voltage were tested and reference and residual voltage per 1mm and the ratio of reference and residual voltage were calculated. The reference voltage per 1mm of varistors manufactured was about 175V/mm but that of A's and B's varistors was nearly 200V/mm. The residual voltage exhibited the same trends as the reference voltage, so the reference and residual voltage per 1mm of domestic varistors should be increased. According to the results of tests, it is thought that if the reference and residual voltage per 1mm were increased to 200V/mm and 330V/mm, domestic ZnO varistors would be possible to apply to the station class arresters in the near future.

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Reference Spent Fuel and Its Characteristics for a Deep Geological Repository Concept Development

  • Choi, Jong-Won;Ko, Won-Il;Kang, Chul-Hyung
    • Nuclear Engineering and Technology
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    • 제31권6호
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    • pp.23-38
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    • 1999
  • This study addresses the reference spent fuel and its characteristics for developing a geological repository concept. As a disposal capacity of the reference repository system to be developed, spent fuel inventories were projected based on the basis of the Nuclear Energy Plan of the Long-term National Power Program. The reference spent fuel encompassing a variability in characteristics of all existing and future spent fuels of interest was defined. Key parameters in the reference fuel screening processes were the nuclear and mechanical design parameters and the burnup histories for existing spent fuels as of 1996 and for future spent fuels with the more extended burnup the initial enrichment and its expected turnup. The selected reference fuel was characterized in terms of initial enrichment, bumup, dimension, gross weight and age. Also the isotopic composition and the radiological properties are quantitatively identified. This information provided in this study could be used as input for repository system development and performance assessment and applied in fuel material balance evaluation for the various types of back-end fuel cycle studies.

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건설재료의 안전적 제어를 위한 표준물질 (Standard Reference Materials) 도출 (Study on the Development of Standard Reference Materials for Safety Control of Construction Materials)

  • 이동규;이건우;최명성
    • 한국안전학회지
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    • 제32권5호
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    • pp.54-61
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    • 2017
  • The purpose of this study is to develop standard reference materials for safety control of construction materials considering the required performance of standard materials including flow performance incorporating particles. The flow characteristics of concrete are very complicated depending on mixing proportions of constituent materials, admixtures, amount of mixing, type of mixer, time of mixing, temperature and so forth. Uncertainties and multidimensional properties of concrete have been evaluated through various studies but there are few researches for the development of standard reference material. In this study, based on the rheological concept, the flow performance of construction materials was evaluated to understand the properties of standard reference materials and was finally obtained representing materials which simulate the standard reference materials.