• Title/Summary/Keyword: Reaction experiment

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Utilization of Seawater in the Production of Artificial Zeolite from Fly Ash (석탄회 이용 인공제올라이트 제조시 바닷물 활용효과)

  • Lee, Deog-Bae;Lee, Kyung-Bo;Henmi, Teruo
    • Korean Journal of Soil Science and Fertilizer
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    • v.31 no.4
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    • pp.334-341
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    • 1998
  • Sodium hydroxide concentrations were adjusted to 2.0, 2.5, 3.0 and 3.5M by dissolution in seawater. The fly ash was hydrothermally reacted with sodium hydroxide solutions (1:8, W:V) at $100^{\circ}C$ under the closed system. X-ray diffractogram proved that Na-P1 type zeolite was produced from bituminous coal fly ash. It is different from the X-ray of artificial zeolite produced by using sodium hydroxide solution dissolving in distilled water. Solid sieve structure was developed well by hydrothermal reaction with the ash and 3.0M sodium hydroxide. However chinks were observed in the structure of the product by 3.5M sodium hydroxide. CEC of the artificial zeolite was $244.5cmol^+\;kg^{-1}$ at 2.0M, 259.8 at 3.0M, 263.4 at 3.0M and 179.8 at 3.5M after 24 hours hydrothermal reaction; Artificial zeolite having high CEC, above $244.5cmol^+\;kg^{-1}$ could produce by using lower concentration of NaOH prepared in seawater than other production methods.

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A Fracture Study on the Bonded DCB Specimen of the Mode III Type with Aluminum Foam (알루미늄 폼으로 된 Mode III 형의 접합된 DCB 시험편에 대한 파괴 연구)

  • Lee, Jung-Ho;Cho, Jae-Ung;Cheon, Seong-Sik
    • Composites Research
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    • v.28 no.4
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    • pp.191-196
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    • 2015
  • In this study, the static analysis and experiment were carried out on DCB specimens manufactured with aluminum foam in order to investigate the fracture toughness at the adhesive joint of the structure bonded with adhesive. In case of static analysis, all specimen models were shown to have the maximum reaction force when the forced displacement proceeded as much as 5 mm. The maximum reaction forces became 0.25 kN, 0.28 kN and 0.5 kN respectively in cases of specimen thicknesses of 35 mm, 45 mm and 55 mm. Two specimens in case of static experiment were selected to verify these analysis results. The maximum reaction forces were shown when the forced displacement proceeded as much as 5 to 6 mm. The maximum reaction forces became 0.22 kN and 0.3 kN respectively in cases of specimen thicknesses of 35 mm and 45 mm. By comparing the derived results, it could be shown that there was not much difference between the data of analyses and experiments. Therefore, It is inferred that the study data can be secured with only analysis by no extra experimental procedure. It is thought that the mechanical properties at the structure bonded of DCB with the type of mode III can be analyzed systematically.

Effect of Cooling Hands in the Cold Water for the Physiological Responses and Clothing Comfort -Focused on Vascular Hunting Reaction, Thermal Sensation and Pain Sensation- (손의 한랭자극이 인체생리반응과 의복의 쾌적성에 미치는 영향 -한랭혈관반응, 온랭감각, 한랭통증을 중심으로-)

  • 이원자
    • The Research Journal of the Costume Culture
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    • v.12 no.2
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    • pp.279-289
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    • 2004
  • This study was conducted to compare the hunting reaction of finger in the cold water. Finger skin temperature is measured the left middle finger tip immersion in cold water of 5℃ for 30 minutes and measurements were made on finger skin temperature(Ts), thermal comfort, and cold pain sensations during the experiment at the spring (March) and Winter(December). Results were follows. Is before immersion was at the highest in spring and at the lowest in winter and was closely related to the indoor temperature Ts during immersion and recovery. Mean of finger skin temperature(MST), the skin temperature at the first rise(TTR) and amplitude of finger skin temperature reaction during immersion(AT) were significant higher in spring than that in winter(P<.01). The lowest skin temperature(LST) during the cold water immersion were significantly higher in spring than that in winter (P<.05). The frequency of the appearance of cold-Induced vase dilation(CIVD) was higher in spring than that in winter. However, time for the first temperature(TTR) and recovery time(RT) had no seasonal variation. In addition, cold pains during immersion were felt more strongly in spring than in winter. Local thermal sensation, finger thermal sensation in dynamic state during hand immersion was different from that in the Winter. Spring was slowly cold in cold water immersion.

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Selective Removal of Toxic Heavy Metals in Fe-Coagulants (철염 응집제 중 유독성 중금속의 선택적 제거)

  • 박상원
    • Journal of Environmental Science International
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    • v.8 no.3
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    • pp.393-397
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    • 1999
  • Among various reactions which metal sulfides can undergo in the reducing environment, the lattice exchange reaction was examined in a attempt to selectively remove heavy metal ions contained in the Fe-Coagulants acid solution. We have examined Zeta potential along with pHs to investigate surface characteristics of ${FeS}_{(s)}$. As a result of this experiment, zero point charge(ZPC) of FeS is pH 7 and zeta potential which resulted from solid solution reaction between Pb(II) and ${FeS}_{(s)}$ is similar to that of ${PbS}_{(s)}$. Solubility characteristics of ${FeS}_{(s)}$ is appeared to that dissolved Fe(II) concentration increased in less than pH 4, and also increased with increasing heavy metal concentration. Various heavy metal ions(Pb(II), Cu(II), Zn(II)) contained in Fe-coagulants acid solution were removed selectively more than ninety-five percent in the rang of pH 2.5~10 by ${FeS}_{(s)}$. From the above experiments, therefore, We could know that the products of reaction between heavy metal ions and $FeS_{(S)}$ are mental sulfide such as $PbS_{(S)}$, $CuS_{(S)}$ and $ZnS_{(S)}$.

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Removal Technology of NOx Using V2O5/TiO2 Catalyst Impregnated Ceramic Candle Filters (바나디아 촉매담지 세라믹 캔들필터를 이용한 질소산화물 제거기술)

  • Lee, Dong-Sub;Park, Jin-Sick
    • Journal of Environmental Science International
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    • v.16 no.9
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    • pp.1077-1083
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    • 2007
  • [ $V_2O_5/TiO_2$ ] catalyst impregnated ceramic candle filters are in principle, capable of performing shallow-bed dust filtration plus a catalytic reaction, promoted by a catalytic deposited in their inner structure. Pilot-scale $V_2O_5/TiO_2$ catalyst impregnated ceramic candle filters were prepared, characterized and tested for their activity towards the SCR reaction. The effect on NO conversion of operating temperature, gas hourly space velocity, amount of deposited catalyst, pressure drops and long-term experiment (life of catalytic filter) was determined. The following effects of $V_2O_5/TiO_2$ catalyst impregnated ceramic candle filters in SCR reaction are observed: (1) It increases the activity and widens the temperature window for SCR. (2) When the content of $V_2O_5$ catalyst increases further from 3 to 9wt.%, activity of NO increases. (3) NO conversion at first increases with temperature and then decreases at high temperatures (above $400^{\circ} over), possibly due to the occurrence of the ammonia oxidation reaction.

The Effect of Temperature and pH on Bromate Formation by Ozonation (오존처리시 Bromate생성에 미치는 온도 및 pH의 영향)

  • Lee, Mu Gang;Kim, Yeong Cheol;Choe, Jong Won
    • Journal of Environmental Science International
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    • v.13 no.7
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    • pp.667-674
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    • 2004
  • The objective of this study was to investigate the effects of pH and temperature on the formation of bromate, which is ozonation by-products, during ozonation. In this experiment, the operating parameters including pH 3 ~ 10 and temperature 15 ~ $30^{\circ}C$ were studied. Through the study for the bromate formation, reaction rate constant, and ozonation effect index on pH and temperature, the results obtained are as follows. At the same initial pH condition, the increase of pH shown similar trends even if the reaction variables such as temperature and reaction time of ozonation were exchanged. As pH and temperature were increasing, the bromate concentration was increased but bromine(HOBr+OBr) was decreased with increasing pH from 3 to 10. The activation energy(J/mol) for bromate formation decreased with increasing pH. The rate constants of bromate formation for the reaction of ozone and bromide, and ozone dosage coefficient$(K_{0})$ increased with temperature and pH. Ozonation effect index(OI) decreased with increasing temperature and pH.

A Quantitative Vigilance Measuring Model by Fuzzy Sets Theory in Unlimited Monitoring Task

  • Liu, Cheng-Li;Uang, Shiaw-Tsyr;Su, Kuo-Wei
    • Industrial Engineering and Management Systems
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    • v.4 no.2
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    • pp.176-183
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    • 2005
  • The theory of signal detection has been applied to a wide range of practical situation for a long time, including sonar detection, air traffic control and so on. In general, in this theory, sensitivity parametric index d' and bias parametric index $\beta$ are used to evaluated the performance of vigilance. These indices use observer's response "hit" and "false alarm" to explain and evaluate vigilance, but not considering reaction time. However, the reaction time of detecting should be considered in measuring vigilance in some supervisory tasks such as unlimited monitoring tasks (e.g., supervisors in nuclear plant). There are some researchers have used the segments of reaction time to generate a pair of probabilities of hit and false alarm probabilities and plot the receiver operating characteristic curve. The purpose of this study was to develop a quantitative vigilance-measuring model by fuzzy sets, which combined the concepts of hit, false alarm and reaction time. The model extends two-values logic to multi-values logic by membership functions of fuzzy sets. A simulated experiment of monitoring task in nuclear plant was carried out. Results indicated that the new vigilance-measuring model is more efficient than traditional indices; the characteristics of vigilance would be realized more clearly in unlimited monitoring task.

Production of Fine Tantalum Powder by Electronically Mediated Reaction (EMR) (도전체 매개반응(EMR)법에 의한 미세 Ta 분말 제조)

  • Park Il;Lee Chuel Ro;Lee Oh Yeon
    • Korean Journal of Materials Research
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    • v.14 no.10
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    • pp.719-724
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    • 2004
  • Production of fine tantalum powder by calciothermic reduction of tantalum oxides ($Ta_{2}O_5$) pellet through an electronically mediated reaction (EMR) has been investigated. $Ta_{2}O_5$ pellet feed and reductant calcium-nickel (Ca-Ni) alloy were charged into electronically isolated locations in a molten $CaCl_2$ bath. The current flow through an external path between the feed (cathode) and reductant (anode) locations was monitored. The current approximately 4.7A was measured during the reaction in the external circuit connecting cathode and anode location. Tantalum powder with approximately 99 $mass\%$ purity was readily obtained after each experiment. Tantalum powder by EMR using $Ta_{2}O_5$ pellet feed was fine compared with that of metal powder by metallothermic reduction and EMR using $Ta_{2}O_5$ powder feed.

A Comparison of EEG Response between TV Advertisements focused on Information Transfer and Emotional Reaction (정보전달형 TV광고와 감성유발형 TV광고의 뇌파반응 비교)

  • Kim, Jeong-Ryong;Park, Ji-Su;Kim, Mi-Suk
    • Journal of the Ergonomics Society of Korea
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    • v.22 no.4
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    • pp.1-13
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    • 2003
  • This study has investigated psychological responses to various TV advertisements by using EEG(electroencephalogram). In particular, it was assumed that the brain wave would show different patterns depending upon the style of the advertisement that could be categorized into two such as 'information transfer' type and 'emotional reaction' type. Ten healthy males participated in the experiment. EEG signal was extracted from six lobes such as right and left frontal, right and left occipital, right and left temporal while the subjects were watching TV advertisements. Alpha and beta relative power spectrum, and beta/alpha parameter were calculated to compare two kinds of advertisement each other. Additionally, subjective questionnaire was used to examine subject's response by using adjective words and preference test. In result, significant differences were found in left frontal and right occipital lobe in terms of beta/alpha between two different advertisements. And, subjects showed different preference between two advertisements. It was shown that the current method could analyze the brain reaction to advertisement quantitatively, that presented the possibility of using it to marketing research.

A Study of BRT System to Analyze Driving Skill (운전 숙련도 분석을 위한 BRT 시스템에 대한 연구)

  • Jeon, Jong-Oh;Park, Seong-Mo;Won, Yong-Gwan
    • Journal of the Institute of Electronics Engineers of Korea CI
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    • v.48 no.1
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    • pp.65-71
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    • 2011
  • In modem society, car are the most important transportation. Thereby, car accidents has been increasing steadily. The driver is the biggest factor of car accident. Therefor, various studies about driver (reaction time, mentality, physiological signal, age, pattern of drive) are underway. In this paper, we design a embedded system for measuring the reaction time by driving skill. The proposed system is composed of measuring brake module, OBD-2 scanner and bluetooth transmission module. Also, we implement GUI program to analyze experiment result and database to store results. Though our proposed system, we can analyze driving skill.