• 소성∙가공
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• 제27권5호
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• pp.301-313
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• 2018

In this paper, tensile test was performed on pure titanium sheet (CP Ti sheet) with HCP structure in each direction to evaluate mechanical and surface properties and analyze microstructural changes during plastic deformation. We also evaluated forming limits of Ti direction in dome-type punch stretching test using a non-contact three-dimensional optical measurement system. As a result, it was revealed the pure titanium sheet has strong anisotropic property in yield stress, stress-strain curve and anisotropy coefficient according to direction. It was revealed that twinning occurred when the pure titanium sheet was plastic deformed, and tendency depends differently on direction and deformation mode. Moreover, this seems to affect the physical properties and deformation of the material. In addition, it was revealed the pure titanium sheet had different surface roughness changes in 0 degree direction and 90 degree direction due to large difference of anisotropy, and this affects the forming limit. It was revealed the forming limit of each direction obtained through the punch stretching test gave higher value in 90 degree direction compared with forming limit in 0 degree direction.

• 한국산학기술학회논문지
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• 제17권3호
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• pp.380-388
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• 2016

본 논문에서는 판형 열교환기 등에 널리 이용되고 있는 순 티타늄 판재의 프레스 성형성을 평가하기 위해 인장실험을 수행하였고 인장실험결과를 가장 잘 피팅할 수 있는 가공경화 모델을 제안하였다. 또한 항복곡면의 도출을 위해 단축변형, 평면변형, 순수전단변형 등 다양한 변형모드 하에서의 인장실험을 실시하였다. 이 제안된 모델을 Hora의 수정된 최대하중조건식에 적용하여 프레스 성형성을 평가하기 위해서 널리 사용되고 있는 성형한계선을 예측하였고 그 결과를 장출성형실험에서 구한 성형한계선과 비교하였다. 도출한 항복곡면을 잘 묘사하기 위한 이방성 항복조건식과 본 연구에서 제안된 가공경화 모델은 순 티타늄 판재의 프레스 성형성의 척도인 성형한계선을 잘 예측함을 알 수 있었다.

• Journal of Welding and Joining
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• 제34권5호
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• pp.6-12
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• 2016

This study was performed bead welding of pure titanium by using fiber laser. Since titanium is very sensitive to oxidation and nitriding during welding, it is important to compose the shielding equipment compared with different material. Thus side and coaxial shield nozzle, rail and chamber type shielding equipment are widely used to protect effectively the weld during welding. Experiments were performed by changing nozzle angle and distance using side and coaxial shield nozzle. The bead colors of gold, brown, blue, purple and yellowish white were obtained by changing variables of shield nozzle, and then its weldability was investigated. As experiment result, sound and not brominated beads were formed when side nozzle angle and distance were respectively $45^{\circ}$ and 10 mm.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 춘계학술대회 논문집
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• pp.148-151
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• 2009

This paper presents an experimental study of deep-drawing and rubber-pad forming process using titanium alloy sheet. The process and results of the work carried out to investigate the capability of the process and to optimize th process parameters to ensure a sound forming. Room and high temperature tensile tests were carried out at various process conditions and microstructural evaluation was investigated. The experimental investigation was done using 150 ton hydraulic press to produce a deep-drawn part. Both graphite lubricant and polyethylene sheet were essential for defect-free product. Regarding the rubber-pad forming, reasonable formability was obtained only for pure-Ti not for Ti-6Al-4V.

• Journal of Welding and Joining
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• 제34권6호
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• pp.69-74
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• 2016

Because the pure titanium has superior corrosion resistance and formability compared with different material, it is widely used as material of welded heat exchanger. When the welding of heat exchanger is carried out, certain area in which welding start and end are overlapped occurs. The humping of back bead is formed in the overlap area due to partial penetration. Thus in this study, the experiments were carried out by changing the length and wave shape of overlap area, and then the weldabiliay was evaluated through the observation of microstructure, the measurement of hardness and tensile-shear strength test in the overlap area. When overlap length was 9.8mm, humping bead was suppressed. The microstructure of overlap area coarsened and its hardness increased due to remelting. As a result of tensile-shear strength test in the overlap area according to applying the wave shape control, it was confirmed that the overlap area applied wave shape control had more excellent yield strength and ductility.

• Journal of Welding and Joining
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• 제28권4호
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• pp.73-80
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• 2010

In this work, the effect of welding variables on weldability of gas tungsten arc(GTA) welding was investigated with experimental analysis for a commercial pure(CP) titanium (Grade.1). The GTA welding tests on sheet samples with 0.5mm in thick were carried out at different process variables such as arc length, welding speed and electrode shape. In order to search an optimum arc length with full penetration, bead- on-plate welding before butt-welding were performed with different arc length conditions. From the bead- on-plate welding results, the optimum condition considering arc stability and electrode loss was obtained in the arc length of 0.8mm. Butt-welding tests based on the arc length of 0.8mm were carried out to achieve the optimum conditions of welding speed and electrode shape. Optimum conditions of welding speed and electrode shape were suggested as 10 mm/s and truncated electrode shape, respectively. It was successfully validated by the microstructural observation, tensile tests, micro-hardness tests and formability tests.

• 한국산학기술학회논문지
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• 제17권4호
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• pp.718-725
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• 2016

본 논문에서는 대형 선박의 판형 열교환기 등에 널리 이용되고 있는 순 티타늄 판재의 소성변형을 유한요소해석하기 위한 기초 데이터로서 순 티타늄 판재의 유동곡선을 평가하였다. 순 티타늄 판재의 프레스 가공 시에 판재에는 국부적으로 큰 소성변형이 발생하고 있다. 그러나 기존의 단축 인장실험에서 얻을 수 있는 소성변형률이 낮아서 티타늄 판재의 가공공정 설계를 위한 유한요소해석의 정밀도를 떨어뜨리는 경우가 있다. 본 연구에서는 큰 소성변형률 까지 안정적으로 성형이 가능한 유압벌지실험을 수행하여 재료의 소성변형에서 가공경화특성을 나타내는 유동곡선으로써 진응력-진변형률 선도를 구하였고 그 결과를 인장실험 결과와 비교하였다. 순 티타늄 판재의 유압벌지실험에서 재료의 변형률은 3D 디지털 영상상관법을 이용한 ARAMIS 시스템으로 실시간 측정된다. 이 유압벌지실험으로부터는 소성 변형률이 0.65 이상 까지도 안정적으로 재료의 소성유동곡선을 얻을 수 있었으며 그 결과는 Kim-Tuan 이 문헌 17[Y.S. Kim, J.H. In, Korean Acadmia-Ind. Coop. Soc.,(be in print), 2016] 의 연구에서 제안한 가공경화식으로 잘 핏팅됨을 알 수 있었다.

• Journal of Welding and Joining
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• 제34권6호
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• pp.62-68
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• 2016

Laser welding has superior characteristic such as low distortion, high welding speed, easy automation and real time control. But it is easy to occur weld defects such as porosity, crater, humping bead in the area of welding start and end. These weld defects can be suppressed by applying the wave shape control. In this study CW fiber laser was used for welding of $0.5mm^t$ pure titanium. Penetration properties were evaluated with the time of slope up and down. After then the bead shape was observed, and the maximum depth and the area of crater were measured. The bead shape of welding start area changed to be sharp with increase of slope up time and non-weld area of welding start increased. The crater and humping bead were suppressed with slope down time. The cooling rate of crater area was understood through measure of the hardness. Also, The distribution tendency of alloying elements was observed by EPMA and EDS. When wave shape control didn't applied to weld, the hardness of end weld increased due to rapid cooling rate and the hardness of rear part in the crater was higher than that of fore part. On the other hand, when the wave shape control was used for end weld, the increase of hardness in the end weld couldn't be found due to gradual cooling rate.

• 열처리공학회지
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• 제32권3호
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• pp.124-130
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• 2019

Friction stir welding is one of the interesting welding methods for titanium and its alloy which proceeds with plastic flow due to thermo-mechanical stirring and friction heat. Solid-state welding can solve severe problems such as high-temperature oxidation, interstitial oxygen diffusion and grain coarsening by liquid-state welding. Dynamic recrystallization and grain refinement can vary significantly with the plunging load and rotational speed of tool during friction stir welding, and suitable process conditions must be optimized to obtain microstructure and better mechanical characteristics. Suitable FSW conditions were 1000 kg of plunging load and 200 rpm of rotational speed and it showed YS 270 MPa, UTS 332.1 MPa, and El 17.3%, which were very similar to those of wrought titanium sheet.

• 대한치과보철학회지
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• 제38권3호
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• pp.358-359
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• 2000

Statement of problem. Confusion about the relationship of surface characteristics of implant to osteoblast cell attachment. Purpose. This study attempted to bone cell attachment to the implant surface which was modified by heat. Material and methods. Commercially pure titanium grade 2, $4{\times}4mm$ sheet 40 pieces were treated for 10 minutes with ultrasonic cleaner with methylethyl ketone, ethanol, deionized distilled water, and half of the specimen 20 pieces were heat treated in $980^{\circ}C$ for 15 minutes. All 40 specimens were autoclaves. Total 6 dishes were prepared, 3 dishes were for control group, and the other 3 dishes were for heat treatment. In fourth day, cell account was done. Conculsion. The change of surface characterization by heat treatment could affect the cell attachment in the early stage however, the change of surface characterization would not be prolonged.