• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2002년도 하계학술대회 논문집
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• pp.503-506
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• 2002

BSCCO 2212 HTS was fabricated by CFP(centrifugal forming process). The powder was initially ground in the mixing ratio of 2:2::1:2 with 10% of SrSO$_4$. The temperature increased up to 1035$^{\circ}C$ and 1200$^{\circ}C$ for melting. The melt was poured into the preheated and rotating copper mould from 200 to 600$^{\circ}C$. The specimen was not broken by thermal impact when the melting temperature was over 1050$^{\circ}C$ and copper mould was preheated over 400$^{\circ}C$ for 30min. A tube type of specimen was annealed at 840$^{\circ}C$ or 860$^{\circ}C$ in oxygen atmosphere for 24hours. Typical microstructure was analyzed in terms of CFP parameters by XRD, SEM, and EDS and also superconducting characteristics were compared.

• 한국세라믹학회지
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• 제35권4호
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• pp.311-318
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• 1998

The reaction bonded alumina ceramics with reinforced particles which have low shrinkage were pro-duced by blending of SiC or TiC or ZrO2 powders to the mixture of Al metal and Al2O3 powder. The powd-ers were attrition milled isostantically pressed and preheated tio 110$0^{\circ}C$ with a heating rate of $1.5^{\circ}C$/min The specimens were then sintered at the temperature range 1500 to 1$600^{\circ}C$ for 5 hours with a heating rate of 5$^{\circ}C$/min. The specimens showed 5-9% weight gain and 2-9% dimensional expansion through the complete oxidation of Al after preheating up to 11--$^{\circ}C$ the overall dimensional change of the specimens after the reaction sintering at 1500-1$600^{\circ}C$ was 6-12% The maximum densities were 92% theoretical. The fine grain-ed(average grain size :0.4 ${\mu}{\textrm}{m}$) microstructure were observed in the specimen with ZrO2 and SiC. But the microstructure of specimen with TiC was relatively coarse.(average grain size : 2.1 ${\mu}{\textrm}{m}$) The mullite phase was formed by the reaction of Al2O3 and SiO2 in a specimen with SiC. In the TiC contained specimen TiC was oxidized into TiO2 and finally reacted with Al2O3 to form Al2TiO5 during sintering.

• 한국주조공학회지
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• 제4권2호
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• pp.96-101
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• 1984

The morphologies of eutectic cell formed during solidification affect on the mechanical properties in high Cr cast iron. In order to investigate the influence of Si on the structure, five kinds of specimen containing 16.42% Cr with varying amount of Si (0.51%, 1.17%, 2.22%, 2.71%, 3.56%) were poured into shell mould preheated $330^{\circ}C$ at $1510^{\circ}C$. The effect of Si on matrix in hypo-eutctic Cr cast iron (2.48% C, 16.42%) were studied through its mechanical tests and observation of microstructure using of metallurgical microscope, EPMA, SEM and Image analyzer systematically. The results obtained from the above studies are as follows: 1. Because of ${\Delta}T$ decreasing with increasing Si content, the morpologies of colony change into uniform bar-type carbide from plate-type ones, moreover eutectic colony size (Ew) becomes narrow and spacing of carbide wider. 2. As Si content increases, the amount of carbides also increases and most of Cr were dissolved in carbides while Si in matrix. 3. The hardness, tensile strength and wear resistance were increasing while impact value decreased with increasing Si content. 4. In fracture section, small amount of dimple pattern was observed in less than 1.17% Si but more than 2.22% Si river pattern was presented.

• 열처리공학회지
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• 제34권4호
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• pp.185-190
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• 2021

The extrusion experiments using the 7075 aluminum billet have been performed to investigate the effects of die cooling and ram speed on the occurrence of surface defects on the extrudate. The purpose of die cooling was to suppress overheating of the extrudate at the moment of extrusion. In the present die cooling system, liquid nitrogen has been injected in to the die and sprayed to the surface of extrudate. Ram speed was either kept or varied in the range of 1.1~1.7 mm/sec. throughout one extrusion shot to check the occurrence of surface defects. Every extrusion started at a ram speed of 1.25 mm/sec. The temperature of extrudate was measured using a laser thermometer. The 7075 billet of 180 mm in diameter and 550 mm in length was preheated at 390℃ and extruded to get a single plate of 8000 mm in length, 150 mm in width and 10 mm in thickness. Each extrudate was checked by eye to find the surface defects. The microstructures were obtained in the specimen cut from each corner of the extrudate using the EBSD micrographs.

• 대한치과보철학회지
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• 제34권1호
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• pp.143-150
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• 1996

The purpose of this study was to evaluate the tensile strength of solder joint between gold alloy and nickel-chromium alloy. The specimens were made with type III gold alloys and Ni-Cr-Be alloy and Degular Lot 2 solder. Eighteen paired specimens were made, and subdivided into three groups. Group I specimens were gold alloy-gold alloy combination, Group II specimens were gold alloy-Ni-Cr alloy combination, Group III specimens were Ni-Cr alloy-Ni-Cr alloy combination. Solder block were made with solder investment(Degussa A,G, Germany) and stored in room temperature for 24 hours. To reduce the formation of metallic oxide and increase wetting properties, flux was used before preheating and soldering procedure. The specimens were preheated at $650^{\circ}C$ and flux were applied again and gas-oxygen torch was used to solder the specimen. All soldered specimens were subjected to a tensile force in the Instron universal testing machine : the crosshead speed was 1 mm/mim. Tensile strength values of three soldered joint groups were 1. Gold alloy-Gold alloy solder joint : $$48.8kg/mm^2$$ 2. Gold alloy-Ni-Cr alloy solder joint : $$30.9kg/mm^2$$ 3. Ni-Cr alloy-Ni-Cr alloy solder joint : $$31.8kg/mm^2$$ The microscopic examination of fracture site showed cohesive and combination fracture modes in gold alloy specimens, but showed all adhesive fracture modes in Ni-Cr alloy containing specimens.

• 터널과지하공간
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• 제21권1호
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• pp.33-40
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• 2011

본 연구에서는 온도와 수압이 암석의 물성 변화에 미치는 영향을 평가하였다. 온도가 암석의 물성에 미치는 영향을 평가하기 위하여 가곡광산에서 채취한 화강암과 석회암 시험편에 200, 300, 400, 500, 600, $700^{\circ}C$(석회암의 경우 $700^{\circ}C$는 제외하였음)의 열을 가하여 예열시험편을 제작하였다. 예열시험편에 대한 실내실험을 통해 비중, 유효공극률, 탄성파속도, 일축압축강도, 탄성계수, 포아송비를 측정한 결과 온도가 증가함에 따라 화강암과 석회암 예열시험편의 물성이 변하는 것으로 나타났다. 비중, 유효공극률, 탄성파속도의 급격한 변화는 화강암의 경우 $400^{\circ}C$ 이상에서 발생하였으며, 석회암의 경우에는 $300^{\circ}C$ 이상에서 나타났다. 온도에 따른 일축압축강도, 탄성계수, 포아송비의 변화도 물리적 특성의 변화와 유사한 것으로 나타났다. 예열시험편의 일축압축강도와 탄성계수로부터 유추한 500, 600, $700^{\circ}C$ 화강암 예열시험편의 GSI는 각기 81, 66, 58로 나타났으며, 400, 500, $600^{\circ}C$ 석회암 예열시험편의 GSI는 각각 76, 71, 65로 나타났다. 500, 600, $700^{\circ}C$ 화강암 예열시험편과 400, 500, $600^{\circ}C$ 석회암 예열시험편에 7.5 MPa의 수압을 가하였다. 수압을 적용한 예열시험편의 유효공극률, 탄성파속도, 일축압축강도, 탄성계수를 측정하여 평균한 결과 수압을 가하기 전 예열시험편에 비해 평균 감소량이 화강암 500, 600, $700^{\circ}C$ 예열시험편 각각에 대해서 7.6, 11.3, 14.9%로 나타났고, 석회암 400, 500, $600^{\circ}C$ 예열시험편에 대해서는 각기 8.2, 13.8, 21.9%로 평가되었다.

• Journal of Biosystems Engineering
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• 제41권1호
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• pp.43-50
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• 2016

Purpose: The present study is aimed at examining the drying characteristics of sea tangle through a combination of microwave and far-infrared drying experiment and finding the optimal drying conditions. Methods: Sea tangle was cleaned and cut into fine pieces (5mm) before they were subjected to combinational drying by microwave and far-infrared ray. The amount of specimen per drying is 2 kg. The finely cut pieces of sea tangle were preheated in a microwave dryer for three different lengths of time (10, 15, and 20 min). Subsequently, they were dried using a far-infrared dryer at tow temperatures ($90^{\circ}C$ and $100^{\circ}C$) at an air velocity of 0.8 m/s until the final moisture content reduced to 10%. Results: Sea tangle dried under the condition of 20 min of preheating in the microwave dryer and drying at $100^{\circ}C$ by the far-infrared dryer. Of the drying models verified in this study, the logarithmic model showed high accuracy with the coefficient of determination $R^2>0.7825$ and RMSE<0.1095. The rehydration ratio of sea tangle was the highest (12.87 g water/g dry matter) under the condition of 15 min of preheating in the microwave dryer and drying at $100^{\circ}C$ by the far-infrared dryer. The energy consumption for the combination of microwave and far-infrared drying was the lowest (4.78 kJ/kg water) under the condition of 20 min of preheating in the microwave dryer and drying at $100^{\circ}C$ by the far-infrared dryer. Conclusions: Considering the drying time, discoloration during drying, rehydration ratio, and energy consumption for the drying of sea tangle, the optimal drying conditions for high-quality sea tangle are 15 min of preheating in a microwave dryer and drying at $100^{\circ}C$ by a far-infrared dryer.

• 한국재료학회지
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• 제9권8호
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• pp.817-824
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• 1999

$Al_2$$O_3$-SiC 화합물 분말이 $SiO_2$, A1 그리고 C 분말들을 원료분말로 하여 SHS(self-propagating High-temperature Synthesis)법에 의해 제조되었다. 원료 분말에서의 몰비, 성형압력, 반응물의 초기온도의 영향이 생성물과 연소과정에 대해 연구되었다. $SiO_2$/A1/C계의 자전연소합성은 낮은 연소온도 때문에 $400^{\circ}C$ 이상으로 예열되어야 한다. 연소반응의 결과로서 최종생성물의 순도는 반응물의 순도보다 높았다. 이 계에서 $SiO_2$:Al:C의 적당한 몰비는 3.0:4.0:6.0이었고, free carbon은 30min 동안 $650^{\circ}C$에서 배소함으로써 제거되었다. 본 연구에서 상압소결은 $1700^{\circ}C$에서 powder bed를 사용한 표본의 분해를 제어하고 치밀한 소결체를 얻는데 매우 효과적이었다. hot-pressing으로 생성된 소결체는 이론비교밀도의 약 98%이었다.