• 제목/요약/키워드: Rapid solidification

검색결과 178건 처리시간 0.025초

Melt spinning법에 의한 n형 90% $Bi_2Te_3$+10% $Bi_2Se_3$ 열전소결체의 열전특성 (Thermoelectric Properties of N-type 90% $Bi_2Te_3$+10% $Bi_2Se_3$ Thermoelectric Materials Produced by Melt spinning method and Sintering)

  • 김익수
    • 한국분말재료학회지
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    • 제5권1호
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    • pp.50-56
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    • 1998
  • A new process using rapid solidification (melt spinning method) followed by pressing and sintering was investigated to produce the n-type thermoelectric ribbons of 90% $Bi_2Te_3$+10% $Bi_2Se_3$ doped with $CdCl_2$. Quenched ribbons are very brittle and consisted of homogeneous $Bi_2Te_3-Bi_2Se_3$ pseudo-binary solid solutions. Property variations of the materials was investigated as a function of variables, such as dopant $CdCl_2$ quantity and sintering temperature. When the process parameters were optimized, the maximum figure of merit was $2.146{\times}10^{-3}K^{-1}$.

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급냉응고법에 의한 금속 섬유제조에 관한 연구 (A Study on the Fabrication of Metal Fiber by Rapid Solidification Process)

  • 백남익;허성강;라형용
    • 한국주조공학회지
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    • 제9권5호
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    • pp.396-402
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    • 1989
  • Metal fibers of Al and stainless steel were fabricated by the PDME method and the Taylor process. Tensile strength of metal fiber produced by both the PDME method and the Taylor process was much higher than that of conventionally solidified materials. Utilizing the PDME method, Al fiber with $100\;{\mu}m$ was fabricated under Ar gas atmosphere, and stainless steel fiber with $50\;{\mu}m$ was fabricated under 0.06 Torr vacuum. Continuous fiber of stainless steel was made by the Taylor process and the surface of this fiber was smother than that fabricated by the PDME method.

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고강도 황동, 알루미늄 청동 및 인청동합금의 용탕단조 조직과 기계적 성질에 관한 연구 (A Study on the Microstructures and Mechanical Properties of Squeeze Cast High Strength Yellow Brass, Al Bronze and Sn Bronze Alloys)

  • 한요섭;이호인
    • 한국주조공학회지
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    • 제19권6호
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    • pp.484-492
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    • 1999
  • The microstructures and mechanical properties of high strength yellow brass, Al bronze and Sn bronze alloys fabricated by gravity die casting and squeeze casting were investigated. A rapid cooling of casting was enhanced by pressure applied during solidification of Cu alloys, the cooling rate of casting was more great for high strength yellow brass alloy than other Cu alloys. Grain size and phases of the squeeze cast products become refined to 1/2 level compared to gravity die castings. Squeeze cast Al bronze and high strength yellow brass has about 10-20% higher yield and tensile strength and slighter decreased or nearly same elongation, compared to gravity die cast ones. Sn bronze has nearly same strength and hardness, but shows increased in elongation, compared to gravity die cast ones.

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Thermoelectric Properties of N-type 90% $Bi_2Te_3+10%Bi_2Se_3$ Thermoelectric Materials Produced by Melt Spinning Method and Sintering

  • Kim, Taek-Soo;Chun, Byong-Sun
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.459-460
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    • 2006
  • N-type $Bi_2Te_3-Sb_2Te_3$ solid solutions doped with 1$CdCl_2$ was prepared by melt spinning, crushing and vacuum sintering processes. Microstructure, bending strength and thermoelectric property were investigated as a function of the doping quantity from 0.03wt.% to 0.10wt.% and sintering temperature from $400^{\circ}C$ to $500^{\circ}C$, and finally compared with those of conventionally fabricated alloys. The alloy showed a good structural homogeneity as well as bending strength of $3.88Kgf/mm^2$. The highest thermoelectric figure of merit was obtained by doping 0.03wt.% and sintering at $500^{\circ}C$.

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급속응고 Al-20 wt% Si 합금 분말의 ECAP를 통한 고형화 (Consolidation of Rapidly Solidified Al-20 wt% Si Alloy Powders Using Equal Channel Angular Pressing)

  • 윤승채;홍순직;서민홍;정영기;김형섭
    • 한국분말재료학회지
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    • 제11권3호
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    • pp.233-241
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    • 2004
  • In this study, bottom-up type powder processing and top-down type SPD (severe plastic deformation) approaches were combined in order to achieve both full density and grain refinement of Al-20 wt% Si powders without grain growth, which was considered as a bottle neck of the bottom-up method using the conventional powder metallurgy of compaction and sintering. ECAP (Equal channel angular pressing), one of the most promising method in SPD, was used for the powder consolidation. The powder ECAP processing with 1, 2, 4 and 8 passes was conducted for 10$0^{\circ}C$ and 20$0^{\circ}C$ It was found by microhardness, compression tests and micro-structure characterization that high mechanical strength could be achieved effectively as a result of the well bonded powder contact surface during ECAP process. The SPD processing of powders is a viable method to achieve both fully density and nanostructured materials.

급냉응고된 Ribbon을 이용한 CuAINi 형상기억합금의 결정미세화 (Grain Size Refinement in CuAlNi Shape Memory Alloy using Melt-spun Ribbon)

  • 최영택
    • 연구논문집
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    • 통권22호
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    • pp.127-139
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    • 1992
  • The mechnial properties such as fracture strength, ductility and fatigue strength of Cu shape memory alloy are lower than those of Ti-Ni SMA, because of their high elastic anisotropy and large grain size. And in order to improve the mechanical property of Cu SMA, some techniques such as casting method by addition of refining element, powder metallurgy and rapid solidification process have been studied on the refinement of the grain size of Cu SMA. This study was carried out to refine the grain size of CuAlNi SMA by applying the melt spinning method. According to this study, the conclusions are as follows; - grain size of the melt-spun ribbon was about $1\mum$ - there was not change in grain size, although increasing of hot pressing temperature -grain size of the hot-extruded specimen was about $30-40\mum$, it is more refiner than that of castings

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CoFeSiBNi 아몰퍼스 합금의 소자 크기에 대한 자기-임피던스 효과 관찰 (Magneto-Impedance Effect of CoFeSiBNi Amorphous Magnetic Films according to the size)

  • 박병규;황성우;문성욱
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.339-341
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    • 2007
  • Soft ferromagnetic materials are very useful for many sensors using magnetic materials with high permeability, low coercivity and low hysteresis loss. Among them, FeCoSiBNi amorphous magnetic films show us a good impedance change(about 3.05%/Oe, at 12MHz) by the exterior magnetic field in this experiment. These are produced by rapid solidification from the melt and the material is ejected in a jet from a nozzle and quenched in a stream of liquid. After that, we make them a shape of wire with different sizes of width. Thus, we can find that the impedance change (122.16%, at 12MHz) is occurred and the fabricated magnetic wire has the characteristics of good sensor element.

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Reverse annealing of boron doped polycrystalline silicon

  • Hong, Won-Eui;Ro, Jae-Sang
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2009년도 제38회 동계학술대회 초록집
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    • pp.140-140
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    • 2010
  • Non-mass analyzed ion shower doping (ISD) technique with a bucket-type ion source or mass-analyzed ion implantation with a ribbon beam-type has been used for source/drain doping, for LDD (lightly-doped-drain) formation, and for channel doping in fabrication of low-temperature poly-Si thin-film transistors (LTPS-TFT's). We reported an abnormal activation behavior in boron doped poly-Si where reverse annealing, the loss of electrically active boron concentration, was found in the temperature ranges between $400^{\circ}C$ and $650^{\circ}C$ using isochronal furnace annealing. We also reported reverse annealing behavior of sequential lateral solidification (SLS) poly-Si using isothermal rapid thermal annealing (RTA). We report here the importance of implantation conditions on the dopant activation. Through-doping conditions with higher energies and doses were intentionally chosen to understand reverse annealing behavior. We observed that the implantation condition plays a critical role on dopant activation. We found a certain implantation condition with which the sheet resistance is not changed at all upon activation annealing.

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급속응고 Al-Si 합금 분말의 항복과 압축거동 (Yield and Compaction Behavior of Rapidly Solidified AI-Si Alloy Powders)

  • 김형섭;장기태;조성석;천병선
    • 소성∙가공
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    • 제6권2호
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    • pp.145-151
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    • 1997
  • In order to obtain high quality products in powder metallurgy, it is important to control and understand the densification behavior of metal powders. The effect of the characters of powders on the compaction behavior was studied in this study by using three types of powders produced by the gas atomization, the centrifugal atomization and the twin roll-pulverization. The shape of the powders was a major factor in the apparent or tap density, and the deformation resistance of the matrix of the powders was a major factor in compactibility. Han's yield function (eq.2) for metal powders was simplified from the relationship based on the experimental results of copper powders. In spite of some assumptions, the calculated compaction curves using a new yield functionw was in accordance with the experimental results.

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분무 주조 과공정 Al-Si계 합금의 응력이완 및 Creep 천이 거동 (Load Relaxation and Creep Transition Behavior of a Spray Cast Hypereutectic Al-Si Based Alloy)

  • 김민수;방원규;박우진;장영원
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2005년도 춘계학술대회 논문집
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    • pp.176-179
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    • 2005
  • Spray casting of hypereutectic Al-Si based alloy has been reported to provide distinct advantages over ingot metallurgy (IM) or rapid solidification/powder metallurgy (RS/PM) process in terms of microstructure refinement. Hypereutectic Al-Si based alloys have been regarded attractive for automotive and aerospace application, due to high specific strength, good wear resistance, low coefficient of thermal expansion, high thermal stability, and good creep resistance. In this study, hypereutectic Al-25Si-2.0Cu-1.0Mg alloy was prepared by OSPREY spray casting process. High temperature deformation behavior of the hypereutectic Al-Si based alloy has been investigated by applying the internal variable theory proposed by Chang et al. The change of strain rate sensitivity and Creep transition were analyzed by using the load relaxation test and constant creep test.

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