• Title/Summary/Keyword: Preheating

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Fabrication of Porous TiNi Alloys by Self-propagating High-temperature Synthesis (자전연소반응에 의한 TiNi 다공체 합금 제조에 관한 연구)

  • 이상진;권대환;배승열;안인섭;김유영
    • Journal of Powder Materials
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    • v.9 no.2
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    • pp.96-102
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    • 2002
  • In the present study, equiatomic porous TiNi shape-memory alloys have been successfully prepared by self-propagating high-temperature synthesis (SHS) using elemental titanium and nickel powders. The porous TiNi alloys thus obtained have an open porous structure with about 64 vol.% porosity, and the pore size is about 1.8 mm. The effect of preheating temperature on the microstructure have been investigated. It is found that the pore size increases with increasing preheating temperature. Moreover, the preheating temperature was shown to have a significant effect on the microstructrue of the SHS-synthesized porous TiNi shape memory alloys.

A Study of Cervical Margin Distortion in Preheating Method during Soldering (관교의치(冠橋義齒) 납착시 Preheating 방법에 따른 치경부(齒經部) 변록의 적합도(適合度)에 관한 실험적 연구)

  • Kim, Won-Tai
    • Journal of Technologic Dentistry
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    • v.6 no.1
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    • pp.11-14
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    • 1984
  • The auther performed this experimental study on cervical margin distortion in preheating method during soldering. 1. In soldering methods, the method using the furnace has less distortion than the method using open-flame and longer the bridge spon, the larger the distortions. 2. Table Ⅰ Showed that buccal margin, lingual margin, mesial margin and distal margin had respectively 0.01mm, 0.02mm, 0.03mm, 0.03mm closer adaptation in 3 unit bridge than in 5 unit bridges. 3. Table II showed that buccal margin, lingual margin, mesial margin and distal margin had respectively 0.06mm, 0.07mm, 0.11mm, 0.05mm closer adaptation in 3 unit bridge than in 5 unit bridges.

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Preparation and Properties of Magnesia-Alumina Spinel by SHS (SHS 법에 의한 Magnesia-Alumina Spinel 제조와 특성)

  • 최태현;전병세
    • Journal of the Korean Ceramic Society
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    • v.33 no.2
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    • pp.235-241
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    • 1996
  • Self-Propagating high temperature synthesis(SHS) technique was used to synthesize the spinel phase of MgAl2O from MgO and Al powder. Processing factors such as mixing time preheating temperature and ignition catalyst were varied to determine the optimum condition to form MgAl2O4 phase. The reaction products were heat treated at the temperature range of 120$0^{\circ}C$ and 150$0^{\circ}C$. to observe phase transformation of unreacted materials. Processing factors such as 48 hrs-mixing 80$0^{\circ}C$-preheating and 20wt% KNO3-ignition catalyst were effective of the formation of MgAl2O spinel. An activation energy 49.7kcal/mol. was calculated to form a MaAl2O4 spinel from unreacted materials.

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Analysis of Moving Heat Source for Laser Assisted Machining of Plate by Feed Rate Control (이송속도 조절에 의한 평판 레이저 보조가공의 이동 열원해석)

  • Kim, Kwang-Sun;Lee, Choon-Man
    • Journal of the Korean Society for Precision Engineering
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    • v.28 no.12
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    • pp.1341-1346
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    • 2011
  • Currently, many researches are carried out for laser assisted machining, which is one of the important fields in materials difficult to process. However, a prediction of heat source is difficult because of moving heat source. In this paper, a thermal analysis of laser assisted machining of plate by change of heat source size is performed, and preheating temperature by adjusting the feed rate is controlled. It was recognized that the maximum preheating temperature increases according to the decrease in heat source size, and feed rate need to adjust as high speed. The results of this analysis can be used as a reference for preheating temperature prediction in laser assisted milling.

Tensile Test for Lap Welded Joints of Rebars(SD400) (일반철근(SD400) 용접 겹침이음 인장실험)

  • Park, Won-Tae;Chun, Kyoung-Sik
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.19 no.5
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    • pp.570-576
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    • 2018
  • In reinforced concrete structures, the joints of ordinary rebars are usually lap joints, which are bound by binding wires with rebars, and mechanical joints by couplers. In domestic design standards (concrete design code), welded lap joints are restricted for ordinary rebars, but overseas standards allow welded lap joints of ordinary rebars through pre-heating. This study investigated the domestic and international standards/criteria and evaluated the fracture strength by performing the tensile test on the lap welded joint of SD400 grade rebars, which is used the most in the construction sites. The weld length of the specimen for weld lap joints is based on the minimum weld length (8d) given in the KS standard (KS B ISO 17660-1). According to AWS D1.4, the preheating temperature was set to $150^{\circ}C$ for D19 and below, and $260^{\circ}C$ for D22 and above. In the test results, the tensile strength of rebars with welded lap joints exceeded the required strength (125% of the yield strength) according to the concrete design code. To analyze the effect of preheating, the tensile strength of the welded rebars after preheating was not significantly different from that of the welded rebars without preheating. The carbon equivalent content (Ceq) of the rebars used in the test was 0.45% or less. Under AWS D1.4, no preheating is required if the carbon equivalent is less than 0.45%. All specimens with a welded lap length of 8d failed by a bar fracture. The effect of preheating was confirmed to be insignificant due to the low carbon equivalent of the rebar.

In vitro Digestibility Assessment of CP4EPSPS in GM Soybean under Different Conditions of Simulated Gastric Fluid and Preheating (인공위액조건과 예열처리에 따른 GM 콩 도입단백질(CP4EPSPS)의 소화성 평가)

  • Choi, Mi-Hee;Kim, Gun-Hee
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.41 no.9
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    • pp.1310-1314
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    • 2012
  • Gastrointestinal digestibility of new proteins inserted in the food supply is a significant parameter for assessing the safety of GM foods based on the assumption that digestive stability is undesirable. In this study, we performed in vitro digestion of CP4EPSPS, a new protein, expressed in genetically modified (GM) soybean in order to evaluate its digestibility in three different ratios of simulated gastric fluid with preheating. Ratios of GM soybean to simulated gastric fluid were 2:2, 2.5:1.5, and 1.5:2 and preheating was conducted at $100^{\circ}C$ for 5 min. Electrophoresis and Western blotting were used to confirm changes in soybean protein patterns and CP4EPSPS gene expression after in vitro digestion. At ratios in which the amount of gastric fluid was equal to (2:2) or relatively higher than that of soybean (1.5:2), no CP4EPSPS (47.4 kDa) protein was detected after 15 seconds of simulated gastric fluid incubation, the earliest time interval evaluated. However, when the ratio of GM soybean to gastric fluid was 2.5:1.5, CP4EPSPS was detected in 5 min and gradually decreased according to time. After preheating, no CP4EPSPS protein was detected after 15 seconds under all conditions. From these results, we concluded that the digestibility of CP4EPSPS in simulated gastric fluid increased upon preheating. Accordingly, we suggest that it is important to account for the ratio of gastric fluid to GM food in in vitro digestibility assessment models of GM food.

A study on Residual Stress Distribution of a Repair Weldment of Casting (주철 보수용접부의 잔류응력 분포에 관한 연구)

  • 김현수;배상득;박윤기
    • Proceedings of the KWS Conference
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    • 2003.11a
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    • pp.207-209
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    • 2003
  • In FE analysis for residual stress of a casting, contact force between mould and casting material and gravity force must be considered for exact simulation. Preheating of a repair weldment had a little effects on the reduction of residual stress. However, preheating with hammer peening had a great deal of effects on the reduction of residual stress. A method for estimation of fatigue life for a repair weldment has been established.

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Experiments on Welding of Ceramics by Use of High Power Laser (고출력 레이저를 이용한 세라믹 재료의 용접 실험)

  • 변철웅
    • Journal of Welding and Joining
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    • v.12 no.2
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    • pp.39-48
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    • 1994
  • In comparison to the conventional brazing, laser welding of ceramics has advantages of direct bonding without filler material, which causes the thermal stress due to the differences of thermal expansion coefficients. In pulse-mode, laser welding of dispersion ceramic having high thermal resistance is possible at relatively low preheating temperature of $1300^{\circ}C$ In CW-mode, alumina can be welded at high preheating temperature $1500^{\circ}C$ under the condition of low feed rate of 500 mm/min, respectively. Further studies on developing mechanism of pores in the bead during laser welding of ceramics is required.

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Influences of thermal preheating of GaAs substrates on structural and optical properties of ZnS epilayers (성장 전 GaAs 기판의 열에칭 온도 변화에 따른 ZnS 에피층의 구조적, 광학적 특성)

  • 남성운;유영문;이종광;오병성;이기선;최용대;이종원
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.10 no.3
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    • pp.252-257
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    • 2000
  • To investigate the thermal preheating effect of the GaAs substrate exerted on the ZnS epilayers for the first time, ZnS epilayers were grown on the GaAs (100) substrate by hot wall epitaxy. The thermal preheating temperature was $450^{\circ}C$~$660^{\circ}C$. The full width at half maximum values of double crystal rocking curve were the smallest for the ZnS epilayers grown on the GaAs thermally preheated at around both $500^{\circ}C$ and $600^{\circ}C$. However, photoluminescence characteristics of ZnS epilayers were better at $600^{\circ}C$ than at $500^{\circ}C$. Therefore, it was shown that the optimum preheating temperature of the GaAs substrate for the growth of high quality ZnS epilayer was around $600^{\circ}C$. From these experimental results, it was shown that the crystal quality and the PL properties of ZnS epilayers were enhanced for the GaAs substrates thermally preheated at $600^{\circ}C$.

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Effects of Red Bean (Vigna angularis) Protein Isolates on Rheological Properties of Microbial Transglutaminase Mediated Pork Myofibrillar Protein Gels as Affected by Fractioning and Preheat Treatment

  • Jang, Ho Sik;Lee, Hong Chul;Chin, Koo Bok
    • Food Science of Animal Resources
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    • v.36 no.5
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    • pp.671-678
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    • 2016
  • Fractioning and/or preheating treatment on the rheological properties of myofibrillar protein (MP) gels induced by microbial transglutaminase (MTG) has been reported that they may improve the functional properties. However, the optimum condition was varied depending on the experimental factors. This study was to evaluate the effect of red bean protein isolate (RBPI) on the rheological properties of MP gels mediated by MTG as affected by modifications (fractioning: 7S-globulin of RBPI and/or preheat treatment (pre-heating; 95℃/30 min): pre-heating RBPI or pre-heating/7S-globulin). Cooking yields (CY, %) of MP gels was increased with RBPI (p<0.05), while 7S-globulin decreased the effect of RBPI (p<0.05); however, preheating treatments did not affect the CY (p>0.05). Gel strength of MP was decreased when RBPI or 7S-globulin added, while preheat treatments compensated for the negative effects of those in MP. This effect was entirely reversed by MTG treatment. Although the major band of RBPI disappeared, the preheated 7S globulin band was remained. In scanning electron microscopic (SEM) technique, the appearance of more cross-linked structures were observed when RBPI was prepared with preheating at 95℃ to improve the protein-protein interaction during gel setting of MP mixtures. Thus, the effects of RBPI and 7S-globulin as a substrate, and water and meat binder for MTG-mediated MP gels were confirmed to improve the rheological properties. However, preheat treatment of RBPI should be optimized.