• Title/Summary/Keyword: Real samples

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Investigation on the Effects of Air-Damping on the Sound Absorption Coefficients Measured in the Tube (관내법 시험시 Air-Damping 이 흡음계수에 미치는 영향 고찰)

  • 정완섭;서재갑;이두희;황재호
    • Journal of KSNVE
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    • v.7 no.5
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    • pp.797-801
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    • 1997
  • This paper raises issues in testing the absorption coefficients of sound-absorptive samples using the standing wave apparatus according to the Korean standard of KS F 2814. The standard code does not consider any effect of air-damping which is significant in testing relatively low sound-absorptive samples. This limitation has been shown to yield much variation of sound absorption coefficients for recent samples tests whose coefficients are less than 10%. An improved method of calculating the sound absorption coefficients is proposed in this work and its effectiveness in real test is also illustrated. Finally, the guideline for the modification of our national standard code KS F 2814 is proposed.

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Nondestructive Quantification of Intact Ambroxol Tablet using Near-infrared Spectroscopy (근적외분광분석법을 사용한 암브록솔 정제의 비파괴적 정량분석)

  • 임현량;우영아;김도형;김효진;강신정;최현철;최한곤
    • YAKHAK HOEJI
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    • v.48 no.1
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    • pp.60-64
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    • 2004
  • Near-infrared (NIR) spectroscopy was used to determine rapidly and nondestructively the content of ambroxol in intact ambroxol tablets containing 30 mg (12.5% m/m nominal concentration) by collecting NIR spectra in range 1100-1750 nm. The laboratory-made samples had 10.3∼15.9% m/m nominal ambroxol concentration. The measurements were made by reflection using a fiber-optic probe and calibration was carried out by partial least square regression (PLSR) with autoscaling. Model validation was performed by randomly splitting the data set into calibration and validation data set (7 samples as a calibration data set and 5 samples as a validation data set). The developed NIR method gave results comparable to the known values of tablets in a laboratorial manufacturing Process, standard error of calibration (SEC) and standard error of prediction (SEP) being 0.49% and 0.49% m/m respectively. The method showed good accuracy and repeatability NIR spectroscopic determination in intact tablets allowed the potential use of real time monitoring for a running production process.

Determination of Trace Elements in Urine Samples by Graphite Furnace Atomic Absorption Spectrophotometry (흑연로 원자흡수분광광도법에 의한 뇨시료 중 흔적량 원소의 정량)

  • Choi, Chong-Moon;Choi, Hee-Seon;Park, Chang Joon;Kim, Young-Sang
    • Analytical Science and Technology
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    • v.7 no.4
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    • pp.555-561
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    • 1994
  • A method was described for the graphite furnace atomic absorption spectrophotometric determination of trace cadmium, copper, chromium and lead in urine samples. The elements were directly determined without any other treatments. The ash temperature was intensively optimized to improve the large background by the removal of organic materials and alkali and alkali earth metals in urine samples. Two kinds of standard solutions were used to plot calibration curves. From the recovery data, it could be confirmed that the analytical results with the synthetic urine matrix similar to real urine were more accurate than with a deionized water matrix.

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A Study on the Development of System for the Micro-Volume Samples Analysis (극미량 시료분석을 위한 시스템 개발에 대한 연구)

  • Lee, Sang Wook;Lee, Jin Ho
    • Journal of the Korean Society for Precision Engineering
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    • v.33 no.9
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    • pp.699-706
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    • 2016
  • Assay of biomolecules based on absorption spectroscopy is a sensitive, minute, quantitative, rapid and real-time process. UV-vis spectrometry has inherent advantages for use in analytical applications. To reduce the consumption of scarce samples, a new generation of miniaturized UV-vis spectrometric systems has been developed. This study determined empirically and through simulations the feasibility of assaying biomolecules by means of UV-vis spectrometry. This paper also reports a fully integrated portable micro-detection equipment system that utilizes a micro-optical path for analysis of micro-volume samples.

Detection of Al3+ by fluorescent turn-on nitrogen/sulphur-binary doped carbon dots

  • Siti Raudhatul Kamali;Chang-Nan Chen;Tai-Huei Wei
    • Analytical Science and Technology
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    • v.36 no.4
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    • pp.161-169
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    • 2023
  • In this study, a straightforward and precise nitrogen/sulphur-codoped carbon dots (N/S-CD) was produced using a microwave irradiation approach. The N/S-CD was formulated from succinic acid (SA), bis-(3-aminopropyl)-amine (BAPA), and sodium thiosulphate (STS) as sources of carbon, nitrogen, and sulphur, respectively. The synthesized N/S-CD established a valuable quantum yield (QY) of 70 % and was sensitive to aluminium ion (Al3+) with a detection limit of 0.21 µM and a linear concentration range of 0-100 µM. When detecting Al3+ in real water samples, the N/S-CD resulted in a satisfactory recovery in the range of 91.14 %-103.37 %. Thus, the proposed study is very promising for Al3+ detection in environmental water samples.

Evaluation of Airborne Volatile Organic Compounds Concentrations During Nail Art Practicing for College Students (대학 네일아트 실습 중 발생하는 휘발성 유기화합물의 공기 중 농도 평가)

  • Park, Yunkyung;Choi, Inja;Choi, Hyeyoung;Ahn, Jaekyoung;Choi, Sangjun;Kim, Sujin;Kim, Hyunseo
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.29 no.4
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    • pp.452-463
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    • 2019
  • Objectives: The purpose of this study is to evaluate airborne concentrations of volatile organic compounds(VOCs) during nail art practice by college students. Methods: Personal samples for students were measured using passive samplers(OVM 3500) during three kinds of practice, including polish nail, gel nail and acrylic French sculpture at two universities located in Gyeongsangbuk-do Province. We also monitored area concentrations using active samplers and real-time total VOC monitors(ppbRAE 3000). All samples were analyzed with a gas chromatography flame ionized detector. Statistical analysis for monitored data were conducted using a web-based Bayesian toolkit, EXPOSTATS(www.expostats.ca). Results: Twenty-four personal samples and ten area samples were collected and five chemicals(acetone, butyl acetate, ethyl acetate, ethyl methacrylate(EMA) and methyl methacrylate(MMA)) were detected. Acetone was detected in all personal samples and ranged from 2.58 ppm to 50.3 ppm. EMA was detected in all personal and area samples with a maximum concentration of 9.78 ppm during acrylic French sculpture. Personal exposure levels to acetone, butyl acetate and mixtures were significantly higher with high occupant density (p<0.05). Geometric mean (GM) concentrations of 3.61 ppm for EMA personal samples were significantly higher than that of area samples, 1.5 ppm (p<0.05). Since there was no local ventilation, total VOC concentration continued to increase as the practice progressed. Conclusions: In order to minimize VOCs exposure for trainees, it is necessary to introduce a local ventilation system and maintain adequate occupant density.

Study on Real Time Sensor Monitoring Systems Based on Pulsed Laser for Microplastic Detection in Tap Water (펄스 레이저 기반 담수용 미세 플라스틱 실시간 센서 모니터링 시스템 연구)

  • Han, Seung Heon;Kim, Dae Geun;Jung, Haeng Yun;Kim, Seon Hoon
    • Journal of Sensor Science and Technology
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    • v.28 no.5
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    • pp.294-298
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    • 2019
  • Pulsed laser-based optical sensor monitoring systems for real time microplastic particle counting are proposed and developed in this study. To develop our real time monitoring system, we used a 450 nm pulsed laser and a photomultiplier with very high quantum efficiency. First, we demonstrated that the microplastic particle counting system could detect standard micro bead samples of 100, 250, and $500{\mu}m$ in river water. We then performed research concerning pulsed laser-based optical spectral sensor systems for real time microplastic monitoring. Additionally, we demonstrated that the real time microplastic remote monitoring system using LoRa communications could detect microplastic in the tap water resource protection area.

A Data Driven Motion Generation for Driving Simulators Using Motion Texture (모션 텍스처를 이용한 차량 시뮬레이터의 통합)

  • Cha, Moo-Hyun;Han, Soon-Hung
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.7 s.262
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    • pp.747-755
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    • 2007
  • To improve the reality of motion simulator, the method of data-driven motion generation has been introduced to simply record and replay the motion of real vehicles. We can achieve high quality of reality from real samples, but it has no interactions between users and simulations. However, in character animation, user controllable motions are generated by the database made up of motion capture signals and appropriate control algorithms. In this study, as a tool for the interactive data-driven driving simulator, we proposed a new motion generation method. We sample the motion data from a real vehicle, transform the data into the appropriate data structure(motion block), and store a series of them into a database. While simulation, our system searches and synthesizes optimal motion blocks from database and generates motion stream reflecting current simulation conditions and parameterized user demands. We demonstrate the value of the proposed method through experiments with the integrated motion platform system.